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Journal of Material Science and Radiation
Published by Balai Publikasi Indonesia
ISSN : -     EISSN : 31235379     DOI : https://doi.org/10.56566/jmsr
Core Subject : Science,
Materials Science & Nanotechnology Physics
Journal of Material Science and Radiation (JMSR) is an open-access, peer-reviewed scientific journal dedicated to the advancement of knowledge in the fields of materials science and radiation. The journal publishes original research articles, comprehensive scientific reviews, and concise scientific communications that are relevant and up to date. JMSR covers a wide range of topics related to material and radiation studies, and promotes interdisciplinary collaboration to support innovation and sustainable development in these fields. As an open-access journal, all articles published by JMSR are freely accessible to the academic community and the general public worldwide. This policy not only enhances the visibility and accessibility of research findings but also increases the scientific impact of each published work. Copyright of all articles is retained by the journal, while authors are granted a license to distribute their work for non-commercial purposes, provided that appropriate citation and attribution are given to the original publication in JMSR.
Arjuna Subject : Ilmu Material (semua kategori) - Ilmu Material (Lain-Lain)
Articles 17 Documents
 1   2 
Chemical, Structural and Thermal Analysis of PET Flakes induced by Electron Beam Irradiation Nor Batrisya Ismail; Mohd Hamzah Harun; Izzuddin Mohamad Zaharuddin; Norfazlinayati Othman; Mahathir Mohamed; Mohd Sofian Alias; Mohd Faizal Abd Rahman; Khairil Nor Kamal Umar; Nurul Huda Mudri; Khairul Azhar Abdul Halim; Rida Tajau; Rusdyana Natasa Ghazali; Siti Nur Eyisha Wafa Mohd Aminuddin
Journal of Material Science and Radiation Vol. 1 No. 2 (2025): August
Publisher : Balai Publikasi Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.56566/jmsr.v1i2.393

Abstract

This study presents a comprehensive chemical, structural, and thermal characterization of polyethylene terephthalate (PET) flakes subjected to electron beam irradiation at doses of 0, 40, and 120 kGy. Post-consumer PET bottle flakes were analyzed using Fourier Transform Infrared Spectroscopy (FTIR), X-ray Diffraction (XRD), and Thermogravimetric Analysis (TGA) to determine irradiation-induced modifications. FTIR results reveal noticeable variations in key functional groups, particularly in the ester (C=O and C–O) and aromatic regions, indicating chain scission, partial cross-linking, and oxidation with increasing radiation doses. XRD analysis shows a progressive reduction in peak intensity and an increase in peak broadening, signifying decreased crystallinity and enhanced amorphous character due to structural disorder. TGA measurements demonstrate improved thermal stability of irradiated PET, with major degradation shifting from ~450 °C in the non-irradiated sample to ~480 °C after irradiation, and a clearer two-stage degradation pattern associated with structural rearrangements. These findings confirm that electron beam irradiation induces significant yet controlled modifications on PET’s molecular structure, crystallinity, and thermal behavior. Such property alterations highlight the potential of electron beam treatment as an effective pre-processing approach to enhance the recyclability and performance of waste PET, contributing to more sustainable plastic waste management strategies
Effect of Gamma Irradiation on the Optical Characteristics of PVA-PANI Composite Polymer Films Norfazlinayati Othman; Mohd Hamzah Harun; Mahathir Mohamed; Mohd Sofian Alias; Zainal Abidin Talib
Journal of Material Science and Radiation Vol. 1 No. 3 (2025): December
Publisher : Balai Publikasi Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.56566/jmsr.v1i3.394

Abstract

This manuscript reports the optical and structural characteristics of PVA/PANI composite polymer films synthesized through gamma-irradiation-induced in-situ polymerization. The in-situ formation of the conductive emeraldine salt phase of polyaniline (PANI) within the polyvinyl alcohol (PVA) binder matrix was achieved under different irradiation doses. The formation of the conductive PANI phase and the presence of Cl⁻ counter-ions were confirmed through FESEM morphological analysis and EDAX elemental mapping, respectively. XRD spectra further verify the semi-crystalline nature of the composite and indicate the structural role of PVA as a binder in stabilizing the polymeric composite system. Thermal behavior analysis using TGA reveals four distinct decomposition phases, with the most pronounced thermal transition observed in the composite irradiated at 50 kGy, suggesting enhanced structural interactions between PVA and PANI at this irradiation dose. Overall, the results demonstrate that gamma irradiation is an effective route for modifying the optical, structural, and thermal properties of PVA/PANI composites, making them promising candidates for optoelectronic and conductive polymer applications
Comparative Characterisation of Structural and Superconducting Properties of Y-123 and Y-247 Synthesised by Thermal Treatment at 980 °C Siew Hong Yap; Tai Pao Er; Mohd Mustafa Awang Kechik; Muhammad Khalis Abdul Karim; Hussien Baqiah; Soo Kien Chen; Kean Pah Lim; Muhammad Kashfi Shabdin; Nurhidayah Mohd Hapipi; Aliah Nursyahirah Kamarudin; Arebat Ryad Alhadei Mohamed; Aris Doyan; Abdul Halim Shaari
Journal of Material Science and Radiation Vol. 1 No. 3 (2025): December
Publisher : Balai Publikasi Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.56566/jmsr.v1i3.425

Abstract

This study presents a comparative analysis of the structural and superconducting properties of YBa₂Cu₃O₇−δ (Y-123) and Y₂Ba₄Cu₇O₁₅−δ (Y-247) superconductors synthesised via a thermal treatment method at 980 °C. Metal nitrates were used as starting precursors, with polyvinylpyrrolidone (PVP) serving as a capping agent to enhance dispersion and control microstructure. X-ray diffraction (XRD) confirmed that Y-123 and Y-247 were the dominant phases in their respective samples, although minor peaks of BaCuO₂ were detected, indicating the presence of secondary phases. Scanning electron microscopy (SEM) revealed that Y-247 exhibited larger grain morphology and higher porosity than Y-123, suggesting that the chosen sintering temperature exceeds the thermal stability range for the Y-247 phase. Electrical resistivity measurements showed a single superconducting transition for both samples, with Y-123 exhibiting a sharper transition width (ΔTc = 8.1 K) compared to Y-247, indicating better grain connectivity and phase uniformity. Energy dispersive X-ray spectroscopy (EDX) supported the elemental presence of Y, Ba, Cu, and O in both samples, though variations in stoichiometry were attributed to secondary phases. The observed expansion in the c-axis lattice of Y-247, combined with its higher porosity, points to oxygen loss during sintering, which contributes to the reduced superconducting performance. Overall, the results confirm that both Y-123 and Y-247 can be successfully synthesised using a simple and environmentally friendly thermal treatment method. However, Y-123 exhibits better structural integrity and superconducting performance at the high sintering temperature of 980 °C, making it a more promising candidate for large-scale production of bulk high-temperature superconductors.
Comparative Study of Y123 Superconductors Synthesized Under Open Air and Oxygen Flow Conditions Aliah Nursyahirah Kamarudin; Mohd Mustafa Awang Kechik; Muhammad Azri Khairudin; Chen Soo Kien; Lim Kean Pah; Muhammad Kashfi Shabdin; Abdul Halim Shaari
Journal of Material Science and Radiation Vol. 1 No. 3 (2025): December
Publisher : Balai Publikasi Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.56566/jmsr.v1i3.426

Abstract

YBa₂Cu₃O₇₋δ (Y123) superconductors is a widely studied high-temperature superconductor due to its high critical temperature, Tc and strong flux pinning properties. In this study, Y123 samples were synthesized via a thermal treatment method under two sintering conditions which were open air and oxygen flow. Structural, microstructural, and superconducting properties were evaluated using X-ray diffraction (XRD), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX), and AC susceptibility measurements. XRD analysis revealed that all Y123 samples exhibited predominantly Y123 phase with orthorhombic structure, with minor secondary phases. The Y123 sample prepared in an open-air condition exhibited larger grain size (0.698 µm), lower porosity, and fewer impurities compared to sample prepared in the oxygen flow condition. AC susceptibility showed a higher Tc-onset exhibited at 92.1 K in the open-air sample, indicating better grain connectivity. These results suggest that open-air sintering offers a simpler, cost-effective route for enhancing Y123 superconductor performance.
Influence of Sintering Temperatures on Pr0.7Ba0.3MnO3 Prepared Using Thermal Treatment Method Xiao Tong Hon; Kean Pah Lim; Lik Nguong Lau; Mohd Mustafa Awang Kechik; Soo Kien Chen; Muhammad Kashfi Shabdin; Nurhidayah Mohd Hapipi; Najihah Rohiat; Abdul Halim Shaari
Journal of Material Science and Radiation Vol. 1 No. 3 (2025): December
Publisher : Balai Publikasi Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.56566/jmsr.v1i3.478

Abstract

In this work, Pr0.7Ba0.3MnO3 (PBMO) was synthesised using a thermal treatment method with sintering temperature ranging from 800 °C to 1100 °C. X-ray diffraction (XRD) confirmed the formation of pure PBMO phase at 1100 °C, while lower sintering temperatures led to the presence of secondary phase, particularly Pr(Mn2O5). Microstructural analysis revealed significant grain growth with rising sintering temperatures, accompanied by enhanced crystallinity and reduced secondary phases. Magnetic measurements indicated ferromagnetic behaviour at room temperature for all samples. However, the electrical resistivity demonstrates an unexpected increase with sintering temperature, attributed to the influence of secondary phase at lower sintering temperatures and grain growth in the pure PBMO phase at higher sintering temperatures. Additionally, microstructural defects such as oxygen non-stoichiometry or porosity might further contribute to the suppression of the metal-insulator transition temperature. Overall, this study highlights the significant role of sintering temperatures in controlling the phase purity, microstructure and physical behaviour of PBMO samples, offering valuable insights for their potential applications in spintronics or magnetic sensing devices.
Characterization of Photocurable Functionalized-CNT Nanocoating to Mitigate the Naturally Emission of Radon Gas Aisha Dalila Ab Aziz; Mohd Hamzah Harun; Izzuddin Mohamad Zaharuddin; Nor Adnin Ezani Mohd Ezani; Norfazlinayati Othman; Mahathir Mohamed; Mohd Sofian Alias; Mohd Faizal Abd Rahman; Khairil Nor Kamal Umar; Nurul Huda Mudri; Khairul Azhar Abdul Halim; Mohamad Syahiran Mustafa; Lakam Mejus; Faizal Azrin Abdul Razalim; Rosley Che Ismail; Abdul Muiz Mohd Sani; Sharilla Mohd Faisal; Rida Tajau
Journal of Material Science and Radiation Vol. 1 No. 3 (2025): December
Publisher : Balai Publikasi Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.56566/jmsr.v1i3.480

Abstract

This study focuses on the synthesis and characterization of an anti-radon photocurable nanocoating formulated using a UV-curable formulation incorporated with functionalized carbon nanotubes (F-CNTs). The coating was prepared using Ebecryl 600 (urethane acrylate oligomer) and TMPTA (monomer), with GPTMS as a coupling agent and various photoinitiator combinations. Different F-CNT loadings ranging from 0.1 to 0.9 wt% were studied to evaluate their effects on coating performance. The samples were cured under UV irradiation for 2–20 passes to investigate the influence of exposure time on polymer crosslinking. Characterization analyses including pendulum hardness, Fourier-transform infrared spectroscopy (FTIR), viscosity, gel content, and radon gas permeability were performed. Results indicated that the incorporation of F-CNTs enhanced the mechanical strength and crosslinking density of the coating. The optimal formulation exhibited a hardness of 150.33 s (BAPO + 8 passes) and a gel content of 97%. Furthermore, radon concentration measurements showed a 28.9% reduction after applying a single coating layer, confirming the coating’s potential as an effective barrier for radon gas mitigation.
Synthesis of Carbon Nanomaterials from Polyethylene Terephthalate (PET) Waste Using Chemical Vapor Deposition Nor Adnin Ezani Mohd Ezani; Mohd Hamzah Harun; Izzuddin Mohd Zaharuddin; Norfazlinayati Othman; Mahathir Mohamed; Mohd Sofian Alias; Mohd Faizal Abd Rahman; Khairil Nor Kamal Umar; Nurul Huda Mudri; Khairul Azhar Abdul Halim; Farah Fadzehah Hilmi; Rida Tajau
Journal of Material Science and Radiation Vol. 1 No. 3 (2025): December
Publisher : Balai Publikasi Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.56566/jmsr.v1i3.482

Abstract

Upcycling is an effective approach to reduce plastic waste, polyethylene terephthalate (PET) and promote sustainability. Plastic bottles usually were made from PET polymer and a raw material to produce carbon nanomaterials (CNMs). CNMs are synthesized using chemical vapor deposition (CVD) process and purified to eliminate catalysts and unwanted compounds. Various catalysts were used to investigate the economic and effective in producing the CNMs. Metal catalysts such as ferrocene, cobalt and iron are the important elements in the CVD process as they provide surfaces for carbon to attach. CNMs morphology and graphitic structure were observed from Raman analysis and TEM analysis. The application of upcycling offers the advantage of utilizing low-cost raw materials to produce higher-value products, providing additional benefits.

Page 2 of 2 | Total Record : 17

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