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Jurnal Teknik Kimia USU

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Chemical Engineering, Chemistry & Bioengineering Chemistry Engineering

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Articles 349 Documents

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PERBANDINGAN GUGUS FUNGSI DAN MORFOLOGI PERMUKAAN KARBON AKTIF DARI PELEPAH KELAPA SAWIT MENGGUNAKAN AKTIVATOR ASAM FOSFAT (H3PO4) DAN ASAM NITRAT (HNO3) Vidyanova Anggun Mentari, Gewa Handika, Seri Maulina
Jurnal Teknik Kimia USU Vol 7, No 1 (2018)
Publisher : Universitas Sumatera Utara

Indonesia is one of the biggest producent of palm oil in the world. According to Badan Pusat Statistik (Central Bureau of Statistics), on 2016 wide of the palm oil estate in Indonesia is 11.672.861 Ha. The waste of palm oil plantations so many and isn’t used optimal, for the example is oil palm frond. Oil palm frond is one of the wet of waste with the number of production as much as 19.143.492 ton on 2016. This research will discuss the comparison of functional group and surface morphology activated carbon of oil palm frond with use H3PO4 and HNO3 as an activator. This research purpose to know the comparison of functional group and surface morphology activated carbon of oil palm frond with use H3PO4 and HNO3 as an activator. The method includes impregnation, carbonization, and washing process. The concentration of activator is 20% with 400 oC activation temperature. This research is used morphology surface activated carbon analysis with SEM and FTIR spectrophotometer. The result of analysis with SEM show there is pore formed on activated carbon and the indentification with spechtrophotometer FTIR shows that activated carbon is contain of functional group are C=O, C=C, C-C, N=O, C-N, C-OH, CH2 and C-H.

BIOBRIQUETTE PRODUCTION FROM PALM FRONDS AND SHELLS: EFFECT OF MATERIAL COMPOSITION AND PARTICLE SIZE Okta Bani; Iriany, Taslim; Cici Novita Sari; Cindy Carnella
Jurnal Teknik Kimia USU Vol 7, No 1 (2018)
Publisher : Universitas Sumatera Utara

Briquettes are solid fuels from organic materials with high calorific values and burn duration. The composition and particle size of the raw material may affect briquette quality. This study aimed to evaluate the effect of composition and particle size on calorific value and characteristics of the resulting briquettes. In this study, briquettes were made using palm oil fronds and shells at mass ratio of 1:2, 1:4, 1:6, 1:8 and particle size of not-dertemined, 50, 70, and 100 mesh. First, raw material was carbonized at 450°C for 30 minutes then added to 20%wt. starch glue and waste oil (1:1 ratio). Resulting briquettes were analyzed for its water content, ash content, density, volatile matter content, fixed carbon content, combustion rate, calorific value, and compressive strength. Satisfying results were obtained for briquettes with a front to shell ratio of 1:8, and a particle size of 100 mesh. At this condition, the resulting briquettes have water content of 5.5%; ash content of 2.54%; density of 0.51 g/cm3; 19.58% vapor content; fixed carbon content of 72.38%; combustion rate of 0.2 g/min (3.4×10-3 g/sec); calorific value of 15.3 kcal/g; and compressive strength of 0.06 N/mm2. These results have complied with the Indonesian National Standard (SNI), Japanese, American, and English standards, except for briquette compressive strength, which have not met the industrial standard.

STUDI PENGOLAHAN AIR BUANGAN DOMESTIK MENGGUNAKAN DIGESTER ANAEROBIK SATU TAHAP DAN DUA TAHAP Tamaria Kesia Hutasoit, Halimatuddahliana, Amir Husin
Jurnal Teknik Kimia USU Vol 7, No 1 (2018)
Publisher : Universitas Sumatera Utara

This research provides an analyzed performance of one and two-stage anaerobic digestion processes. One-stage and two-stage analyzed, individual, from substrate degradation, microbiological, metabolite and biogas production. First, the research initiated by acclimatization in a neutral condition and acid condition. Both one (R1) and two-stage (R2) digesters filled up with domestic wastewater. Into the digesters, it added cow dung as inoculums. pH in R1 maintained at pH 7 for 40 days and pH 5.5 in two-stage anaerobic: first stage (R2-1) for two days. After that, the mixture added with inoculums and then adjusted at pH 7 for the second stage (R2-2) for 38 days. The results showed that the substrate removal efficiency of two-phase is higher one-phase. The highest metabolite production obtained at R2-1: the 2nd day.

PENGOLAHAN LIMBAH CAIR TAHU MENGGUNAKAN BIOREAKTOR ANAEROB SATU TAHAP DAN DUA TAHAP SECARA BATCH Florence T.N. Silalahi, Halimatuddahliana, Amir Husin
Jurnal Teknik Kimia USU Vol 7, No 1 (2018)
Publisher : Universitas Sumatera Utara

This research aimed to study the effect of one stage and two stage anaerobic fermentation on the performance of bioreactors in tofu liquid waste treatment. This research started with acclimatization that is adaptation process of microorganism derived from cow dung with tofu liquid waste. Acclimatization is carried out in acid condition (pH 5.5) and in neutral condition (pH 7). This is followed by a batch bioreactor operation for 40 days for one stage anaerobic fermentation (pH 7), while for the first stage of the two stage anaerobic fermentation (pH 5.5) lasted two days and proceeds with the second stage of the two stage anaerobic fermentation (pH 7) lasts 38 days The results obtained were COD removal efficiency of 76.6% for one stage anaerobic and 83.05% for two stage anaerobic. While the VFA concentration in the first stage of the two stage anaerobic increased by 33% of the one-stage anaerobic VFA concentration. One-stage anaerobic biogas yield of 0.24 L/g CODconverted and 0.27 L/g CODconverted for to two stage anaerobic.

EFEKTIFITAS JENIS DESIKAN DAN KECEPATAN UDARA TERHADAP PENYERAPAN UAP AIR DI UDARA Rosdanelli Hasibuan, Ivo Dian Sari Marbun
Jurnal Teknik Kimia USU Vol 7, No 1 (2018)
Publisher : Universitas Sumatera Utara

Dry air is widely used in many fields, but the excessive water vapor in the air will make some problem and should be minimized to get the required dry air. The purpose of this research to observe the effect of air velocity and various of desiccants on the absorption of water vapor in the air on the tray dryer. The process of absorption of water vapor in the air performed with variations of the normal air velocity, 1.2 m/s, 2.3 m/s, and 3.6 m/s or volumetric rate of 0.059 m3/s; 0.113 m3/s; 0.178 m3/s and the type of desiccant of silica gel, alumina, and zeolite. Adsorption of water vapor in the air by desiccant was done by weighing the mass of desiccant before and after being crossed by air every interval of 60 minutes for 3 hours. Humidity measurement are performed on the upstream and downstream of the tray dryer to obtain a decrease in air humidity. The highest moisture adsorption using silica gel was obtained at velocities of 2.3 m/s and 3.6 m/s with adsorption of 0.266 grams water vapor / grams adsorbent and 0.264 grams water vapor / grams adsorbent as well as humidity of final air of 0.0194 kg water vapor/ kg dry air and 0.0198 kg water vapor/ kg dry air . The highest adsorption of water vapor using alumina was obtained at velocities of 2.3 m/s and 3.6 m/s with adsorption of 0.147 grams water vapor / gram adsorbent and 0.140 grams water vapor / gram adsorbent and the final humidity of 0.0207 kg water vapor / kg dry air and 0.0194 kg water vapor / kg dry air and the highest water vapor adsorption using zeolite was obtained at 3.6 m/s with the adsorption capacity of 0.130 grams water vapor / grams adsorbent and the final humidity of 0.0193 kg water vapor / kg dry air. Silica gel was the best desiccant in the process of moisture adsorption in air compared to alumina and zeolite.

PENGARUH PENAMBAHAN LAURIL ALKOHOL TERHADAP SIFAT-SIFAT UJI TARIK KOMPOSIT KARET ALAM TERISI SILIKA Rieska Wulandari Sianturi, Indra Surya
Jurnal Teknik Kimia USU Vol 7, No 1 (2018)
Publisher : Universitas Sumatera Utara

By using a semi-efficient vulcanisation system; the effects of lauryl alcohol (LA) as a new rubber additive on tensile properties of silica-filled natural rubber (NR) composites were investigated. The NR composites were filled by silica filler with a fixed loading, 30.0 phr (part per hundred rubber). The LA is a fatty alcohol based on palm kernel oil and incorporated into the silica-filled NR composites. The LA loadings were 1.0 phr, 2.0 phr, 3.0 phr and 4.0 phr. It was found that LA functioned as an internal plasticiser. As an internal plasticiser, LA decreased the tensile modulus and increased elongations at break of silica-filled NR composites. It was also found that LA increased the crosslink density and tensile strength up to 3.0 phr of LA loading. The 3.0 phr of LA was the optimum loading.

PENGARUH RASIO ISOPROPIL ALKOHOL TERHADAP RECOVERY DAN KARAKTERISTIK SERBUK PEKTIN DARI KULIT KAKAO Venitalitya A. S. Augustia; Dian Ika Nugraha; Sang Kompiang Wirawan
Jurnal Teknik Kimia USU Vol 7, No 2 (2018)
Publisher : Universitas Sumatera Utara

Cocoa is a fruit crop which is able to be planted in tropical climate, e.g. Indonesia. Generally, people only take the flesh of cocoa fruit and the peel is removed so that it will increase the volume of waste. The cocoa peel contains useful compounds for food and pharmaceutical industries, such as pectin. Hence, a research to increase the pectin retrieval quality from cocoa peel is needed in order to utilize the useful cocoa waste. Methods used in this research is solid-liquid extraction with water as solvent in the presence of acid (HCl). The process of making pectin powder is done through several steps here: (1) Raw material preparation, (2) Pectin extraction, and (3) Analysis of pectin powder. The extraction process is done at temperature of 70℃ for 90 minutes with the pH of the solvent is 1.5. The variation is done on the ratio of volume of isopropyl alcohol to the retrieved pectin. The result of the research shows that the recovery of pectin is at its peak at 6.50% with the percentage of water at 5,82%, equivalent weight of 6454,5242, metoxyl percentage of 5,76%, galacturonate percentage of 35,45%, and esterification level of 92,31%. The best quality of pectin, determined by the highest value of characterization, is obtained when the ratio of the filtrate to the volume of isopropyl alcohol is 1:1.

POTENSI PEMANFAATAN KITOSAN TERMODIFIKASI ASAP CAIR SEBAGAI BAHAN EDIBLE COATING ANTI MIKROBA UNTUK PENGAWETAN DAGING M. Hanafiah; M. Faisal; Izarul Machdar
Jurnal Teknik Kimia USU Vol 7, No 2 (2018)
Publisher : Universitas Sumatera Utara

This research is a preliminary study of the utilization of chitosan modified with liquid smoke to produce edible coating material that can be used as a preservative of beef. Chitosan compounds obtained from shrimp shell waste, while liquid smoke produced from pyrolysis of palm shells at a temperature of 340oC. Edible coating solution with various concentrations was made by dissolving chitosan (1-1.5%) into 3% liquid smoke, which was then applied as a meat preservative. Meat samples that have been dipped edible coating for 15 minutes, then stored in the refrigerator and observed decreased endurance every 24 hours for 8 days. Analysis results of Gas Chromatography-Mass Spectrometry (GC-MS) showed that liquid smoke contains phenol and acetic acid compounds that have antimocrobial properties. Meat endurance test was done by analyzing the aroma, texture and color of meat. The results showed that the beef that has been coated liquid chitosan solution can last up to 7 days. Chitosan concentration affects the endurance of meat, the greater the chitosan concentration, the better the meat endurance. The optimum concentration was obtained at 1% of chitosan, the meat still has an acceptable aroma, texture and color for up to 6 days. This suggests that chitosan-liquid smoke can be used as an edible coating material.

PIROLISIS PELEPAH KELAPA SAWIT UNTUK MENGHASILKAN FENOL PADA ASAP CAIR Seri Maulina, Nurtahara, Fakhradila
Jurnal Teknik Kimia USU Vol 7, No 2 (2018)
Publisher : Universitas Sumatera Utara

Palm midrib is a waste in oil palm plantations that containing cellulose, hemicellulose and lignin compounds. Palm midrib pyrolysis will produce phenol derived from lignin. The purpose of this study was to obtain phenol compounds as a function of time and temperature. The pyrolysis process was carried out at 200 °C, 300 °C, 400 °C, 500 °C and 600 °C with variation of pyrolysis time of 30 minutes, 60 minutes and 90 minutes. The analysis was performed using UV-Visible Spectrophotometer. The content of phenol compounds in liquid smoke increases with the rise of temperature and pyrolysis time. The highest total phenol content in liquid smoke was obtained at 600 °C for 90 minutes pyrolysis, which was 17.966%.

EKSTRAKSI KALIUM DARI KULIT BUAH KAPUK (Ceiba petandra) Chandra Sitorus, Lilis Sukeksi, Andy Junianto Sidabutar
Jurnal Teknik Kimia USU Vol 7, No 2 (2018)
Publisher : Universitas Sumatera Utara

The purpose of this study was to determine the best of combustion time and temperature of ash production from kapok fruit peel ( Ceiba Petandra ) to get the most potassium. The experiment was begun to dry kapok fruit peel for 24 hours at oven with temperature 110 oC and combustion to obtaine the ash from kapok fruit peel. The combustion was done by muffle furnace which time variables were from 3 hours, 4 hours, 5 hours, and 6 hours and burning temperature variables were from, 500 oC, 550 oC,600 oC, 650oC. The potassium that contained in ash have been extracted by distilled water with volume 30 ml for 24 hours. Observed responses were normality, pH, ash content, and potassium oxide content (% K2O). The best result of ash was in 3 hours with temperature 500 oC. The ash was analyzed by using AAS Atomic Absorption Spectroscopy, and 35.91 % of potassium oxide (K2O) content was obtained as maximum result.

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