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Science and Technology Indonesia

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Published by Universitas Sriwijaya

ISSN : 25804405 EISSN : 25804391 DOI : -

Core Subject : Science, Social, Engineering,

Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Environmental Science Materials Science & Nanotechnology Physics

An international Peer-review journal in the field of science and technology published by The Indonesian Science and Technology Society. Science and Technology Indonesia is a member of Crossref with DOI prefix number: 10.26554/sti. Science and Technology Indonesia publishes quarterly (January, April, July, October). Science and Technology Indonesia is an international scholarly journal on the field of science and technology aimed to publish a high-quality scientific paper including original research papers, reviews, short communication, and technical notes. This journal welcomes the submission of articles that covers a typical subject of natural science and technology such as: > Chemistry > Biology > Physics > Marine Science > Pharmacy > Chemical Engineering > Environmental Science and Engineering > Computational Engineering > Biotechnology Journal Commencement: October 2016

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Articles 551 Documents

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Tablet Formula Optimization From Helminthostachys Zaylanica Extract Using A Simplex Lattice Design Fitrya Fitrya; Najma Annuria Fithri; Budi Untari; Aprililianti
Science and Technology Indonesia Vol. 6 No. 3 (2021): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Helminthostachys zeylanica extract has pharmacological activities such as antioxidant, antiinflamatory, and antihyerucemia. This extract is nontoxic substance from the acute and subchronic toxicity tests. This extract has a potency to be formulated into tablet dosage forms. This study aims to optimize a tablet formula from Helminthostachys zeylanica extract. Disintegrant and binder concentrations were independent variables, while physical properties and dissolution time of the tablets were dependent variables. The tablet was prepared by a wet granulation method. Formula was optimized by Simplex Lattice Design. Physicochemical propertiesof granule, physical properties and dissolution of tablet were then analyzed with One Way ANOVA (p = 0.05). Based on granule analysis, specification of physicochemical parameters, such as hausner’s ratio, compressibility index, flowability, repose angle, and water content, met standard British Pharmacopeia. In addition, the starch and PVA concentrations influenced thickness, weight variation, hardness, friability, disintegration time and dissolution of the tablets (p <0.05), except for friability (p> 0.05). Based on this study, the starch and PVA concentrations for the optimum tablet formula were 19.5% and 1.05%, respectively.

Utilization of Activated Charcoal from Sawdust as an Antibiotic Adsorbent of Tetracycline Hydrochloride Gatut Ari Wardani; Ega Maulana Qudsi; Anindita Tri Kusuma Pratita; Keni Idacahyati; Estin Nofiyanti
Science and Technology Indonesia Vol. 6 No. 3 (2021): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

The use of activated charcoal from sawdust as an adsorbent of tetracycline hydrochloride compounds has been successfully carried out. Sawdust activated charcoal was carbonized at 450°C for 40 minutes with a charcoal size of 100 mesh and activated using H3PO4 solution. The characteristics of active sawdust charcoal showed that water content, iodine adsorption, and methylene blue adsorption had met SNI 06-3730-1995 regarding technical activated charcoal. Testing the morphology of charcoal using a Scanning Electron Microscope showed that the charcoal pores were opened through the activation process. In the functional group analysis test using infrared spectroscopy, the active group contained in charcoal after being activated contained carbon atoms that were purer than sawdust. The adsorption process of tetracycline hydrochloride using sawdust activated charcoal is known to follow Ho orPseudo second-order (K = 0.0039 g/mg.min), while the adsorption isotherm follows the Langmuir equation, KL = 0.0076 L/mg and adsorption capacity amounting to 242.1307 mg/g. Thermodynamically, the adsorption process occurs not spontaneously with a Gibbs free energy value of 120.8949 kJ/mol and occurs by chemisorption.

Silica from Natural Sources: a Review on the Extraction and Potential Application as a Supporting Photocatalytic Material for Antibacterial Activity Annisa Luthfiah; Yusi Deawati; M. Lutfi Firdaus; Iman Rahayu; Diana Rakhmawaty Eddy
Science and Technology Indonesia Vol. 6 No. 3 (2021): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Silica has become a popular material due to its high abundance and many advantages in various fields. This material can be produced synthetically and extracted from nature with resultant advantages in the application of green production. Therefore, this article deals with the form of silica extracted from quartz sand, leaves, and agricultural wastes found in nature. The extraction process from various sources would be described using thermal, biological, and chemical methods. This review also highlights the potential application of silica as a photo catalytic antibacterial-supporting material and discusses its role in increasing the effectiveness of the process. The discussion was continued with research on this procedure, where synthetic auxiliary materials were compared to the extracted silica. Furthermore, results obtained indicated that the extracted material had very good potential as a photocatalyst adjunct in its application in the antibacterial field.

Antibacterial Activity of Endophytic Fungi from Sembukan (Paederia foetida L.) Leaves Hary Widjajanti; Christina Vivid Handayani; Elisa Nurnawati
Science and Technology Indonesia Vol. 6 No. 3 (2021): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

The antibiotic resistance of phatogenic bacteria has become a serious health problem and has encouraged the search for novel and effective antimicrobial metabolites. Meanwhile, endophytic fungi have great potential as a natural source for antimicrobial agents. The endophytic fungi that live in plant tissue produces secondary metabolites which potentially act as an antibacterial compound. The isolation of fungi for antibacterial sources reduces the large amount of plant as a source of antibacterial agents. Hence, this study aims to obtain endophytic fungi isolates from Paederia foetida L. that are capable of producing secondary metabolites as antibacterial, carry out in vitro tests to verify the antibacterial properties of secondary metabolites of the Paederia foetida L. endophytic fungi, and identify the potential of Paederia foetida L. endophytic fungi in producing antibacterial compounds. The antibacterial activity was tested against Escherichia coli ATCC8739 and Staphylococcus aureus ATCC6538 while seven isolates of endophytic fungi that potentially produced antibacterial were obtained from Sembukan (P. foetida L.). The results showed that antibacterial activities of SL1, SL4 and SL6 secondary metabolites against S. aureus ATCC6538 and E. coli ATCC8739 were moderate to strong activities. Furthermore, the Minimum Inhibition Concentration (MIC) of secondary metabolites extract of SL1 against S. aureus ATCC6538 value was 250 ????g/mL while the values of MIC extract of SL4 against S. aureus ATCC6538 and E. coli ATCC8739 were 125 ????g/mL and 250 ????g/mL respectively and MIC extract of SL6 against E. coli ATCC8739 value was 125 ????g/mL. The secondary metabolites extract of SL1 isolate were alkaloid and tannin, SL4 were phenolic and alkaloid while SL6 isolate were alkaloid and terpenoid. Hence, endophytic fungi SL1 isolate was identified as Fusarium sp., SL4 as Dematophora sp., and SL6 isolate as Acremonium sp.

Heterogeneous Catalytic Conversion of Citronellal into Isopulegol and Menthol: Literature Review Amri Yahya; Dwiarso Rubiyanto; Is Fatimah
Science and Technology Indonesia Vol. 6 No. 3 (2021): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

The conversion of citronellal into isopulegol is a key route in the production of a number of important chemicals. In the perspective of green conversion, the use of a heterogeneous catalyst is superior due to its ease in separation and reusability, so it facilitates a highly economical conversion. In this review, we examine the use of some transition metals in cyclization reactions, which are suitable for citronellal conversion into isopulegol, and consider the potential progress in clay-based catalysts. The structure of clay which potentially provides the porosity by modification and supporting active metal is proposed to be the low-cost catalyst for the conversion. As other mechanism by porous materials-supported metal, the porosity of clay support contributes to conduct thesurface adsorption mechanism and the Broensted acid supply, meanwhile the metal acts as active site for cyclization, and in the one-pot conversion into menthol, as both cyclization and hydrogenation.

The Ability of Composite Ni/Al-carbon based Material Toward Readsorption of Iron(II) in Aqueous Solution Normah Normah; Neza Rahayu Palapa; Tarmizi Taher; Risfidian Mohadi; Hasja Paluta Utami; Aldes Lesbani
Science and Technology Indonesia Vol. 6 No. 3 (2021): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

In this research, NiAl-LDH was synthesized using the coprecipitation method and modified with biochar and graphite to produce NiAlbiochar and NiAl-graphite composite materials. The adsorbent that has been synthesized is used for the application of adsorption of Fe(II) ions in aqueous solution. The resulting material was characterized by XRD (X-ray Diffraction) analysis, spectrophotometer FT-IR, BET analysis for determine the specific surface area and TG-DTA analysis. XRD diffractogram showed that the NiAl-Biochar and NiAl-graphite composite material had the diffraction pattern characteristic of the precursor. LDH that has been modified will have a larger surface area than the precursor. The surface area of NiAl-biochar reaches 438.942 m2/g and the surface area of NiAl-graphitereaches 21.595 m2/g. This composite material supports adsorbents with a large adsorption capacity to adsorb metals. Adsorption of Fe (II) using NiAl-Biochar and NiAl-graphite was stable for five regeneration cycles (<75.30%). The Fe(II) ion adsorption process tends to follow the Langmuir isotherm model which has a maximum capacity value (Qmax) of NiAl-Biochar composite material reaching 20 times with a value of 243.902 mg/g and the NiAl-graphite composite reaching 72.464 mg/g, so that the carbon-based composite material is considered effective. adsorbent to remove Fe(II) ion and can increase the stability of the structure for adsorption regeneration. The results of the analysis of thermodynamic parameters showed that the adsorption process was endothermic, tookplace spontaneously and the solid-liquid phase interface increased according to the increasing degree of disorder.

The Capability of Biochar-Based CaAl and MgAl Composite Materials as Adsorbent for Removal Cr(VI) in Aqueous Solution Novie Juleanti; Neza Rahyu Palapa; Tarmizi Taher; Nurlisa Hidayati; Bunga Indah Putri; Aldes Lesbani
Science and Technology Indonesia Vol. 6 No. 3 (2021): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

The development of layered double hydroxide materials into composites with carbon-based materials in the form of CaAl-Biochar and MgAl-Biochar has been successfully carried out. The success parameters of the preparation process include XRD, FT-IR, Adsorption-Desorption N2, SEM, and TG-DTA. The success through XRD is evidenced by the appearance of the typical diffraction peaks of double-layer hydroxy around 2???? = 11°(003), 20°(006), and 60°(113). In addition, there is diffraction around 22°(002) which is the typical diffraction of biochar. FT-IR analysis showed successful preparation in the presence of functional groups around 1381cm−1 which indicated nitrate vibrations from double-layer hydroxy. Another spectrum that also appears on 1103 cm−1 is a characteristic of biochar (???? Si-O-Si). Adsorption-Desorption N2 analysis showed that the surface area data of 2 −1 2 −1 CaAl-Biochar was greater than MgAl-Biochar, which were 150.987 m .g and 111,404 m .g , respectively. The adsorption capacity of CaAl-Biochar reached 588.235 mg.g−1 and 426.316 mg.g−1 for MgAl-Biochar. The adsorbent materials of CaAl, MgAl, Biochar, CaAl-Biochar, and MgAl-Biochar tend to follow the Langmuir isotherm model with adsorption processes that tend to be spontaneous. The results of regeneration of the composite material lasted up to 5 cycles. The first cycle of CaAl-Biochar reached 96.647% to 82.666% in the last cycle, while MgAl-Biochar reached 90.885% in the first cycle to 73.454% in the last cycle.

Chemical Characterization of Secondary Metabolite from the Endophytic Fungus Trichordema reecei isolated from The Twig of Syzygium aqueum Ummi Hiras Habisukan; Elfita Elfita; Hary Widjajanti; Arum Setiawan
Science and Technology Indonesia Vol. 6 No. 3 (2021): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Endophytic fungi are microorganisms that live in plants, without negative effects and are mutually related to hosting plants. Exploration of bioactive compounds from Endophytic fungi is easier and cheaper because they do not require a large area, a short growing time, and uncomplicated mixed compounds. Endophytic fungi are new and patent base secondary metabolites but they are not extensively characterized and investigated for the exploration of raw materials for drugs. The purpose of this study was to obtain antioxidant secondary metabolites from Endophytic fungi that live in the Syzygium aqueum medicinal plant. In this study, Endophyticfungi were isolated from S. aqueum twigs and molecular identification. The secondary metabolites were isolated by chromatographic method and chemical structure identified by spectroscopy. Antioxidant activity was evaluated by method 1,1diphenyl-2-picryl hydrazyl (DPPH). Phylogenetic analysis showed the Endophytic fungi of S. aqueum twig have a high similarity with the Trichordema reecei twig 19MSr.B2.3. The secondary metabolites from the ethyl acetate extract of the liquid culture of the fungus were identified as (4-hydroxy-3-(4-hydroxyphenyl)-5 oxotetrahydrofuran-2-yl) methyl acetate with IC50= 75.13 ????g/mL. The secondary metabolites can be developed into starting molecules for potential antioxidant agents.

The Utilization of Modified Chitosan from Shrimp Shell As Photodegradation of Pesticides Paraquat Dichloride Risfidian Mohadi; Neza Rahayu Palapa; Rudi Hartono; Nurlisa Hidayati; Rozirwan
Science and Technology Indonesia Vol. 6 No. 3 (2021): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

In this study, the chitosan modification of shrimp shell has been made by impregnated the chitosan from shrimp shell with Ti/ZrO2 and ZrO2 to formed composite of chitosan-Ti/ZrO2 and chitosan-ZrO2. These composites were made by immobilization technique and characterized by FTIR and SEM-EDX. The chitosan-Ti/ZrO2 and chitosan-ZrO2 composite were used as a catalyst to degrade the pesticide paraquat dichloride in the presence of UV light (????= 257 nm). The photodegradation process of paraquat dichloride takes place under 10 watts UV light irradiation and was measured using spectrophotometer UV. The maximum degradation percentage of pesticide paraquat dichloride photodegradation by chitosan-Ti/ZrO2 and chitosan-ZrO2 composites are 61.97% and 57.97% within 30 minutes irradiation time.

Modification of Cu/Cr Layered Double Hydroxide by Keggin Type Polyoxometalate as Adsorbent of Malachite Green from Aqueous Solution Neza Rahayu Palapa; Tarmizi Taher; Alfan Wijaya; Aldes Lesbani
Science and Technology Indonesia Vol. 6 No. 3 (2021): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Modification of Cu/Cr layered double hydroxides (LDHs) has been conducted by intercalation using Keggin type polyoxometalate [a-SiW12O40]4- to form CuCr-[a-SiW12O40]. The materials were analyzed by XRD, FTIR, and surface area analyses. Furthermore, materials were used as selectivity adsorbents of cationic dyes such as malachite green, rhodamine-B and methylene blue. The malachite green is more selective than others from an aqueous solution. The adsorption of malachite green showed that the adsorption capacity of CuCr-[a-SiW12O40] was higher than pristine LDHs. The adsorption process was followed pseudo second order kinetic model and Langmuir isotherm adsorption. The Qmax value of CuCr-[a-SiW12O40] reached 55.322 mg/g at 323 K after 100 minutes adsorption time. Thermodynamic parameters such as ΔG, ΔH and ΔS confirm that the adsorption process was endothermic, spontaneous, and more favorable at high temperatures. The intercalated material was higher structural stability toward reusability adsorbent than pristine LDHs.

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