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All Journal SAINTIFIK@ : Jurnal Pendidikan MIPA Chemistry Indonesian Journal of Chemical Research Hydrogen: Jurnal Kependidikan Kimia Panrita Inovasi: Jurnal Pengabdian Kepada Masyarakat
Sumarna, Sabir
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Humanities Biochemistry, Genetics & Molecular Biology Chemistry Education Engineering Environmental Science Physics Public Health Social Sciences Other

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Journal : Chemistry Indonesian Journal of Chemical Research

 1 
Sintesis Turunan Amida N-4-O-Asetilferuloilmorfolina dari Asam Ferulat Melalui Metode Konversi Tidak Langsung Sumarna, Sabir; Firdaus, Firdaus; Soekamto, Nunuk H.
Indonesian Journal of Chemical Research Vol 4 No 1 (2016): Edisi Bulan Juli (Edition For July)
Publisher : Jurusan Kimia, Fakultas Sains dan Teknologi, Universitas Pattimura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30598/ijcr.2016.4-sab

Abstract

Synthesis of N-4-O-asetilferuloylmorpholine from ferulic acid via indirect conversion methods with acetylation, chlorination and amidation (in situ) reactions have been conducted. The acetylation was carried out using acetic anhydride reagent in pyridine solvent at room temperature for 6 hours. The chlorination was performed with thionyl chloride in benzene solvent by reflux at 75°C for 4 hours, proceeded by in situ amidation utilizing morpholine in the presence of triethylamine and pyridine using dichloromethane solvent at room temperature. The target molecule as white crystalline solids with m.p. of 91-92°C. Characterization of these compounds was committed by FTIR spectrophotometry.
Co-Authors Ahmad Muchsin Jayali Baturante, Nurjannah Bertha Mangallo Darma Santi Firdaus Firdaus Islam, Muh. Fajar Islam, Muhammad Fajar Jamius Bin Stepanus Khadijah Khadijah Markus Heryanto Langsa Merlin Merlin, Merlin Morin, Jacson Viktor Novitasari, Agnes Dyah Nunuk H. Soekamto Patiran, Abdul Zaid Santoso, Bimo Budi Sernita, Sernita Sirampun, Alfhons Daniel Somar, Evelina Stepanus, Jamius Bin Susilowati Susilowati Taher, Achmad