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Ekstraksi EKSTRAKSI DAN KARAKTERISASI PEKTIN DARI LIMBAH KULIT JERUK LIMAU (Citrus amblycarpa) Fiqi Estuning Nava Maulida; Alimuddin Alimuddin; Erwin Erwin
JURNAL KIMIA MULAWARMAN Vol 20 No 2 (2023)
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/jkm.v20i2.527

Abstract

Research on the extraction and characterization of pectin from lemon lime peel waste (Citrus amblycarpa) has been done. The purpose of this research is to process lime waste into raw material of pecti
EFFECT OF TIME VARIATION ON XYLENE USING ACTIVE CARBON FROM WASTE OF BANANA STEM (Musa paradisiaca L) Ashari, Ayu Wanti; -, Alimuddin; Sitorus, Saibun
JURNAL ATOMIK Vol 5 No 2 (2020)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

Test of activated carbon adsorption ability of banana stem waste (Musa paradisiaca L) on xylene has been carried out. In the characterization of activated carbon Scanning Electron Microscopy (SEM) was used to show the morphological differences in activated carbon after activation and before activation while xylene adsorption using a UV spectrophotometer with variations in the time of adsorption. The optimum xylene adsorption time was obtained on the weight of 0.4 gram adsorbent, the concentration of xylene 40 ppm was 45 minutes, the adsorption capacity was 1.772 mg/g.
THE MANUFACTURING OF SILICA GEL FROM BAMBOO LEAF ASH (Dendrocalamus asper (Schult. f) Backer ex Heyne) AND THE APPLICATION FOR ADSORPTION Cd (II) ION -, Yasrin; -, Alimuddin; Panggabean, Aman Sentosa
JURNAL ATOMIK Vol 5 No 2 (2020)
Publisher : Jurusan Kimia FMIPA UNMUL

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The research about silica gel manufacturing from bamboo leaf ash (Dendrocalamus asper (Schult.) Backer ex Heyne) and the application for Cd (II) ion adsorption has been done. The adsorption of Cd (II) ion done by some varieties, such as pH, concentration, and contact time. The result of the research showed the optimum pH was 8, the optimum concentration was 4 ppm and the contact time was 60 minutes. The adsorption capacity was 0.388 mg/g and the percentage of recovery was 93.44%.
MODIFICATION OF ADSORBEN SILICA FROM RICE HUSK ASH WITH CHITOSAN TO ADSORPTION ION MANGANESE (TOTAL) Fauzi, Akhmad; -, Alimuddin; Widodo, Nanang Tri
JURNAL ATOMIK Vol 5 No 2 (2020)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

Adsorbent silica from rice husk ash supported by chitosan can be used to adsorb Mn (Total) metal. The adsorbent is regulated by adjusting the composition of 65% silica and 35% chitosan. The characteristics of the silica-chitosan adsorbent and the adsorbent interaction with Mn (Total) are believed to be based on Fourier Transform Infared (FTIR) data. The concentration of Mn (Total) ion after adsorption is determined by Atomic Absorption Spectrophotometer (AAS). The results showed optimum pH at pH 5 percentage adsorption 79.45% and optimum contact time at 60 minutes with adsorption percentage 96.78%, and obtained chitosan-silica adsorption capacity of Mn (Total) ions of 1.0349 mg/g.
Analisis Kadar Asam Sianida dalam Solanum melongena L dan Solanum quitoense L Sebelum dan Sesudah Perebusan Sabaniah Indjar Gama; Alimuddin Alimuddin; Eva Marliana
Journal of Tropical Pharmacy and Chemistry Vol. 1 No. 1 (2010): J. Trop. Pharm. Chem.
Publisher : Faculty of Pharmacy, Universitas Mulawarman, Samarinda, Indonesia, 75117, Gedung Administrasi Fakultas Farmasi Jl. Penajam, Kampus UNMUL Gunung Kelua, Samarinda, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25026/jtpc.v1i1.10

Abstract

ABSTRACT Analysis cyanide acid in Solanum melongena and Solanum quitoense L before and after boiling. Cyanide acid is esthabushed by argonometricm method (Volhard) with three times repetition, for each kinds of eggplants Solanum melongena L dan Solanum quitoense L. The research showed have endireated that before boiling the content of cyanide acid Solanum melongena L (Craigi eggplant 71,712 mg/kg, kopek eggplant 46,310 mg/kg, gelatik eggplant 0 mg/kg) and Solanum quitoense L (asam eggplant 30,434 mg/kg) after boiling, the cyanide acid to slop Solanum melongena (Craigi eggplant 19,321 mg/kg, kopek eggplant 6.620 mg/kg, gelatik eggplant 0 mg/kg and Solanum quitoense L (asam eggplant 3.445 mg/kg). There is significant content have been reduced of cyanide acid in Solanum melongena L dan Solanum quitoense L Keywords: Solanum melongena dan Solanum quitoense L, Cyanide acid ABSTRAK Telah dilakukan analisis asam sianida dalam Solanum melongena dan Solanum quitoense L sebelum dan sesudah perebusan menggunakan metode Volhard dengan tiga kali pengulangan. Data hasil penelitian menunjukkan kandungan asam sianida sebelum perebusan Solanum melongena (terong Craigi 71,712 mg/kg, terong kopek 46,310 mg/kg, terong gelatik 0 mg/kg) dan Solanum quitoense L (terong asam 30,434 mg/kg) sedangkan setelah dilakukan perebusan (terong Craigi 19,321 mg/kg, terong kopek 6.620 mg/kg, terong gelatik 0 mg/kg) and Solanum quitoense L (terong asam 3.445 mg/kg). Terdapat perbedaan kandungan penting yang dapat mengurangi kadar asam sianida dalam Solanum melongena L dan Solanum quitoense L. Kata kunci: Solanum melongena dan Solanum quitoense L, Asam Sianida
DETERMINATION OF PARAMETER QUALITY OF GROUND WELL WATER USING ADSORBENT FILTER FROM RICE HUSK ASH Said, Yahya; -, Alimuddin; Gunawan, Rahmat
JURNAL ATOMIK Vol 6 No 1 (2021)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

Determining the parameters of the quality of well water in Mugirejo, Sungai Pinang, Samarinda, using an adsorption filter from rice husk ash, has been carried out. Determination of the optimum flow rate and the level of each water quality parameter BOD, TSS and levels of metals (Pb, Fe, Mn). Based on the results of the filtration process in well water samples showed that the effect of the flow rate obtained the optimum flow rate of 1 hour per liter against decreasing levels of BOD, TSS and levels of metals (Pb, Fe and Mn) of 8.1, 17.28 mg/L O2, 1.4 mg/L, 68 mg/L, ND (No Detection), 0.0012 µg/mL and 0 µg/mL. For the flow rate of ½ hour per liter against decreases in BOD, TSS and levels of metals (Pb, Fe and Mn) respectively at 8.0, 30.52 mg/L O2, 2.01 mg/L, 46 mg/L, 0 µg/mL, 0.0109 µg/mL and 0.021 µg/mL.
ANALISIS KADAR ION TIMBAL (Pb) DAN ION KROMIUM (Cr) PADA RAMBUT PEKERJA PERBENGKELAN DI KOTA SAMARINDA -, Sugiarti; Gunawan, Rahmat; -, Alimuddin
JURNAL ATOMIK Vol 1 No 2 (2016)
Publisher : Jurusan Kimia FMIPA UNMUL

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Telah dilakukan penelitian ini yang bertujuan untuk mengetahui kadar ion timbal dan ion kromium pada rambut pekerja perbengkelan dengan variasi umur dan lama bekerja dengan kadar ion timbal dan ion kromium pada rambut pekerja perbengkelan. Rambut yang sudah dikumpulkan dicuci kemudian diabukan dan dihomogenkan kemudian dianalisis dengan Atomic Absorption Spectrophotometer (AAS). Panjang gelombang untuk analisis logam timbal 283,3 nm dan untuk logam kromium 357,9 nm. Hasil menunjukkan analisis kadar ion timbal sampel pada rambut pekerja bengkel terendah 3,892 (mg/kg) yang tertinggi 48,814 (mg/kg) dan untuk kadar ion kromium sampel rambut pada pekerja bengkel terendah 1,578 (mg/kg) yang tertinggi 36,884 (mg/kg). Berdasarkan uji statistik analisis korelasi yang berhubungan positif umur dan lama bekerja dengan kadar ion timbal dan ion kromium pada rambut pekerja perbengkelan. Dengan Koefisien determinan besarnya kadar ion timbal berdasarkan hubungan lama bekerja 98,2 % dan   untuk ion kromium 97,7 %,  dan koefisien determinan berdasarkan hubungan umur dengan kadar ion timbal 78,2 % dan ion kromium 83,2 %.
PEMBUATAN BIODIESEL DARI LEMAK IKAN PATIN(Pangasius sp) DENGAN RADIASI GELOMBANG MIKRO Tanjung, Albayssag Faisal; -, Alimuddin; Yusuf, Bohari
JURNAL ATOMIK Vol 1 No 2 (2016)
Publisher : Jurusan Kimia FMIPA UNMUL

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The research about made biodiesel from fat of patin fish (Pangasius sp) as raw material and known influence time exposure microwave radiation to concentration biodiesel that was produced have been done.Fat of patin fish heated to get oil extract. The oil extract was refluxed with methanol as reactant and H2SO4 as catalyst for 120 minute. Then transesterified with methanol as reactant and NaOH as catalyst with different time that was for 2, 4, 6, 8, and 10 minutes. The high product of biodiesel is 87,2 b/v that was exposured microwave radiation for 8 minutes. To knew kind of methyl ester in biodiesel used GC-MS and the high concentration of methyl ester in biodiesel is methyl oleat with concentration 24,74%.
KARAKTERISASI BIOIDIESEL LEMAK IKAN BAUNG (MYTUS NEMURUS) DENGAN KATALIS CaO DARI CANGKANG TELUR AYAM Pali, Mendriyani; -, Alimuddin; -, Daniel
JURNAL ATOMIK Vol 1 No 2 (2016)
Publisher : Jurusan Kimia FMIPA UNMUL

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The research abaout the use ash of eggchell as source of base catalyst in application for reaction of transseterification from fish baung fat. Conten of base compound in eggchell ash was analyzed by AAS and acidy alkalimetry. The result of the research showed that calcium concentration as carbonat calcium salt in the as of eggchell was 74,8% (w/w). weight variation on the eggchell as catalyst transeterification process is performed to find the optimum reqaction condition if the biodiesel production. Aqquisition of the highest biodiesel yield at catalyst weight of 2,5 % was 96.7663 %. The composition of fatty acid of fish baung fat from transesterification result it is determinate with FT-IR and GC-MS. GC-MS analysis showed that fatty acids are the dominant constituent in the biodiesel is methyl oleate in the amount of 39,39%.
PENURUNAN INTENSITAS WARNA REMAZOL RED RB 133 DALAM LIMBAH BATIK DENGAN ELEKTROKOAGULASI MENGGUNAKAN NaCl Fatimah, Nurul; -, Alimuddin; Gunawan, Rahmat
JURNAL ATOMIK Vol 3 No 1 (2018)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

A decrease in the intensity of dye Remazol Red RB 133 in batik waste with electrocoagulation method using electrodes aluminum and stainless steel has been done. Analysis was performed using a spectrophotometer Visibel. The results showed that the optimum effect of adding NaCl at a concentration 7 g/L with degradation was 84.95% percent, optimum contact time 60 minutes with degradation was 86.36%, stronger optimum voltage 12 Volts with degradation was 94.31% and pH optimum at pH 4 with degradation was 96.86%. Electrocoagulation in optimum condition dye Remazol Red RB 133 produces an average degradation was 96.41%, and electrocoagulation of batik waste obtained an average degradation was 91.38%.