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Antibacterial Test and Isolation of Xanthones from Pericarps Mangosteen (Garcinia mangostana L.) using Calcium Oxide (CaO) as a Vacuum Liquid Chromatography (VLC) Stationary Phase Ni Komang Tri Dharmayani; Inggit Garnasih; Emmy Yuanita; Maria Ulfa; Sudirman Sudirman; Made Ganesh Darmayanti; Maulida Septiyana
Acta Chimica Asiana Vol. 5 No. 1 (2022)
Publisher : The University of Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/aca.v5i1.117

Xanthones are one of the biggest classes of compounds in natural product chemistry. Xanthones have been isolated from pericarp mangosteen (Garcinia mangostana L.) and then purified with VLC using calcium oxide (CaO) as the stationary phase and eluted using n-hexane: EtOAc of increasing polarity. Extraction of the pericarp mangosteen using the maceration method with acetone as the solvent. The isolation of xanthones was carried out through various chromatography techniques, such as vacuum liquid chromatography (VLC), gravitational column chromatography (GCC), and thin layer chromatography (TLC). The molecular structure of the compound was identified based on spectroscopy data, including IR, 1D NMR (1H and 13C), and 2D NMR (HSQC and HMBC). Based on the analysis of spectrum data, the isolated compound is ɑ-mangostin. The acetone extract and ɑ-mangostin were also examined for antibacterial activity against Gram positive (+) Staphylococcus aureus (S. aureus) ATCC 25923 and Gram negative (-) Escherichia coli (E. coli) ATCC 25922. The largest inhibition zone was shown by ɑ-mangostin against S. aureus (12.16 mm) more than E. coli (12 mm).

QSAR treatment of meisoindigo derivatives as a potentbreast anticancer agent Evie Kama Lestari; Agus Dwi Ananto; Maulida Septiyana; Saprizal Hadisaputra
Acta Chimica Asiana Vol. 2 No. 2 (2019)
Publisher : Chemistry Education Program, the University of Mataram

A quantitative structure-activity relationship (QSAR) analysis of meisoindigo derivatives as a breast anticancer has been carried out. This study aimed to obtain the best QSAR model in order to design new meisoindigo based compounds with best anticancer activity. The semiempirical PM3 method was used for descriptor calculation. The best QSAR model was built using multilinear regression (MLR) with enter method. It was found that there were 19 new meisoindigo derivativeswith better predictive a potent anticancer agent. The best compound was (E)-2-(1-((3-ethylisoxazol-5-yl)methyl)-2-oxoindolin-3-ylidene)-N-(4-methoxyphenyl)acetamide with the value of IC505.31144 x10-15 (Î¼M).

Pelatihan Pembuatan Buah Kering dan Serbuk Stroberi di Desa Sembalun Bumbung Kabupaten Lombok Timur Maria Ulfa; Emmy Yuanita; Ni Komang Tri Dharmayani; Sudirman Sudirman; Baiq Nila Sari Ningsih; Maulida Septiyana
Jurnal Pengabdian Inovasi Masyarakat Indonesia Vol. 2 No. 2 (2023): Edisi Agustus
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/jpimi.v2i2.3341

Panen yang berlimpah dan masa simpan buah stroberi yang cukup singkat merupakan permasalahan petani buah stroberi di desa Sembalun Bumbung dan juga menjadi salah satu alasan dilaksanakannya kegiatan pelatihan ini. Tujuan utama dari kegiatan pengabdian kepada masyakat ini adalah masyarakat mampu mengolah buah stroberi menjadi produk olahan dengan metode pengeringan, dan memadukan keahlian ini ke dalam wisata agro yang sudah cukup dikenal. Kegiatan pengabdian dilakukan dengan metode ceramah terkait dengan produk olahan sehat, metode pengawetan buah, dan fungsi food dehydrator; demonstrasi pembuatan buah kering dan serbuk stroberi serta aplikasinya pada makanan dan minuman; diskusi terkait dengan materi pelatihan dan pengembangan hasil pelatihan; dan evaluasi terkait dengan pemahaman materi pelatihan dan kemampuan masyarakat dalam memberikan ide inovatif dan kreatif dalam diversifikasi produk. Hasil kegiatan menunjukkan masyarakat mempunyai kemampuan untuk meningkatkan nilai jual buah stroberi menjadi produk olahan dan menjadikannya sebagai salah satu daya tarik wisata agro.

Microwave Assisted Hydrolysis Ulva sp. Using HCl for the Production of Bioethanol Raw Materials Bekti Palupi; Nadia Ayumna Fa’iqoh; Alifia Rahma Putri Neysella; Boy Arief Fachri; Ditta Kharisma Yolanda Putri; Lukman Nulhakim; Maulida Septiyana
Journal of Biobased Chemicals Vol. 2 No. 2 (2022): Journal of Biobased Chemicals
Publisher : Program Studi Teknik Kimia Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/jobc.v2i2.272

The challenges faced by the Indonesian state are increasing greenhouse gases, climate change, and depleting fossil fuel reserves. This requires the exploration of alternative energy that is environmentally friendly and sustainable. Algae biomass, especially Ulva sp. is one of the resources that have the potential for bioethanol production as an alternative energy producer. The purpose of this study is to determine the potential of Ulva sp. as raw material for bioethanol and to determine the effect of particle size, solvent concentration, and power on the hydrolysis process. This study used Ulva sp. as raw material. hydrolyzed with HCl solvent using the microwave assisted hydrolysis method. Hydrolysis with HCl concentrations of 0.1 N, 1 N, 2 N, variations of microwave power 150 watts, 300 watts, 450 watts, and particle sizes of 60 mesh, 80 mesh, and 100 mesh. Measurement of reducing sugar levels was carried out using the dinitro salicylic acid (DNS) method. The results showed that the best conditions for hydrolysis were when the HCl concentration was 0.1 N, the microwave power was 450 watts, and the particle size was 80 mesh which resulted in a reducing sugar content of 20.751 mg/mL.

Sosialisasi Pengemasan Produk dengan Plastik Biodegradable Berbahan Selulosa dan Strategi Pemasarannya di Kelompok Wanita Tani Alummahat, Lendang Nangka, Lombok Timur, NTB Ningsih, Baiq Nila Sari; Ulfa, Maria; Yuanita, Emmy; Dharmayani, Ni Komang Tri; Septiyana, Maulida; Haviz, Nur Vinna; Hayani, Hafiyatul; Tamara, Cynthia Claudia; Septiari, Wayan Uni
Jurnal Pengabdian Inovasi Masyarakat Indonesia Vol. 3 No. 2 (2024): Edisi Agustus
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/jpimi.v3i2.6002

Desa Lendang Nangka di Lombok Timur, NTB, yang termasuk dalam World Geopark UNESCO di lereng Gunung Rinjani, memiliki potensi besar dalam sektor pertanian. Namun, tantangan muncul dalam pengemasan produk pertanian yang belum ramah lingkungan. Kegiatan ini bertujuan meningkatkan nilai produk pertanian bagi kelompok Wanita Tani Alummahat melalui penggunaan kemasan ramah lingkungan berbahan selulosa dengan metode gelatinisasi dan pemasaran melalui e-commerce. Pelaksanaan kegiatan melibatkan transfer pengetahuan, teknologi, serta pembinaan dan pendampingan untuk memastikan peningkatan nilai ekonomi lokal secara berkelanjutan. Kegiatan meliputi penyuluhan, pelatihan praktis, dan pembentukan Kelompok Usaha Bersama (KUB) sebagai wadah pengembangan ide inovatif. Evaluasi menunjukkan peningkatan signifikan dalam pengetahuan dan keterampilan partisipan terkait pengemasan ramah lingkungan, serta antusiasme yang tinggi. Program ini berkontribusi pada pengembangan strategi pemasaran dan pengemasan yang berkelanjutan di tingkat desa, dengan harapan dapat memberikan dampak positif pada ekonomi masyarakat lokal.

Enhanced Methods for Synthesizing Hydroxyxanthone Using Eaton and ZnCl2 Catalyst with Microwave Irradiation Yuanita, Emmy; Eryani, Farica; Septiyana, Maulida; Lestarini, Ima Arum; Dharmayani, Ni Komang Tri; Sugara, Taufan Hari
Science and Technology Indonesia Vol. 10 No. 3 (2025): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26554/sti.2025.10.3.753-758

The methods for synthesizing hydroxyxanthone compounds are continually advancing. Among these, microwave-assisted organic synthesis (MAOS) has emerged as a particularly advantageous technique due to its reduced reaction times, improved yields, and enhanced selectivity. This study reports the efficient synthesis of 3,7 dihydroxyxanthone through the reaction of 2,5-dihydroxybenzoate and resorcinol, using Eaton’s reagent and zinc chloride (ZnCl2) as catalyst under MAOS conditions. The structures of the resulting compounds were analyzed using Fourier-transform infrared spectroscopy (FTIR) and proton nuclear magnetic resonance (1H-NMR). The efficiency of the catalytic systems was evaluated based on the product yields. The Eaton reagent catalysis resulted in a 9.38% yield of a red solid, while the ZnCl2-catalyzed reaction produced a significantly higher yield of 23.07%, with the product appearing as an orange solid. These results demonstrate that Zn

Hydrophilic Surfaces Turning of Graphene Nano Platelets by 1,3,6-Trihydroxyxanthone: π–π Stacking Interaction Affair in 2-D Yuanita, Emmy; Sirojuttolibin, Sirojuttolibin; Dharmayani, Ni Komang Tri; Ulfa, Maria; Septiyana, Maulida; Sudirman, Sudirman
Indonesian Journal of Chemistry Vol 25, No 3 (2025)
Publisher : Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/ijc.89894

Graphene nanoplatelet (GNP) has a good potential to be developed as a drug carrier material. In this study, the interaction of GNP with one type of drug, namely 1,3,6-trihydroxyxanthone (THX), has been studied. The results of XRD analysis and FTIR uptake show an excellent interaction between THX and GNP through the π–π stacking channel. This interaction makes the GNP surface more polar and soluble in the aqueous media. THX-graphene shows physical and chemical stabilities, where THX can be released under specific and controlled conditions. The results of this study show the potential of utilizing graphene as a drug carrier material for more specific disease targets with a longer drug release time.

MENGOPTIMALKAN PEMANFAATAN SUMBER DAYA KENTANG: KETERLIBATAN MASYARAKAT DAN PENINGKATAN KETERAMPILAN DALAM MENGGALI POTENSI TINGGI TEPUNG KENTANG DI DESA WISATA SEMBALUN BUMBUNG Dharmayani, Ni Komang Tri; Yuanita, Emmy; Ulfa, Maria; Ningsih, Baiq Nila Sari; Sudirman, Sudirman; Septiyana, Maulida; Wardhana, I Gede Adhitya Wisnu
Jurnal Pengabdian Inovasi Masyarakat Indonesia Vol. 3 No. 1 (2024): Edisi Februari
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/jpimi.v3i1.3344

Potatoes are one of the staple crops widely cultivated worldwide, with significant production, especially in Europe and North America. However, the economic potential of potatoes has not been fully harnessed, particularly in villages like Sembalun Bumbung, West Nusa Tenggara Province, Indonesia. This article outlines a community engagement approach aimed at enhancing the understanding and skills of the community in utilizing potato flour as a valuable local resource. The implementation methodology involves three main approaches: knowledge transfer, technology transfer, and mentoring. The activities encompass education, hands-on training, as well as testing and evaluating processed potato flour products, particularly noodles. The results of the program demonstrate high enthusiasm among participants, who have successfully produced high-quality potato flour and noodles. This program provides new opportunities for the community to utilize potatoes as an additional source of income and has the potential to significantly boost the village's economy.

Sosialisasi Pengemasan Produk dengan Plastik Biodegradable Berbahan Selulosa dan Strategi Pemasarannya di Kelompok Wanita Tani Alummahat, Lendang Nangka, Lombok Timur, NTB Ningsih, Baiq Nila Sari; Ulfa, Maria; Yuanita, Emmy; Dharmayani, Ni Komang Tri; Septiyana, Maulida; Haviz, Nur Vinna; Hayani, Hafiyatul; Tamara, Cynthia Claudia; Septiari, Wayan Uni
Jurnal Pengabdian Inovasi Masyarakat Indonesia Vol. 3 No. 2 (2024): Edisi Agustus
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/jpimi.v3i2.6002

Desa Lendang Nangka di Lombok Timur, NTB, yang termasuk dalam World Geopark UNESCO di lereng Gunung Rinjani, memiliki potensi besar dalam sektor pertanian. Namun, tantangan muncul dalam pengemasan produk pertanian yang belum ramah lingkungan. Kegiatan ini bertujuan meningkatkan nilai produk pertanian bagi kelompok Wanita Tani Alummahat melalui penggunaan kemasan ramah lingkungan berbahan selulosa dengan metode gelatinisasi dan pemasaran melalui e-commerce. Pelaksanaan kegiatan melibatkan transfer pengetahuan, teknologi, serta pembinaan dan pendampingan untuk memastikan peningkatan nilai ekonomi lokal secara berkelanjutan. Kegiatan meliputi penyuluhan, pelatihan praktis, dan pembentukan Kelompok Usaha Bersama (KUB) sebagai wadah pengembangan ide inovatif. Evaluasi menunjukkan peningkatan signifikan dalam pengetahuan dan keterampilan partisipan terkait pengemasan ramah lingkungan, serta antusiasme yang tinggi. Program ini berkontribusi pada pengembangan strategi pemasaran dan pengemasan yang berkelanjutan di tingkat desa, dengan harapan dapat memberikan dampak positif pada ekonomi masyarakat lokal.

Pelatihan dan Penerapan Teknologi Filtrasi Ramah Lingkungan untuk Pengolahan Limbah Pewarna Songket di UMKM Ungga Creative, Lombok Tengah Septiyana, Maulida; Putri, Baiq Yusmiar Aulia; Tsani, M. Khairul; Ningsih, Apriliya; Ramdhani, Restu Agung; Nursofia, Baiq Ike; Ningsih, Baiq Nila Sari; Dharmayani, Ni Komang Tri; Ulfa, Maria; Yuanita, Emmy; Budiana, Irwan
Jurnal Pengabdian Inovasi Masyarakat Indonesia Vol. 4 No. 2b (2025): Edisi khusus Dies Natalis Universitas Mataram
Publisher : Program Studi Pendidikan Kimia FKIP Universitas Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/4mhjgv27

Usaha Mikro, Kecil, dan Menengah (UMKM) Ungga Creative yang berlokasi di Desa Ungga, Lombok Tengah, merupakan UMKM yang berfokus pada produksi kain songket, mulai dari proses pewarnaan benang hingga tahap penenunan. UMKM ini menghadapi permasalahan berupa limbah cair hasil pewarnaan yang berpotensi mencemari lingkungan sekaligus meningkatkan biaya produksi. Oleh karena itu, kegiatan pengabdian ini dilaksanakan untuk memberikan solusi melalui penerapan teknologi pengolahan limbah tekstil berbasis pengendapan tawas dan filtrasi sederhana dengan memanfaatkan media berupa pasir, kain perca, zeolit, dan serabut kelapa. Metode kegiatan Pengabdian kepada Masyarakat ini meliputi penyuluhan mengenai dampak limbah tekstil, pelatihan praktis, serta pendampingan implementasi teknologi. Hasil kegiatan menunjukkan bahwa masyarakat menjadi lebih memahami bahaya limbah pewarna tekstil apabila terpapar ke lingkungan. Selain itu, teknologi filtrasi terbukti dapat diaplikasikan secara langsung pada skala UMKM dan mampu menurunkan intensitas warna serta tingkat kekeruhan limbah, sehingga air hasil olahan dapat digunakan kembali dalam proses pewarnaan. Masyarakat mitra juga mengalami peningkatan pengetahuan dan keterampilan dalam pengelolaan limbah tekstil. Selain memberikan manfaat ekonomi berupa efisiensi penggunaan air, kegiatan ini turut mendukung keberlanjutan usaha dan berkontribusi pada pencapaianSDG 6 (air bersih dan sanitasi layak), SDG 12 (konsumsi dan produksi yang bertanggung jawab), serta SDG 13(penanganan perubahan iklim).

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