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Published by Universitas Sumatera Utara

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Chemical Engineering, Chemistry & Bioengineering Chemistry Engineering

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Articles 349 Documents

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SIFAT-SIFAT MEKANIK KOMPOSIT POLIPROPILENA BERPENGISI ABU PEMBAKARAN BIOMASSA KELAPA SAWIT Danil Tarmizi, Kartini Noor Hafni, A. Haris Simamora
Jurnal Teknik Kimia USU Vol 3, No 1 (2014)
Publisher : Universitas Sumatera Utara

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32734/jutek.v3i1.6245

This study aimed to determine the effect of palm oil fuel ash composition of the mechanical properties of polypropylene composites. Composites made by extrusion and injection molding method by mixing polypropylene and palm oil fuel ash with filler composition, respectively 10, 15, and 20 (% w/w). Mechanical properties which tested are tensile strength, elongation at break, and impact strength. The results obtained from the study is the addition of filler palm oil fuel ash in polypropylene composites decrease the mechanical properties of the composites, such as tensile strength, elongation at break, and impact strength.

KAJIAN AWAL PEMBUATAN FILM PLASTIK (BAHAN PLASTIK PENGEMAS) DARI PATI BATANG UBI KAYU Harrison Situmorang, M. Hendra S. Ginting
Jurnal Teknik Kimia USU Vol 3, No 1 (2014)
Publisher : Universitas Sumatera Utara

Starch plastic films made from cassava stem starch by using glycerol as plasticizer and acetic acid as a catalyst gelatinized at 75 °C for 15 minutes. Starch weight, water volume, glycerol volume, and acetic acid volume were varied. The variation conditions of 3 ml of acetic acid volume (3:10 w/w) and 2 ml of glycerol volume (1:4 w/w) gave the best of tensile strength and elongation at break analysis. While at water volume variation, the tensile strength value is inversely proportional to the elongation at break. In FTIR analysis found that α-1,6 glycosidic (1010 cm-1) spectrum disappears as the effect of acetic acid presence, while the spectrum of α-1,4 glycosidic, COH, C=O, and OH shifted as the plasticization effect.

PENGARUH ASAM STEARAT TERHADAP SIFAT KETEGUHAN PATAH/MODULUS OF RUPTURE PAPAN PARTIKEL TERMOPLASTIK BEKAS BERPENGISI TEMPURUNG KELAPA Muh. Hendra S Ginting, Rosdanelli Hasibuan
Jurnal Teknik Kimia USU Vol 3, No 1 (2014)
Publisher : Universitas Sumatera Utara

The utilization of former thermoplastic and coconut shell as particle board is one way to reduce plastic waste packaging, the ratio of the former as a thermoplastic matrix and coconut shells as fillers 60:40. Purpose of this study was to determine the effect of stearic acid on properties of modulus of rupture former thermoplastic particle board filler of coconut shell. Method of shell particle board manufacturing using the extruder, starting with the modification of coconut shell particles (size 80 mesh) with stearic acid (0 g, 3 g, 6 g and 9 g in 60 ml of ethanol ) and then dried in an oven at a temperature 70oC . Matrix and coconut shell ( 60:40 ) mixed in the extruder and then printed with hot press at a temperature of 170oC, until forming particle board with a size of 200 mm x 200 mm x 10 mm. Particle board analyzed the modulus of rupture in accordance with SNI 03-2105-2006. The results showed an increase in modulus of rupture properties. The modulus of rupture is 37.402 MPa greatest.

KAJIAN AWAL PEMBUATAN PUPUK CAIR ORGANIK DARI EFFLUENT PENGOLAHAN LANJUT LIMBAH CAIR PABRIK KELAPA SAWIT (LCPKS) SKALA PILOT Fristyana Sosanty Lubis, Irvan, Dedy Anwar, Basril Amirza Harahap, Bambang Trisakti
Jurnal Teknik Kimia USU Vol 3, No 1 (2014)
Publisher : Universitas Sumatera Utara

The objective of this study is to design an organic liquid fertilizer manufacturing process from palm oil mill effluent (POME) at pilot scale. Materials used were effluent from further processing of biogas fermentation from POME and starter (mixture of molasses, yeast and effective microorganism). Variables measured were total solid (TS), volatile solid (VS), total suspended solid (TSS), volatile suspended solid (VSS), and chemical oxygen demand (COD), in addition, analysis content of liquid fertilizers was performed. The research consisted of production of starters and fermentation process. Loading rate was started from hydraulic retention time (HRT) 2,500 days and bioreactor performance was observed at HRT 100, 90 and 80 days. The results showed that COD concentration of bioreactor effluent decreased from 8,600 to 1,580 mg/l and from analysis content, liquid fertilizers are composed of nitrogen 0.14%, P2O5 0.05%, K2O 0.07%, MgO 0.01%, CaO 0.001mg/l, C-Organic 0,12%, and C/N Ratio 0.86.

PENGARUH PENAMBAHAN GLISEROL TERHADAP SIFAT KEKUATAN TARIK DAN PEMANJANGAN SAAT PUTUS BIOPLASTIK DARI PATI UMBI TALAS Rinaldi Febrianto Sinaga, Gita Minawaris Ginting, M. Hendra S Ginting, Rosdanelli Hasibuan
Jurnal Teknik Kimia USU Vol 3, No 2 (2014)
Publisher : Universitas Sumatera Utara

Bioplastics are a type of plastic made from renewable biomass sources, such as vegetable oil, corn starch, pea starch, and microbiota. Starch from tubers of talas (Colocasia esculenta) as a potential raw material for bioplastics by using glycerol as plastizicer. The purposes of the research are to know effect of adding glycerol to the properties of tensile strength and elongation at break bioplastic from starch taro tubers. In this research, the manufacture of bioplastics using casting methode with variations of starch solution (0,2 w/v, 0,3 w/v, and 0,4 w/v). The next additions to vary the volume of glycerol (1 % v, 2 % v, and 3 % v) and heating temperature of gelatin formation (60oC, 70oC, and 80oC). The results showed that bioplastics made from taro tuber starch has gelatinization temperature of 70oC. The addition of glycerol volume effect value of tensile strength and elongation at break of bioplastics. Increasing volume of glycerol will decrease tensile strength but increase elongation at break value. The best of bioplastics in this research is a variation of starch bioplastic 0,3 w/v, addition of 1 % v glycerol at a temperature of 70°C with a value of tensile strength is 18,4992 MPa and elongation at break value is 2,1290%.

PENGARUH PENAMBAHAN BERBAGAI AKTIVATOR DALAM PROSES PENGOMPOSAN SEKAM PADI (Oryza sativa) Irvan, Permata Mhardela, Bambang Trisakti
Jurnal Teknik Kimia USU Vol 3, No 2 (2014)
Publisher : Universitas Sumatera Utara

Composting process of rice husk (Oryza sativa) by adding various activators have been carried out in LPPM Training Center, University of Sumatera Utara. The purpose of this study was to compare the effect of variation of slurry and bacteria (yeast and EM4) on rice husk composting results. The parameters observed were changes in temperature, water content, C/N ratio, and pH. At the end of the composting results showed that the addition of slurry, yeast and EM4 can lower the temperature and C / N ratio, and with the addition of yeast and 2 liters of slurry can speed up the process of decomposition of compost.

EKSTRAKSI KATEKIN DARI DAUN GAMBIR (Uncaria gambir roxb) DENGAN METODE MASERASI Desta Donna Putri Damanik, Nurhayati Surbakti, Rosdanelli Hasibuan
Jurnal Teknik Kimia USU Vol 3, No 2 (2014)
Publisher : Universitas Sumatera Utara

Catechins are a major components in the plant gambier. Beside catechins, there are several other components such as acid catechu tannat, quersetin, red catechu, gambier flouresin, fats and waxes. More than 80% of gambier production in Indonesia comes from the province of West Sumatra and North Sumatra, mainly in Limapuluh and Pakpak Bharat. Extraction of catechins from gambir leaf was performed by means of maceration that is soaking with a solvent polar. Maceration is carried out by temperature variations, 30°C, 40°C, 60°C and 80°C; maceration of time that is 1 hour, 6 hours, 12 hours, and 24 hours; and the type of solvent is aquadest, 96% ethanol, 95% ethyl acetate, and a mixture of 96% ethanol and 95% ethyl acetate (1:1). The results were filtered to obtain the filtrate which is then concentrated by rotary vacuum evaporator to test the levels of catechins, moisture content, and ash content. Based on this research the highest levels of catechins obtained the maceration temperature operating conditions of 60 ° C with a time of 6 hours maceration and used 95 % ethyl acetate as solvents in the amount of 87.14 % to 0.925 % moisture content and ash content of 0.04 % .

PEMBUATAN SIRUP GLUKOSA DARI KULIT PISANG KEPOK (Musa acuminatabalbisianacolla) SECARA ENZIMATIS Zulqarnain Albaasith, Rahmad Nauli Lubis, Rondang Tambun
Jurnal Teknik Kimia USU Vol 3, No 2 (2014)
Publisher : Universitas Sumatera Utara

Glucose syrup is a trade name of hydrolysis of starch solution. The purpose of this research is to produce glucose syrup from banana peel and examine the variables that affect the hydrolysis process. The process of making glucose syrup in this study through a series of treatment until the resulting slurry is ready to be processed banana peel. Hydrolysis process is then performed using α-amylase and glucoamylase enzyme. This process is carried out in four phases: liquefaction, saccharification, purification and concentration. In the liquefaction process to vary the weight of raw materials: water (10% w / v, 20% w / v, 30% w / v and 40% w / v) and heating temperature (60oC, 70oC, 80oC and 90oC). In this research shows that the best glucose syrup is in the variation of glucose syrup raw materials: water 10% w / v at a temperature of 90oC which produces reducing sugar 9.86% and 98.56% DE value. Keywords : starch, enzyme, glucose syrup

EKSTRAKSI PIGMEN ANTOSIANIN DARI KULIT BUAH NAGA MERAH (Hylocereus polyrhizus) Lidya Simanjuntak, Chairina Sinaga, Fatimah
Jurnal Teknik Kimia USU Vol 3, No 2 (2014)
Publisher : Universitas Sumatera Utara

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32734/jutek.v3i2.7178

Extraction of anthocyanin pigments from the red pitaya’s peel (Hylocereus polyrhizus) has been done. Anthocyanin pigment from the red pitaya’s peel (Hylocereus polyrhizus) can be used as an alternative for sinthetys dye. Extraction of anthocyanin pigments in this experiment is using maceration method. There are three independent variables used in this experiment, they are the type of solvent (distilled water, 95% ethanol, ethyl acetate and 10% citric acid), solvent ratios (1:2, 1:3 and 1:4,) and the time of extraction process (1, 2 and 3 days). This experiment aims to determine the right type of solvent, better solvent ratio and better extraction time that used to get anthocyanin pigments from red pitaya’s peel. The measurements in this experiment are based on the pH value, the absorbance value and anthocyanin pigment yield. The experimental results shows that the levels of anthocyanin pigments of red pitaya’s peel dissolved in a solvent mixture of distilled water plus 10% citric acid produce the highest level of anthocyanin pigment yield is 62.68% at pH 2 and the extraction time are 3 days.

STUDY OF EICHORNIA CRASSIPES POWDER FROM PANTE RIEK FOR PB2+ ION ADSORPTION Mirna Rahmah Lubis
Jurnal Teknik Kimia USU Vol 3, No 3 (2014)
Publisher : Universitas Sumatera Utara

Adsorption capacity was calculated in Eichornia crassipes adsorbent. In several areas of Aceh province such as Meulaboh, Takengon, and Tamiang, people extirpate Eichornia crassipes because it is considered disturbing water flow. Therefore, this research tries to investigate the utilization of Eichornia crassipes so that it could be used as bioadsorbent in order to reduce heavy metal from waste water. The main obejctive of this research is to reduce lead content, and to determine the best condition of lead adsorption in solution by using Eichornia crassipes powder. The analysis is conducted by using Atomic Adsorption Spectrophotometer. Research result indicates that optimum adsorption occurs at solution with pH of 4.4, lead concentration of 40 mg/L, and contact time of 75 minutes. Lead adsorption by Eichornia crassipes biomass follows adsorption isotherm of Langmuir and pseudo-second order with capacity of adsorption (am) of 27,78 mg/g, and adsorption constant (K) is 12 L/mg.

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