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All Journal Jurnal Sains Materi Indonesia Journal of Batteries for Renewable Energy and Electric Vehicles
Hapsari, Ade Utami
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Chemical Engineering, Chemistry & Bioengineering Electrical & Electronics Engineering Energy Engineering Industrial & Manufacturing Engineering Materials Science & Nanotechnology Mechanical Engineering

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The Influence of Anodizing Electrolyte Concentration on Ni-P Deposition on Anodic Aluminum Oxide (AAO) Rizkia, Vika; Susanto, Iwan; Belyamin; Garjati, Vina Nanda; Hapsari, Ade Utami; Raharjo, Jarot; Damisih; Pravitasari, Retna Deca
Jurnal Sains Materi Indonesia Vol. 27 No. 1 (2025): Jurnal Sains dan Materi Indonesia
Publisher : BRIN Publishing (Penerbit BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/jsmi.2025.9708

Abstract

Aluminum alloys suffer from deficiencies in surface performance due to insufficient resistance to corrosion and mechanical qualities in harsh environments. Therefore, it is crucial to apply a protective surface modification during the manufacturing process of the aluminum component. The electroless deposited Ni-P shows great potential as a protective coating due to its simple manufacturing process and outstanding performance. This study investigates the effect of oxalic acid concentration in the anodizing process on electroless Ni-P coating. In this study, Anodic Aluminum Oxide (AAO) is formed by an anodizing process on 0.3,0.5, and 0.7 oxalic acids prior to Ni-P electroless deposition. The resulting Ni-P layer has a nodular-like morphology with a size in the order of 0.5 m or less. Moreover, the AAO surface is covered by a thin and tightly formed layer of nickel particles. The EDX analysis shows the oxygen percentage falls by up to 70% after Ni deposition in all anodizing parameters, as compared to the anodized specimens alone. In addition, the nickel content gradually decreases as the concentration of oxalic acid increases from 0.3 M to 0.7 M.
The Calcination Temperature Effect on Crystal Structure of LiNi1/3Mn1/3Co1/3O2 Cathode Material for Lithium-Ion Batteries Rahayu, Sri; Saudi, Aghni Ulma; Tasomara, Riesma; Gumelar, Muhammad Dikdik; Utami, Wahyu Tri; Hapsari, Ade Utami; Raharjo, Jarot; Rifai, Abdulloh; Khaerudini, Deni Shidqi; Husin, Saddam; Saputra, Dita Adi; Yuliani, Hanif; Andrameda, Yurian Ariandi; Taqwatomo, Galih; Arjasa, Oka Pradipta; Damisih, Damisih; Hardiansyah, Andri; Pravitasari, Retna Deca; Agustanhakri, Agustanhakri; Budiman, Abdul Hamid
Journal of Batteries for Renewable Energy and Electric Vehicles Vol. 1 No. 02 (2023): NOVEMBER 2023
Publisher : NBRI Press

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.59046/jbrev.v1i02.22

Abstract

The lithium-ion battery has gained popularity among other secondary batteries for portable electronic devices and electric vehicle applications, especially the LiNi1/3Co1/3Mn1/3O2 or NMC111, considering its well-balanced configuration resulting in stable and safe electrochemical performance. NMC111 has been successfully prepared using a coprecipitation process at calcination temperatures from 800 to 950°C. The physical characteristics were investigated using X-Ray Diffraction (XRD), Scanning Electron Microscopy-Energy Dispersive Spectroscopy (SEM-EDS), and Particle Size Analysis (PSA). The XRD patterns showed the rhombohedral single phase for all calcination temperatures. Meanwhile, higher calcination temperatures offer higher degree of crystallinity, lower intensity ratio and more undesirable cation mixing. The particles with a uniform rectangle or pyramid shape are observed at the calcination temperature range from 800 to 900°C. However, bigger submicron particles with a rectangle or pyramid shape are detected at a higher temperature (950°C). The SEM-EDS mapping shows the homogeneity composition for all variation calcination temperatures. PSA analysis showed that calcination temperature at 800 and 850°C gives the particle less than 400 nm suggesting a potential material for a cathode of lithium-ion batteries.
Co-Authors Abdul Hamid Budiman Agustanhakri, Agustanhakri Andrameda, Yurian Ariandi Belyamin Damisih Damisih, Damisih Deni Shidqi Khaerudini Garjati, Vina Nanda Gumelar, Muhammad Dikdik Hardiansyah, Andri Husin, Saddam Iwan Susanto Jarot Raharjo Oka Pradipta Arjasa Pravitasari, Retna Deca Rifai, Abdulloh Saputra, Dita Adi Saudi, Aghni Ulma SRI RAHAYU Taqwatomo, Galih Tasomara, Riesma Vika Rizkia Wahyu Tri Utami Yuliani, Hanif