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All Journal Reaktor BERKALA FISIKA Jurnal Penelitian Fisika dan Aplikasinya (JPFA) Jurnal Sains Materi Indonesia Chem Info YOUNGSTER PHYSICS JOURNAL Prosiding Seminar Nasional Sains Dan Teknologi Fakultas Teknik Bulletin of Chemical Reaction Engineering & Catalysis JITEK (Jurnal Ilmiah Teknosains) Indonesian Journal of Chemistry Journal of Physics and Its Applications Astonjadro Jurnal Pijar MIPA Bulletin of Chemical Reaction Engineering & Catalysis JURNAL REKAYASA KIMIA & LINGKUNGAN
Iis Nurhasanah
Department Of Physics, Faculty Of Science And Mathematics, Diponegoro University, Jl. Prof. Soedarto SH, Tembalang, Semarang 50275, Indonesia
Agriculture, Biological Sciences & Forestry Astronomy Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Civil Engineering, Building, Construction & Architecture Computer Science & IT Control & Systems Engineering Earth & Planetary Sciences Education Energy Engineering Materials Science & Nanotechnology Mathematics Mechanical Engineering Physics Veterinary

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Evaluation of Novel Integrated Dielectric Barrier Discharge Plasma as Ozone Generator Muhammad Nur; Ade Ika Susan; Zaenul Muhlisin; Fajar Arianto; Andi Wibowo Kinandana; Iis Nurhasanah; Sumariyah Sumariyah; Pratama Jujur Wibawa; Gunawan Gunawan; Anwar Usman
Bulletin of Chemical Reaction Engineering & Catalysis 2017: BCREC Volume 12 Issue 1 Year 2017 (April 2017)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.12.1.605.24-31

Abstract

This paper presents a characterization of an integrated ozone generator constructed by seven of reactors of Dielectric Barrier Discharge Plasma (DBDP). DBDP a has spiral-cylindrical configuration. Silence plasma produced ozone inside the DBDP reactor was generated by AC-HV with voltage up to 25 kV and maximum frequency of 23 kHz. As a source of ozone, dry air was pumped into the generator and controlled by valves system and a flowmeter. We found ozone concentration increased with the applied voltage, but in contrary, the concentration decreased with the flow rate of dry air. It was also found that a maximum concentration was 20 mg/L and ozone capacity of 48 g/h with an input power of 1.4 kW. Moreover, in this generator, IP efficiency of 8.13 g/kWh was obtained at input power 0.45 kW and air flow rate of 9 L/min. Therefore, be the higher ozone capacity can be produced with higher input power; however, it provided lower IP efficiency. The effect of dry air flow rate and applied voltage on ozone concentrations have been studied. At last, spiral wire copper was very corrosive done to the interaction with ozone, and it is necessary to do a research for finding the best metals as an active electrode inside of the quartz dielectric. 
French Fries-Like Bismuth Oxide: Physicochemical Properties, Electrical Conductivity and Photocatalytic Activity Yayuk Astuti; Fauzan Musthafa; Arnelli Arnelli; Iis Nurhasanah
Bulletin of Chemical Reaction Engineering & Catalysis 2022: BCREC Volume 17 Issue 1 Year 2022 (March 2022)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.17.1.12554.146-156

Abstract

Bismuth oxide synthesis using hydrothermal method has been conducted. This study aims to examine the effect of the hydrothermal reaction time on product characteristics and photocatalytic activity in degrading methyl orange dye. Bismuth oxide synthesis was initiated by dissolving bismuth nitrate pentahydrate (Bi(NO3)3.5H2O) and Na2SO4 in a distilled water and added NaOH gradually. The solution formed was transferred into a Teflon-lined autoclave and heated at 120 °C with time variations of 8–16 h. The formation of bismuth oxide was indicated by the vibrations of the Bi−O−Bi and Bi−O groups and the crystal structure consisting of a-Bi2O3, β-Bi2O3, and g-Bi2O3. In addition, the highest photocatalytic activity can be examined through several factors, such as: content of Bi−O−Bi and Bi−OH groups, crystal structure, band gap values, morphology, and surface area, acquired as a result of the effect of hydrothermal reaction time. Copyright © 2021 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). 
Structural and Optical Properties of Bismuth-doped Cerium Oxide Prepared at a Low Temperature Paramita, Safira Arta; Nurhasanah, Iis; Khumaeni, Ali
Jurnal Penelitian Fisika dan Aplikasinya (JPFA) Vol. 13 No. 1 (2023)
Publisher : Universitas Negeri Surabaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26740/jpfa.v13n1.p16-24

Abstract

Cerium oxide (CeO2) is a functional material with excellent physicochemical properties. Its properties can be modified by doping with different elements, including bismuth, which can be done through various synthesis methods. The precipitation method combined with ultrasonic radiation was used to synthesize bismuth-doped cerium oxide (CeO2:Bi) at a low temperature of 200oC. In this study, we investigate the alteration of structural and optical properties of as-prepared CeO2:Bi by subjecting it to additional calcination at a high temperature of 500oC. The structural and optical properties of CeO2:Bi were characterized using thermal gravimetric analysis, X-ray diffraction, Scanning Electron Microscope-Energy Dispersive X-Ray, Fourier Transform Infrared spectroscopy, and UV-Visible spectroscopy. The additional calcination produced a less significant weight-loss percentage than the as-prepared CeO2:Bi observed from the gravimetric curve. The Fourier transform infrared spectrum revealed the loss of a small number of hydroxyl molecules trapped on the CeO2:Bi surface when additional calcination was subjected. Based on the X-ray diffraction spectra, additional calcination results in the smallest crystallite size and compressive strain without the changed cubic crystal structure of CeO2:Bi. The successful doping of Bi in CeO2 was confirmed by the composition analysis from Energy Dispersive X-Ray measurement. Scanning electron microscope image showed spherical and agglomerated particles of calcined CeO2:Bi. The optical properties of both CeO2:Bi possessed similar trend absorption spectra and almost the same band gap energy. The results indicated that the calcination of as-prepared CeO2:Bi at a temperature of 500oC did not affect its structural and optical properties significantly. Thus, combining ultrasonic radiation with precipitation is an advantageous method to synthesize at a low temperature of stable CeO2:Bi crystalline.
Green Synthesis of Silver Nanoparticles Using Citrus sinensis Peels Assisted by Microwave Irradiation as a Contrast Agents for Computed Tomography Imaging Fatikasari, Tanty; Nurhasanah, Iis; Khumaeni, Ali
Indonesian Journal of Chemistry Vol 24, No 5 (2024)
Publisher : Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/ijc.95690

Abstract

Contrast agents are extensively used to enhance the quality of images in computed tomography (CT) scans for brain exams, vascular imaging, and full-body imaging. Recent data indicate that iodine-based contrast agents have brief durations of blood circulation and may lead to harmful toxicity effects. This study aims to produce silver nanoparticles using environmentally friendly synthesis techniques facilitated by microwaves. The characteristics of nanoparticles have been studied using UV-vis, FTIR, XRD, and TEM techniques. The TEM analysis reveals that the silver nanoparticle has an average diameter of 9 nm and exhibits a spherical shape. The contrast-to-noise ratio (CNR) values of silver nanoparticles at 100, 150, and 200 mg/L concentrations are 35.79, 48.16, and 74.66, respectively. In comparison, iodine exhibits CNR values of 28.57, 34.69, and 48.56 at the same concentrations. The CNR values for tube currents of 140, 160, and 180 mA are 37.83, 44.98, and 48.26, respectively. In contrast, the CNR values in silver nanoparticles are 63.64, 75.32, and 81.67. The results obtained from the different concentrations and tube currents clearly demonstrate that silver nanoparticles have a higher CNR than iopamidol. Hence, silver nanoparticles have significant potential as contrast agents.
ESTIMASI CELAH ENERGI DAN INDEKS BIAS SEMIKONDUKTOR SENG OKSIDA BERDASARKAN SPEKTRUM ABSORBSI ULTRAVIOLET-CAHAYA TAMPAK Nurhasanah, Iis; Arkadea Pringgodani, Andra
(JITEK)Jurnal Ilmiah Teknosains Vol 11, No 1/Mei (2025): Jitek
Publisher : Universitas PGRI Semarang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26877/jitek.v11i1/Mei.22901

Abstract

Celah energi dan indeks bias merupakan parameter intrinsik penting yang mencirikan sifat optik material, khususnya semikonduktor.  Penelitian ini bertujuan untuk mengestimasi celah energi dan indeks bias semikonduktor seng oksida dari spektrum absorbsi ultraviolet-cahaya tampak.  Seng oksida berbentuk batang diperoleh melalui proses presipitasi.  Spektrum absorbsi seng oksida diamati menggunakan spektrofotometer ultraviolet-cahaya tampak.  Analisis spektrum absorbsi ultraviolet-cahaya tampak memberikan celah energi seng oksida 2,8 eV.   Indeks bias seng oksida yang dihitung menggunakan berbagai model teoritis memberikan nilai yang bervariasi dari 2,28 sampai 2,84.  Seng oksida memiliki kemampuan menyerap cahaya ultraviolet sampai cahaya tampak (~ 450 nm) dan kemampuan tinggi untuk membiaskan cahaya, sehingga sesuai untuk aplikasi piranti optik dan optoelektronik yang bekerja dengan memanfaatkan radiasi ultraviolet dan cahaya tampak.
HUBUNGAN ANTARA VOLUME, KECEPATAN DAN KEPADATAN LALU LINTAS DENGAN MENGGUNAKAN METODE LINIER Nurhasanah, Iis; Susanto Haryadi, Eri; Rulhendri, Rulhendri
ASTONJADRO Vol. 1 No. 1 (2012): ASTONJADRO
Publisher : Universitas Ibn Khaldun Bogor

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32832/astonjadro.v1i1.784

Abstract

Arus lalu lintas berkenaan dengan teori lalu lintas menyebutkan bahwa pada saat sekarang ini dikonsentrasikan pada variabel-variabel volume (V/Flow), kerapatan kendaraan (Density/D/ Konsentrasi) dan Kecepatan Speed /Us). Ketiga variabel lalu lintas tersebut semakin hari semakin mendapat perhatian khusus dimana kesemuanya ini disebabkan arus/kondisi lalu lintas yang ada sekarang menggambarkan berapa banyak kendaraan yang bergerak pada saat bersamaan, dan semenjak hubungan dari ketiga variabel tersebut menggambarkan kualitas dari kapasitas dan tingkat pelayanan yang dialami oleh pengemudi masing-masing kendaraan. Penelitian ini akan mencari bagaimana hubungan dari ketiga variabel tersebut dengan media penelitian yaitu jalan KH. Sholeh Iskandar Bogor. Data dalam penelitian ini dicatat langsung dari lokasi penelitian, yaitu volume lalulintas dan kecepatan kendaraan. Kemudian data tersebut dianalisa sesuai dengan metode yang dikemukakan oleh Greenshield. Hasil penelitian ini adalah bagaimana hubungan kecepatan-kepadatan digambarkan sebagai sebuah garis lurus atau berfungsi linier dan bagaimana hubungan volume-kecepatan masing-masingdigambarkan sebagai garis lengkung.
A comparison of image quality of cerium oxide nanoparticles and iodine contrast agents in computed tomography scan Nasrullah, Faiz; Nurhasanah, Iis; Triadyaksa, Pandji; Rukmono, Dito Andi
Jurnal Pijar Mipa Vol. 18 No. 6 (2023): November 2023
Publisher : Department of Mathematics and Science Education, Faculty of Teacher Training and Education, University of Mataram. Jurnal Pijar MIPA colaborates with Perkumpulan Pendidik IPA Indonesia Wilayah Nusa Tenggara Barat

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/jpm.v18i6.6004

Abstract

Computed tomography (CT) scan, with iodine-based contrast, produces good image quality by improving the visualisation of relatively low-contrast internal body structures. However, the impact of using iodinated difference should be considered in patients susceptible to contrast allergy and renal impairment. Therefore, alternative contrast materials, such as cerium oxide nanoparticles (CeO2 NPs), must be used, with biocompatible properties and strong X-ray attenuation capabilities. This study compared the CT scan image quality of CeO2 NPs and iodinated contrast agents. This experimental study started by preparing a suspension of CeO2 NPs and iodine in aquabidest at a concentration of 500 ppm. The suspension was scanned using a CT scan with a helical scanning method. The exposure coefficient parameters were set for the tube voltage of 80 kV, Field of View of 28 cm, slice thickness of 5 mm, and tube current time of 150 mAs, 200 mAs, and 250 mAs. Then, CT images in DICOM data format were processed using MicroDICOM Viewer software. The quality of the CT scan images was analysed based on the CT number value, noise level, and contrast resolution. The images of CeO2 nanoparticles have higher CT values, lower noise levels, and better contrast resolution than those of iodine contrast agents. The results show that the CT image results of CeO2 NPs have better quality than those of iodine-containing contrast agents.
Precipitation Synthesis of CeO2 Nanopowder Pigment Nurhasanah, Iis; Astuti, Yayuk; Triadiyaksa, Pandji
Jurnal Rekayasa Kimia & Lingkungan Vol 18, No 1 (2023): Jurnal Rekayasa Kimia & Lingkungan (June, 2023 )
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v18i1.28648

Abstract

Nanopowder pigments of CeO2 and CeO2:Fe were synthesized by precipitation method at a moderate calcination temperature of 500oC. The pigments exhibited pale yellow for CeO2 nanopowder and brick red for CeO2:Fe nanopowder. Both pigments possessed mesoporous and cubic fluorite structures of CeO2. The incorporation of Fe into CeO2 reduced crystallite size and increased surface area. Moreover, it widens bandgap energy and significantly improved the absorption property of CeO2 nanopowder.
Fotokatalisis Nanopartikel Magnetis Zinc Ferrite dengan Penyinaran Cahaya UV dan Cahaya Tampak Nurhasanah, Iis; Priyono, Priyono; Karnaji, Karnaji; Richardina, Very
Jurnal Rekayasa Kimia & Lingkungan Vol 13, No 1 (2018): Jurnal Rekayasa Kimia & Lingkungan (June, 2018)
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v13i1.9953

Abstract

Nanopartikel magnetis ZnFe2O4 telah disintesis menggunakan metode presipitasi untuk degradasi rhodamine B dengan penyinaran cahaya UV dan cahaya tampak. Analisis pola difraksi sinar-X dan spektrum Fourier Transform Infrared (FTIR) menunjukkan pembentukan kubik spinel ZnFe2O4 dengan ukuran kristalit sekitar 13 nm. Spektrum absorpsi dalam rentang cahaya UV (200 nm) sampai cahaya tampak (~ 600 nm) dan celah energi 2,04 eV teramati dari pengukuran spektrofotometer UV-Vis. Sifat magnetik nanopartikel diukur menggunakan vibrating sample magnetometer (VSM) menunjukkan sifat magnet lemah yang sesuai untuk aplikasi magnetis fotokatalis. Nanopartikel ZnFe2O4 menunjukkan aktivitas fotokatalisis dengan cahaya UV maupun cahaya tampak untuk degradasi rhodamine B dengan konstanta laju reaksi 8,2 x 10-3 /menit dan 4,5 x 10-3/menit.
MIKROSTRUKTUR SENG OKSIDA YANG DISINTESIS MENGGUNAKAN EKSTRAK DAUN ANTING-ANTING Nurhasanah, Iis; Mukti, Nursanti Ajune; Paramita, Safira Arta
(JITEK)Jurnal Ilmiah Teknosains Vol 9, No 2/Nov (2023): JiTek
Publisher : Universitas PGRI Semarang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26877/jitek.v9i2/Nov.17270

Abstract

Cakupan aplikasi yang luas dari seng oksida telah meningkatkan produksi seng oksida menggunakan berbagai metode fisika dan metode kimia. Penggunaan bahan kimia berbahaya dalam produksi seng oksida, mendorong pemanfaatan bahan alam yang ramah lingkungan untuk mereduksi dampak lingkungan.  Penelitian ini bertujuan untuk mensintesis seng oksida dengan memanfaatkan ekstrak daun anting-anting.  Seng oksida disintesis menggunakan proses presipitasi dari campuran larutan seng nitrat dengan ekstrak daun anting-anting.  Produk presipitasi dikalsinasi pada temperatur 500oC selama 3 jam.  Mikrostruktur produk presipitasi dianalisis menggunakan difraksi sinar-x dan scanning electron microscope.  Pola difraksi sinar-x menunjukkan intensitas puncak-puncak difraksi yang tajam dan tinggi mengindikasikan pembentukan material kristalinitas tinggi.  Analisis parameter-parameter struktur menghasilkan nilai yang bersesuaian dengan struktur wurtzite dari seng oksida.  Partikel-partikel berbentuk bulat dengan ukuran 100 nm teramati pada citra electron microscope. Analisis mikrostruktur mengindikasikan bahwa seng oksida kristalin berhasil disintesis. Ekstrak daun anting-anting potensial sebagai bahan alami untuk sintesis oksida logam.
Co-Authors . Istadi Abidin, Nur Ade Ika Susan Affandi Faisal Kurniawan Agus Bashori Agus Subagio Aldilla Lutfia Ali Khumaeni Andi Wibowo Kinandana Andi Wibowo Kinandana Anwar Usman Arkadea Pringgodani, Andra Arnelli Arnelli Bambang Ariwahjoedi Eko Hidayanto Eko Hidayanto Fajar Arianto Fajar Arianto Fatikasari, Tanty Fauzan Musthafa Gunawan Gunawan H Hadiyanto Hella Arofah Heri Sutanto Hernowo, Alfian Holyness Nurdin Singadimedja I. Istadi Isrina Nur Laili Kadarisman Kadarisman Karnaji Karnaji Karnaji, Karnaji Khairurrijal Khairurrijal Kinasih, Diah Ayu Suci Maman Budiman MARIA BINTANG Maryanto - Mikrajudin Abdullah Muhammad Nur Muhammad Nur Mukti, Nursanti Ajune Nasrullah, Faiz Ndaru Adyono Nofi Marlini Nursidi Yunanto Nurul Wahyu Puspaningrum P Priyono, P Pandji Triadyaksa Paramita, Safira Arta Pratama Jujur Wibawa Priyono Priyono Ririn Futikhaningtyas Rukmono, Dito Andi Rulhendri Rulhendri Sari Pratiwi Singgih Wibowo Sukirno Sukirno Sulistia Nurdianik Sumariyah Sumariyah Susanto Haryadi, Eri Syamsul Arifin Syifa Avicenna Tri Windarti Triadiyaksa, Pandji Ummi Kaltsum Very Richardina Very Richardina Wahyu Ambikawati Weni Safitri Widiyanto Widiyanto Yayuk Astuti Yunita Indriyani Zaenal Arifin Zaenul Muhlisin Zaenul Muhlisin