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All Journal Reaktor Jurnal Teknik ITS IPTEK Journal of Proceedings Series IPTEK The Journal for Technology and Science Indonesian Journal of Chemistry ASEAN Journal of Chemical Engineering Jurnal Teknik Kimia Indonesia Sewagati Jurnal Teknik Kimia dan Lingkungan Bulletin of Chemical Reaction Engineering & Catalysis

Winardi, Sugeng

Departemen Teknik Kimia Institut Teknologi Sepuluh Nopember

Author-ID : 1454235

Arts Humanities Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Control & Systems Engineering Education Energy Engineering Languange, Linguistic, Communication & Media Materials Science & Nanotechnology Public Health Social Sciences Other

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Computational Fluid Dynamics Simulation of Clearance Effect in High Solid Loading Polydisperse Solid-Liquid Mixing Iman Mukhaimin; Tantular Nurtono; Sugeng Winardi
IPTEK Journal of Proceedings Series No 2 (2017): The 2nd Internasional Seminar on Science and Technology (ISST) 2016
Publisher : Institut Teknologi Sepuluh Nopember

A high solid loading concentration of solid-liquid mixing was investigated to observe the effect of ratio C, Clearance, and T, diameter tank, with C/T 0.33; C/T 0.25 and C/T 0.17 on local volume of hydrodynamic and spatial distribution of polydisperse solid suspension using CFD, Computational Fluid Dynamics. The 45o pitch blade turbine, diameter 0.5T, with down pumping flow simulation was used to remove solid particle from bottom of the tank. The tank is also equipped with four baffle with the size of 0.1T.. A solid-liquid mixing consists of five fractions of glass beads with equal proportion (X1=X2=X3=X4=X5=0.2X) have 40% wt total solid concentration with liquid fraction is aqueous solution of NaCl. The effect of ratio C/T at impeller speed 612 rpm create a flow pattern in the tank different. Effect ratio C / T also indicated the distribution on solid had a good uniformity index when N≥ Njs, just suspended speed. The highest uniformity was obtained on C/T 0.17. it also made difference power consumption on each geometry with C/T 0.17, 0.25, and 0.33 respectively are 251.18, 238.13, and 270.65watt.

Effect of Mixing Time to Homogeneity of Propellant Slurry Luthfia H. Abdillah; Sugeng Winardi; Sumarno Sumarno; Tantular Nurtono
IPTEK Journal of Proceedings Series No 1 (2018): 3rd International Seminar on Science and Technology (ISST) 2017
Publisher : Institut Teknologi Sepuluh Nopember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.12962/j23546026.y2018i1.3515

Propellant is a rocket fuel that can be solid or liquid. This research focused on composite solid propellant that was made from solid and liquid materials become a slurry. Homogeneity of the propellant slurry is important to investigate because it can affect specification and performance of the propellant. This research objective was to study effect of mixing time to homogeneity of propellant slurry that was processed by horizontal sigma blade mixer. Density data were used to assess the homogeneity and stated as degree of homogeneity. The result showed that the mixing time affect the density values and it was obtained the most homogeneous slurry was at total mixing time 135 minute

Study of Hydrodynamics and Overall Gas Hold Up Validation in Bubble Column by Computational Fluid Dynamics Yukh Ihsana; Sugeng Winardi; Tantular Nurtono
IPTEK The Journal for Technology and Science Vol 31, No 1 (2020)
Publisher : IPTEK, LPPM, Institut Teknologi Sepuluh Nopember

The study of overall gas hold up has been carried out experimentally with the bed expansion. The superficial gas velocities used for the experiments are 6.369 m/s and 10.616 m/s. The experiment is carried out in a bubble column with inside diameters of 7 cm and a height of 100 cm. Gas from the gas cylinder is supplied through a distributor consisting of a perforated plate and glass beads. The perforated plate has a hole diameter of 1 mm and 0.5 mm. Computational Fluid Dynamic (CFD) using a Eulerian coupled with Population Balance model is developed to predict overall gas hold up and bubble size distribution. The effect of superficial gas velocity, perforated plate diameter, gas properties, and initial liquid level on gas hold up were studied. The use of population balance can significantly improve the overall gas hold-up results compared to constant bubble diameter. It is found that several operating conditions affect the whole gas hold up, namely initial liquid level, superficial gas velocity, and differences in gas properties. While the influence of the difference in perforated plate diameter to overall gas holds up, results are small compared to other operating conditions.

Hydrothermal Synthesis: Low−Temperature Subcritical Water for Ceria−Zirconia Mixed Oxides Preparation Siti Machmudah; Widiyastuti Widiyastuti; Wahyudiono Wahyudiono; Sugeng Winardi; Hideki Kanda; Motonobu Goto
Indonesian Journal of Chemistry Vol 21, No 1 (2021)
Publisher : Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/ijc.47357

A low-temperature hydrothermal synthesis technique was employed as a medium to produce ceria−zirconia mixed oxides particles at temperatures of 200–300 °C and pressure of 10 MPa in a batch process. At these conditions, the average crystallite sizes of ceria−zirconia mixed oxides increased slightly with increasing reaction temperature when the feed solution containing ceria and zirconia with a ratio of 1:1 was fed. SEM images illustrated that the morphologies of the ceria−zirconia mixed oxides particles were spherical and spherical−like with a diameter of around 100 nm. The EDX spectrum indicated that the signal corresponding to the ceria and the zirconia elements at 5 and 2 keV, respectively, were strongly detected in the products. The XRD pattern revealed that the mixed metal oxides particle products that comprised of cerium and zirconium oxides particles with cubic and monoclinic structures, respectively, were affected by their molar content in the feed solution.

Microparticles Formation of Ganoderma lucidum Extract by Electrospraying Method Siti Machmudah; Dwi Setyorini; Sugeng Winardi; Wahyudiono Wahyudiono; Hideki Kanda
ASEAN Journal of Chemical Engineering Vol 19, No 2 (2019)
Publisher : Department of Chemical Engineering, Universitas Gadjah Mada

In this work, Ganoderma lucidum (G. lucidum) extract was produced in microparticles form by electrospraying. G. lucidum was extracted hydrothermally at temperature of 160oC and pressure of 7 MPa. The extract solution was subsequently mixed with 6% of Polyvinyl pyrrolidone (PVP) and formed into microparticles by electrospraying process. The electrospraying was carried out at applied voltage of 12, 14, and 16 kV, and the distance between syringe tip and electrospun collector of 8, 10, and 12 cm. The microparticles formed was analyzed using scanning electron microscope (SEM), fourier-transform infrared (FTIR) spectroscopy, and UV-Vis spectrofotometer. The antioxidant efficiency of particles was also analyzed by 1,1-diphenyl-2-picrylhydrazyl (DPPH) assay. Based on the SEM analysis, the G. lucidum extract (GLE) – PVP spherical particles were formed by electrospraying. The finer fibres were clearly formed with the increasing applied voltage. The results showed that applied voltage and distance of tip to electrospun collector significantly influence the antioxidant efficiency and the diameter size of particles. The antioxidant efficiency increased with the rising applied voltage and gap of tip to electrospun collector, while the particle diameter decreased with the rising applied voltage and gap of tip to electrospun collector due to fast mass transfer and evaporation. The largest antioxidant efficiency of particles was 0.377/min obtained at 16 kV and 12 cm. It indicated that electrospraying is an effective process to produce pharmaceutical compounds in powder form.

Yield and Extraction Rate Analysis of Phytochemical Compounds from Eucheuma cottonii, Ganoderma lucidum, and Gracilaria sp. using Subcritical Water Extraction Fesa Putra Kristanto; Siti Machmudah; Sugeng Winardi; Wahyudiono Wahyudiono; Motonobu Goto
ASEAN Journal of Chemical Engineering Vol 21, No 1 (2021)
Publisher : Department of Chemical Engineering, Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/ajche.60513

Eucheuma cottonii (E. cottonii), Ganoderma lucidum (G. lucidum), and Gracilaria sp. are plants that contain high phytochemicals, such as flavonoids, polyphenols, saponins, and tannins. In this work, the phytochemicals were obtained using the subcritical water extraction (SWE) process. The SWE method uses water as a solvent in subcritical conditions. Therefore, the SWE process is an environmentally friendly process for extraction. In order to run the SWE process optimally, measurement of the extraction rate of SWE is needed. Calculation of the extraction rate of SWE process used first and second-order models according to Lagergren equation. SWE process was started by setting temperatures from 140 to 180oC at a pressure of 7 MPa and solvent flow rate of 1 ml/min. Before starting the extraction, the raw material was loaded into the extractor. The raw materials used were E. cottonii, G. lucidum, and Gracilaria sp. The extraction process was carried out for 3 hours, and the product was collected every 30 minutes. The collected product was put into a sample bottle and dried using a freeze dryer. After that, the products obtained were balanced by an analytical scale. Based on the result, the optimum temperature for the SWE process was 180oC for E. cottonii and G. lucidum and 160oC for Gracilaria sp. The yields of the SWE process under the optimum temperature were 85.37%, 58.42%, and 75.73% for E. cottonii, G. lucidum, and Gracilaria sp, respectively. The extract contained phytochemical compounds detected by high-performance liquid chromatography analysis. The kinetics model of extraction rate for all variables exhibited a second-order kinetics model that indicated that the extraction process was influenced by more than one factor.

Identifikasi Kandungan Boraks dan Formalin pada Makanan dengan Menggunakan Scientific Vs Simple Methods Siti Nurkhamidah; Ali Altway; Sugeng Winardi; Achmad Roesyadi; Yeni Rahmawati; Siti Machmudah; Widiyastuti; Tantular Nurtono; Siti Zullaikah; Lailatul Qadariyah
Sewagati Vol 1 No 1 (2017)
Publisher : Pusat Publikasi ITS

Seiring dengan meningkatnya kebutuhan akan bahan makanan yang tidak mudah rusak, boraks banyak sekali digunakan dalam industri makanan, seperti: dalam pembuatan mie basah, lontong, ketupat, tahu, bakso, sosis, dan lain-lain. Selain boraks, formalin juga banyak digunakan sebagai bahan pengawet makanan. Padahal zat-zat kimia tersebut merupakan bahan beracun dan bahan berbahaya bagi manusia sehingga sangat dilarang digunakan sebagai bahan baku makanan. Oleh karena itu, diperlukan metode identifikasi yang sederhana (simple method) untuk kedua bahan berbahaya tersebut dalam makanan. Sehingga, dapat dilakukan oleh konsumen terutama para ibu rumah tangga dengan mudah. Untuk menguji validitas dari simple method tersebut, maka hasil ujinya perlu dibandingkan dengan scientific method. Hasil uji kandungan boraks pada makanan dengan menggunakan simple method telah dilakukan di Laboratorium dan hasil uji menunjukaan bahwa dari 28 sampel yang di uji, ada dua sample yang positif mengandung boraks. Hasil dari metode nyala api yang merupakan scientific method untuk uji kandungan boraks menunjukkan hasil yang sama dengan hasil uji menggunakan simple method. Sedangkan pada uji formalin, baik menggunakan scientific method menunjukkan hasil bahwa terdapat tujuh sampel yang positif mengandung formalin dari 28 sampel yang diuji dan sebagian besar sampel tersebut merupakan ikan asin. Hasil dari uji tersebut telah disosialisasikan kepada masyarakat sekitar Institut Teknologi Sepuluh Nopember (ITS), yaitu ibu-ibu PKK di Perumahan Sukolilo Dian Regency RT 8 dan 9, RW 2 Kelurahan Keputih Kecamatan Sukolilo Surabaya pada 26 Juni 2016 dan dilakukan sosialisasi kedua pada tanggal 30 Juli 2016 untuk melihat tingkat keberhasilan dan keberlanjutan dari sosialisasi yang pertama.

Studi Fluidisasi dan Pembakaran Batubara Polydisperse di Dalam Fluidized Bed Berbasis Simulasi CFD (Computational Fluid Dynamic) Mochammad Agung Indra Iswara; Tantular Nurtono; Sugeng Winardi
Jurnal Teknik Kimia dan Lingkungan Vol. 2 No. 1 (2018): April 2018
Publisher : Politeknik Negeri Malang

Penelitian ini bertujuan untuk mengetahui fenomena pembakaran batubara dimana dimensi alat, distribusi ukuran partikel, dan jenis kualitas batubara menggunakan validasi dari penelitian Wang. Penelitian ini mengarahkan pada simulasi berbasis CFD. Kondisi operasi pada saat simulasi pembakaran dilakukan pada kecepatan bubbling. Metode yang digunakan sebelum melakukan simulasi pembakaran merupakan kelanjutan dari simulasi fluidisasi dimana masih menggunakan geometri 2-D fluidized bed lalu dilakukan meshing, selanjutnya memasukkan persamaan energi. Geometri fluidized bed yang digunakan berbentuk tabung dengan panjang silinder fluidized bed 1370 mm, diameter silinder 152 mm. Bahan yang digunakan pada penelitian ini berupa pulverized coal dengan jenis batubara Bituminous dimana ukuran partikel dianggap polydisperse dengan ukuran partikel 1 mm dan 1,86mm yang masing-masing sebesar 50% fraksi massa dengan kecepatan 0,2 Kg/s dan suhu 1200 K, dan udara luar yang diinjeksikan dengan kecepatan 0,8 m/s dan suhu 300 K. Analisa pengambilan data adalah berupa kontur fase padatan, kontur temperatur pada fase-1 dan fase padatan, fraksi massa produk pembakaran, massa padatan awal dan akhir simulasi dengan time step sebesar 0,0001 detik dan number of time step sebesar 300000. Selanjutnya data tersebut diplot menjadi grafik temperatur terhadap time step dan disajikan dalam setiap 1 menit simulasi selama 5 menit simulasi. This research aims to determine coal combustion’s phenomenon, where the device’s dimension, particle size distribution, and the quality of rank coal which validated Wang’s reseach. This reseach leads on CFD simulation. The operation condition has did in bubbling velocity. This method is a continuation from fluidization simulation which is use 2-D Geometry and then used the meshing method, and enter the energy equation. The geometry of fluidized bed used was tubular cylinder with 1370 mm length and 152 mm. Materials used in this study was pulverized coal with Bituminous coal type which the particle size was considered as monodispers with particle size was 1.43 mm and polydispersed with particle size was 1 mm with 50% mass fraction and 1.86 mm with 50% mass fraction with flow rate 0,2 Kg/s and the temperature is 1200 K, and the outside air are injected in 0,8 m/s and 300 K. The analysis of data retrieval is solid phase contour, temperature contours in phase-1 and solid phase, mass fraction of combustion product, initial solid mass and final solid mass simulation with time step 0,0001 s and the numberof time step 300000. Then the data is plotted into a graph temperature vs time step and presented in 1 minute simulation for 5 minute simulation.

Kinetic Model of LiFePO4 Formation Using Non-Isothermal Thermogravimetric Analysis Abdul Halim Abdul Halim; Widiyastuti Widiyastuti; Heru Setyawan; Sugeng Winardi
Bulletin of Chemical Reaction Engineering & Catalysis 2014: BCREC Volume 9 Issue 1 Year 2014 (April 2014)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.9.1.5508.60-65

The formation reaction of LiFePO4 from decomposition of precursors LiOH, FeSO4.7H2O and (NH4)2HPO4 with mol ratio of Li:Fe:P=1:1:1 was investigated. The experiment was carried out by thermogravimetric differential thermal analysis (TG-DTA) method using nitrogen as atmosfer at a constant heating rate to obtain kinetic constant parameters. Several heating rates were selected, there are 5, 7, 10, 15, 17.5, 22.5 and 25 °C/min. Activation energy, pre-exponential factor and reaction order were taken using Kissinger method and obtained respectively 56.086 kJ/mol, 6.95×108 min-1, and 1.058. Based on fitting result between reaction model and experiment were obtained that reaction obeyed the three dimension diffusion model. © 2014 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0)

Desain Pabrik Bioetanol Melalui Fraksinasi Lignoselulosa dari Tandan Kosong Kelapa Sawit (TKKS) Nurcahyani, Centri; Safitria, Nadiya Rizki; Machmudah, Siti; Winardi, Sugeng
Jurnal Teknik ITS Vol 13, No 3 (2024)
Publisher : Direktorat Riset dan Pengabdian Masyarakat (DRPM), ITS

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.12962/j23373539.v13i3.126185

Bioetanol adalah bahan bakar alternatif yang diolah dari tumbuhan yang memiliki keunggulan karena mampu menurunkan emisi CO2 hingga 18%, dibandingkan dengan emisi bahan bakar fosil seperti minyak tanah. Tandan Kosong Kelapa Sawit (TKKS) yang merupakan salah satu limbah padat yang dihasilkan dari pabrik CPO yang jumlahnya mencapai 95,56% dari jumlah CPO yang diproduksi. Proses produksi bioetanol terdiri dari empat proses yaitu pre-treatment, fraksinasi, fermentasi dan proses pendukung (pemurnian). Proses ini dapat menghilangkan air hingga kadar etanol menjadi 99,5% dan dihasilkan etanol absolute (murni). Pabrik bioethanol ini akan menghasilkan produk sebesar 16.614.108,61 kg/tahun dengan kemurnian etanol 99,5%. Dari perhitungan analisi ekonomi didapatkan nilai NPV sebesar Rp 249.539.009.136, untuk IRR sebesar 25,02%, POT selama 2,42 tahun, dan BEP sebesar 25,98%. Dari data tersebut menunjukkan bahwa pabrik Lignin dari Tandan Kosong Kelapa Sawit ini layak untuk didirikan.

Co-Authors Abdul Halim Abdul Halim Abdul Halim Achmad Roesyadi Adhi Setiawan Agung Nugroho Agung Nugroho Ali Altway Brario Anindito Dwi Setyorini Dwi Setyorini Fadlilatul Taufany Heru Setyawan Hideki Kanda Hideki Kanda Hideki Kanda Iva Maula Kristianto, Fesa Putra Kusdianto Kusdianto Lailatul Qadariyah Ling Ling Luthfia H. Abdillah M Rachimoellah Machmudah, Siti Mochammad Agung Indra Iswara Mochammad Agung Indra Iswara Motonobu Goto Motonobu Goto Motonobu Goto Mukhaimin, Iman Nadiem Anwar Novia Larasati Nurcahyani, Centri Nurkhamidah, Siti Safitria, Nadiya Rizki Siti Chasanah Siti Machmudah Siti Machmudah Siti Machmudah Siti Machmudah Siti Machmudah Siti Machmudah Siti Zullaikah Sjarief Widjaja Sumarno Sumarno Suryadi, Joko Tantular Nurtono Wahyudiono Wahyudiono Wahyudiono Wahyudiono Wahyudiono Wahyudiono Wahyudiono Wahyudiono Widiyastuti Widiyastuti Widiyastuti Widiyastuti Widiyastuti Widiyastuti Widiyastuti Yeni Rahmawati, Yeni Yukh Ihsana

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