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INDONESIA
Jurnal Teknik Kimia USU
Published by Universitas Sumatera Utara
ISSN : -     EISSN : -     DOI : -
Core Subject : Science, Engineering,
Chemical Engineering, Chemistry & Bioengineering Chemistry Engineering
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Articles 349 Documents
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EKSTRAKSI MINYAK ATSIRI BUNGA MELATI: PENGARUH RASIO MASSA BUNGA MELATI DENGAN VOLUME PELARUT N-HEKSANA, WAKTU EKSTRAKSI, DAN TEMPERATUR EKSTRAKSI Michael Dillo Rizki Ginting, Febrina Iskandar, Iriany, Okta Bani
Jurnal Teknik Kimia USU Vol 8, No 1 (2019)
Publisher : Universitas Sumatera Utara

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32734/jutek.v8i1.23753

Abstract

Jasmine flower (Jasminum sambac) contains essential oil compounds. Jasmine flower essential oil is a high-quality essential oil. Essential oils are volatile oils that have aroma similar to the original plant. Jasmine flower essential oil is sought due to its calming and anti-depression nature. In this study, the effect of extraction temperature, extraction time and solvent to jasmine flower ratio on jasmine oil was studied. The extraction was carried out at 30oC, 35oC, and 40oC for 2 hours, 3 hours, 4 hours, and 5 hours by using n-hexane. The ratio of jasmine flower to n-hexanes were 1:3; 1:4; and 1:5 (w/v). Resulting jasmine oil was analyzed by GC-MS, and its quality was assessed according to SNI 06-2385-2006 which include colour test, refractive index analysis, acid number analysis, and ester number analysis. This experiment showed that increasing of extraction time, extraction temperature, and volume of solvent lead to increase of absolute yield of jasmine essential oil. The highest jasmine oil yield obtained at 11.69 %. The jasmine oil contained was 47.14 % benzyl acetate and had yellow color. Its refractive index, acid number, and ester number were 1.478, 20.92 mg KOH/gram jasmine essential oil, and 150.27 mg KOH/gram jasmine essential oil respectively.
JTK USU Journal Management
Jurnal Teknik Kimia USU Vol 8, No 1 (2019)
Publisher : Universitas Sumatera Utara

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (13.549 KB) | DOI: 10.32734/jutek.v8i1.23757

Abstract

JTK USU
Efek Penambahan Antioksidan dan Demulsifier Secara Polimerisasi Pada Proses Penimbunan Diesel Fuel Venriza, Oksil; Lestari, Ika Gita; Riesdiawan, Yudhistira
Jurnal Teknik Kimia USU Vol. 12 No. 2 (2023): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32734/jtk.v12i2.9140

Abstract

B30 is an environmentally friendly fuel used for diesel engines. B30 is very easily contaminated with water sourced from the production process and raw materials from the B30. This water content causes corrosion and has an impact on landfilling. A demulsifier is a way to break down the B30 and water emulsion. In this study, the demulsifier used was acrylate-based and mixed with polar and non-polar solvents. The addition of a demulsifier with a volume of 2 mL, 5 mL, and 10 mL in the stockpiling process with variations of 2 hours, 4 hours, and 6 hours obtained an effect on the volume of water, where the volume of water increases with longer storage time. But the effectiveness of the demulsifier can be evaluated by potentiometrically measuring the water content and FTIR. The demulsifier that was made was also added with an antioxidant in the form of tertiary butylhydroquinone (TBHQ) with a concentration of 0.5 M and obtained more separate water layers than without the addition of TBHQ. To obtain the water content value after adding TBHQ, the coulometric and Fourier Transform Infra Red methods were used, which yielded higher results when compared to the absence of TBHQ. So that antioxidants and dimulsifiers have a positive effect on the process of storing diesel fuel.
Pengaruh Penambahan Polyvinyl Alcohol (PVOH) pada Biofoam dari Tepung Biji Nangka dan Ampok Jagung dengan Metode Thermopressing Fitrianti, Yanis; Azzahra, Rheisya Talitha; Kusumawati, Endang; Keryanti
Jurnal Teknik Kimia USU Vol. 12 No. 2 (2023): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32734/jtk.v12i2.9228

Abstract

Starch and fiber-based biofoam as a solution to replace the role of styrofoam. However, the biofoam still unqualified as a good foam characteristic. Polyvinyl alcohol (PVOH) is added to improve the physical characteristics of biofoam. This study aims to determine the effect of PVOH addition on the quality of starch-based biofoam from jackfruit seeds and corn hominy. The gelatinization process was carried out using a mixer in 350 rpm speed at 100 °C for 5 minutes, then moulded in a thermopressing unit for 25 minutes at 100 °C. The characteristics of the material with amylose and amylopectin contents 17.30% and 31.60% respectively and corn hominy's fiber content at 2.72%. The best PVOH addition was 10% addition based on its characteristics from parameters such as water absorption, density, and biodegradability were close to Synbra Technology’s standard. However, all the physical and mechanical characteristics of the produced biofoam still can't reach the standard.
Pengaruh Kondisi Operasi terhadap Karakteristik Pengeringan Jahe Merah (Zingiber officinale Var. Rubrum) Menggunakan Tray Dryer dengan Udara Panas dari Proses Pirolisis Hasibuan, Rosdanelli; Hamdanah Hasibuan; Yovani Nissi Madani; Viqry Pramananda; Risma Fazillah; Vikram Alexander
Jurnal Teknik Kimia USU Vol. 12 No. 2 (2023): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32734/jtk.v12i2.11496

Abstract

Red ginger (Zingiber officinale Var. Rubrum) is a rhizome plant often used as a complementary spice, a mixed ingredient in the food and beverages, and herbal medicines. One of the post-harvest processing of red ginger is drying, which aims to reduce the water content of red ginger to a point where the growth of microorganisms and the activity of enzymes that can damage red ginger can be prevented. This study aims to evaluate the effect of tray height and drying air temperature on moisture content, drying rate, drying characteristics, and quality of red ginger dried using a tray dryer with hot air from a biomass pyrolysis process. The results showed that both tray height and drying temperature affected red ginger's water content and drying rate. The quality of red ginger that complies with SNI 1-3393-1994 was obtained at a tray height of 60 cm and a drying temperature of 70 °C, with distinctive aroma and taste characteristics, the water content of 8,9%; ash content of 5,5%; oil content of 4,93 mL/100 g; and no fungus on the red ginger.
Pembuatan Gum Xanthan dengan Proses Fermentasi dari Hidrolisat Selulosa Eceng Gondok dan Penerapannya dalam Enhanced Oil Recovery Ramadhan, Handi; Arif Dharmawan, Wahyu; Susilowati, Titi
Jurnal Teknik Kimia USU Vol. 12 No. 2 (2023): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32734/jtk.v12i2.11574

Abstract

Water hyacinth is a freshwater plant that has a negative impact on waters, but has a high cellulose content (77.6%) and is still underutilized. One alternative in controlling the amount of water hyacinth is to utilize its potential cellulose content as an ingredient in xanthan gum. Fermentation was carried out with the help of Xanthomonas campestris and xanthan gum was obtained, which can be used as a polymer injection material to increase crude oil production in the oil refinery industry. The stages to obtain xanthan gum are delignification, hydrolysis, and anaerobic fermentation (28 °C) with a time variation of 24 hours to 120 hours with an interval of 24 hours. The cellulose hydrolysate variable is 0.5%, 1.0%, 1.5%, 2.0%, and 2.5%. The yield of xanthan gum in this research was 18%, with a moisture content was 13% – 15% and an ash content was 3% –3.9%. The resulting xanthan gum was analyzed for its functional groups using Fourier Transform Infra Red (FTIR) and was in agreement with commercial xathan gum.
Penggunaan Adsorben Bentonit pada Proses Pencucian Kering dalam Pemurnian Biodiesel Minyak Jelantah Amaliah Azis, Hijrah; Mustam, Mariaulfa; Ramdani, Nurfika; Amin, Ida Ifdaliah; Sari, Nurmala; Gregorius, Geraldy
Jurnal Teknik Kimia USU Vol. 12 No. 2 (2023): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32734/jtk.v12i2.11644

Abstract

Biodiesel can be made by utilizing used cooking oil through a chemical process, namely through a transesterification reaction, namely changing the oil (triglycerides) into fatty acid methyl esters. Washing must be done to remove the remaining impurities in biodiesel. The dry washing method is purification by utilizing the adsorption process to remove impurities in crude biodiesel. Bentonite is an alternative adsorbent that can be used as dry washing in the biodiesel refining process because it is cheaper, abundant in nature and has a layered structure with the ability to swell. The purpose of the study was to determine the ability of bentonite activated with acid as a dry washing agent in biodiesel purification. The research method used is the dry washing process method using bentonite adsorbents. The application of bentonite adsorbent as much as 6 grams with a contact time of 3 hours is the best operating condition to produce biodiesel with a pH of 6 and a clarity value of 96.7.
Efektivitas Katalis Zeolit Alam Ende pada Pirolisis Polietilena dari Sampah Plastik Bani, Gregorio Antonny
Jurnal Teknik Kimia USU Vol. 12 No. 2 (2023): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32734/jtk.v12i2.11822

Abstract

The high amount of plastic waste in landfills will pollute the environment. Direct combustion releases pollutants into the air, and recycling is only possible in small quantities. One method to overcome this problem is pyrolysis. However, pyrolysis requires a catalyst such as zeolite to accelerate the reaction rate, lower the activation energy, and improve the basic properties of the pyrolysis liquid. This study aims to characterize the activated natural zeolite Ende and determine the effect of the catalyst from the activated natural Ende zeolite on the activation energy, as well as the quality of the liquid resulting from the pyrolysis. Based on the research results, the activation process could change the degree of crystallinity became 36.63%, the surface area became 74.57 m2/g, the average radius became 20,21 Ã…, the pore volume became 72.34 cm3/g, and the number of acid sites became 4.342 NH3/g zeolite. Ende's active natural zeolite catalyst in the polyethylene pyrolysis process from plastic waste reduced the activation energy to 4,371.1 cal/mol in treating 0.10% catalyst composition from 1 kg of plastic. Increasing the temperature and catalyst improves the quality of pyrolysis oil, but the composition of the catalyst ratio is 0.10% of 1 kg of plastic.
Analisis Kuat Geser Perekat Alami Berbahan Soy Protein Isolate dengan Variasi Natrium Sulfit dan Asam Oksalat Koesman, Steven; Budhijanto; Bennet, David; Pancasakti, Bima
Jurnal Teknik Kimia USU Vol. 12 No. 2 (2023): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32734/jtk.v12i2.11929

Abstract

Along with the technology development, the use of bioadhesive for medical purpose is a common thing. The purpose of this bioadhesive is to give support for the medication because it can be decomposed and ejected by human body. This research aims to analyze the quality of bioadhesive made of soy protein isolate (SPI) as main ingredient. SPI has food-grade level of safety thus it is safe for human body. This bioadhesive is made by two main processes: denaturation of protein dan acid crosslinking. The processes are done under condition of 55 °C dan atmospheric pressure for 30 minutes dan 10 minutes. Shear strength, wet shear strength, viscosity, solid content, and fourier transform infrared spectroscopy (FTIR) analysis were done to find out the impact of oxalic acid addition. The best shear strength result obtained was 1.9051 MPa and wet shear strength result was 1.6093 MPa.
Ekstraksi Minyak Atsiri Kulit Jeruk Lemon (Citrus limon (L.) Burm.f.) dengan Pretreatment Microwave dan Distilasi Air-Uap Elvianto Dwi Daryono; Dwi Ana Anggorowati; Firyaal Putri Verdina; Vina Nur Laily
Jurnal Teknik Kimia USU Vol. 12 No. 2 (2023): Jurnal Teknik Kimia USU
Publisher : Talenta Publisher (Universitas Sumatera Utara)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32734/jtk.v12i2.12923

Abstract

Lemon peel is a waste containing essential oils which can be used as an aroma enhancer in food and drinks as well as aromatherapy. This study aims to determine the effect of microwave pretreatment power and time on the extraction of lemon peel essential oil. The research phase began with microwave pretreatment, namely lemon peel was put into the microwave with pretreatment times of 2 minutes, 4 minutes, 6 minutes, 8 minutes, and 10 minutes with microwave power of 100 W, 200 W, and 300 W followed by water-steam distillation 150 g of lemon peel. Furthermore, the distillate is put in a separatory funnel for ± 12 hours to separate the essential oil and water. The top layer is essential oil added ± 5 g of sodium sulfate (Na2SO4) to adsorb water. The best conditions for the extraction process of lemon peel essential oil was at 300 W microwave power and 2 minutes of pretreatment which produces clear yellowish lemon peel essential oil with a distinctive lemon smell with a yield of 4.88%, limonene content of 27.501%, and refractive index of 1.48.

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