Renny Febrida
Laboratory Of Material Processing, Department Of Engineering Physics, Institute Of Technology Bandung, Bandung 40132, Jawa Barat

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Effect of 3-methacryloxypropyltrimethoxysilane on diametral tensile strength of rice husk silica-based dental composite Febrida, Renny; Wulanhapsari, Madeiva; Faza, Yanwar; Karlina, Elin; Cahyanto, Arief; Solihudin, Solihudin; Eddy, Diana Rakhmawati
Padjadjaran Journal of Dentistry Vol 34, No 2 (2022): July
Publisher : Faculty of Dentistry Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24198/pjd.vol34no2.41242

Abstract

ABSTRACTIntroduction: Rice husk silica has been studied as a filler in dental composite, however, the mechanical properties of the resulting composites are below the commercial due to the poor surface modification between silica and resin matrix. 3-methacryloxyprpyltrimethoxysilane (MPTS) is one of the coupling agents that are effective to modify the silica surface. The purpose of this study to analyze the effect of MPTS on the diametral tensile strength (DTS) of the self-made composite using rice husk silica.  Methods: The research type of this study was an experimental research laboratory. The samples (26 samples) were divided into two groups, namely the test group (using MPTS-modified silica) and the control group (using non-modified silica). The samples were cylindrical in shape with a diameter of 6.0 ± 0.1 mm and a height of 3.0 ± 0.1 mm according to ANSI/ADAS No. 27, 1993 and ISO 4049, 1988. The Fourier Transform Infrared (FTIR), HORIBA, was used to characterize the MPTS grafting on the silica surface. The DTS value is measured by Universal Testing Machine (UTM), Lloyd LRX Plus. Results: FTIR presents the additional peak of carboxyl and methacryloyl group at 1716, 1555, and 1410 cm-1 wavenumber, respectively in MPTS-modified silica. The DTS value of the test group was 43.40 ± 4.43 MPa and the control group was 25.80 ± 2.63 MPa. The test group was significantly higher than the control group (p-value = 0.001). Conclusion: The MPTS is effective to enhance the DTS value of rice husk silica-based composite.Keywords: Rice husk silica; dental composite; diametral tensile strength; 3-methacryloxypropyltrimethoxysilane.
Preparation of micro-calcite powder using fine-bubble assisted carbonation as toothpaste material Febrida, Renny; Nabillah Salma, Dinda Jihan; Azzahra, Fauziah; Karlina, Elin; Andiesta, Niekla Survia; Faza, Yanwar
Padjadjaran Journal of Dentistry Vol 35, No 1 (2023): March 2023
Publisher : Faculty of Dentistry Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24198/pjd.vol35no1.44519

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ABSTRACTIntroduction: Calcite (CaCO3) is typically used in commercial toothpaste with particle size ranges from 1-12 μm. In the latest study, calcite was synthesized by using Ca(OH)2 precursor from natural resources However, the resulting particle size does not match the size of the toothpaste filler. This study aims to prepare micro-calcite via fine-bubble assisted carbonation as toothpaste material. Methods: The calcite powder was prepared from Ca(OH)2 analytical grade powder utilizing the fine-bubble carbonation process with the Ca(OH)2 concentration and initial pH variation. The study was started by making a Ca(OH)2 suspension with a concentration of 0.25, 0.5, 0.75, 1 and 1.25 M using 2.000 ml methanol as a solvent. 0.5 M NaH2PO4 solutions were utilized to adjust the initial pH of 0.5 M Ca(OH)2 suspension into 8, 9, and 10. The suspensions were aerated using CO2 fine-bubble for two hours to produce CaCO3 samples. All precipitated CaCO3 particles were characterized by PSA, Zeta-Potential, and FTIR measurements. Results: The calcite phase was identified from the FTIR transmittance. Aragonite or vaterite phase was not observed in the samples. PSA result shows the size of CaCO3 particles from samples 0.25 M to 1.25 M are as follows 3.03, 3.23, 2.79, 3.70, 0.99 μm respectively. Meanwhile, the particle sizes of CaCO3 in samples with a pH of 8, 9 and 10 are 3.00, 2.03 and 2.50 μm respectively. The zeta potential shows the value ranges from -23.2 mV to -11.9 mV, indicating fair dispersion ability. Conclusion: The fine bubble assisted carbonation method in this study helps in producing calcite in micron size that could be used as alternative fillers for toothpaste.Keywords: calcite, fine-bubble, carbonation, particle size, toothpaste
The effect of ZrCl4, Al(NO3)3 and Na2SiO3 precursors concentration on particle size as dental composites filler through spray pyrolysis method Karlina, Elin; Idznihaq, Khairina; Febrida, Renny; Andiesta, Niekla Survia
Padjadjaran Journal of Dentistry Vol 35, No 1 (2023): March 2023
Publisher : Faculty of Dentistry Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24198/pjd.vol35no1.44518

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ABSTRACTIntroduction: one of the important components in dental composites is a filler which can be made through various methods, including spray pyrolysis. In the spray pyrolysis method, some factors determine the size and morphology of the resulting filler particles, one of which is the concentration of precursors. This study aimed to analyze the effect of precursor concentration on the particle size produced using the spray pyrolysis method. Methods: in this experimental laboratory study, zirconia-alumina-silica particles were synthesized using the spray pyrolysis method. The precursor solution consisted of ZrCl4, Al (NO3)3, and Na2SiO3 with a concentration variation of (0.1; 0.2; and 0.3) M. The furnace temperature was set at 750°C, and the electric precipitator temperature was 100°C with a feed rate of 3L/min. Then, the tests performed were using PSA (Particle Size Analyzer), and XRF (X-Ray Fluorescence). Results: The results showed that the best zirconia alumina silica filler particle with the smallest size is the result with a concentration of 0.1 M and its size was 618.6 nm. The particle size for 0.2 M was 911.9 nm and 1799.4 nm for 0.3 M.  According to XRF test results the zirconia alumina silica filler system contains all the precursor elements. Conclusions: The effect of precursor concentration on the particle size produced using the spray pyrolysis method showed that the smaller the precursor concentration used, the smaller the particle size produced. The best results from synthesizing a filler system with a concentration of 0.1 M precursor solution. All the results are in submicron and micron size, and could be used as the component of dental composites.Keywords: precursors concentration, particle size, spray pyrolysis, dental composites filler
Effect of mixed water and methanol solvents ratio on the CaCO3 characteristics via fine bubble diffuser as a dental biomaterial Febrida, Renny; Ramadhan, Muhammad Farhan; Karlina, Elin; Andiesta, Niekla Survia
Padjadjaran Journal of Dental Researchers and Students Vol 7, No 1 (2023): Februari 2023
Publisher : Fakultas Kedokteran Gigi Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24198/pjdrs.v7i1.40418

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ABSTRACTIntroduction: The application of calcium carbonate in dental biomaterial depends on the charcateristics after the synthesis process. This study aims to determine the effect of the ratio of methanol and water on the characteristics of the CaCo3 produced through the fine bubble diffuser method. Methods: Synthesis of calcium carbonate by CO2 carbonation method using fine bubble diffuser to produce fine CO2 bubbles (bubble size range 100-500 nm). The Ca(OH)2 precursor was dissolved in various ratios of water and methanol mixtures, namely: 25% water 75% methanol, 20% water 80% methanol, 15% water 85% methanol, 10% water 90% methanol, 5% water 95% methanol, and 100% methanol. The suspension was carbonated using CO2 fine bubbles for 2 hours to produce CaCO3 powder. The resulting calcium carbonate powder was tested with FTIR (Fourier Transform Infra Red), PSA (Particle Size Analyzer), and Zeta-Potential. Results: The FTIR test obtained the wave numbers of calcite (712 cm-1), vaterite (744, 873, 874, and 875 cm-1) and aragonite (848, 849, and 854 cm-1) phases in the six variations of the solvent used. The PSA test showed that the particle size produced was submicron with the smallest size being 191.1 nm and the largest being 576.2 nm. The ZetaPotential test showed that the particles were relatively stable in solution with a Zeta-Potential value range of -15.1 mV to -20.8 mV and particles with moderate stability -21.2 mV to -25.1 mV. Conclusion: The addition of the organic solvent methanol to water increases the solubility of CaOH and increases the formation of the vaterite phase. Increasing the amount of water decreases the amount of vaterite phase, increasing the particle size and zeta potential value. but the addition of 15% water decreases the particle size of CaCO3 KEY WORDSCaCO3, fine bubble diffuser, FTIR, PSA, zeta potential Pengaruh perbandingan campuran pelarut air dan metanol terhadap karakteristik CaCO3 melalui metode fine bubble diffuser sebagai biomaterial kedokteran gigiABSTRAKPendahuluan: Kalsium karbonat (CaCO3) merupakan salah satu sumber kalsium yang umum digunakan di bidang biomaterial kedokteran gigi. Aplikasi kalsium karbonat tergantung dari fasa dan ukuran partikelnya. Penelitian ini bertujuan untuk mengetahui pengaruh perbandingan metanol dan air terhadap karakteristik CaCO3 yang dihasilkan melalui metode fine bubble diffuser. Metode: Prekursor Ca(OH)2 dilarutkan dengan berbagai variasi campuran pelarut air dan metanol, yaitu: 25% air 75% metanol, 20% air 80% metanol, 15% air 85% metanol, 10% air 90% metanol, 5% air 95% metanol, dan 100% metanol. Suspensi Ca(OH)2 dikarbonasi menggunakan gelembung halus CO2 selama 2 jam untuk menghasilkan bubuk CaCO3. Bubuk CaCO3 yang dihasilkan diuji dengan FTIR (Fourier Transform Infra Red), PSA (Particle Size Analyzer), dan ZetaPotential. Hasil: Uji FTIR didapatkan bilangan gelombang fasa kalsit (712 cm-1 ), vaterit (744, 873, 874, dan 875 cm-1 ) dan aragonit (848, 849, dan 854 cm-1 ) pada keenam variasi pelarut yang digunakan. Uji PSA didapatkan ukuran partikel terkecil 191,1 nm dan terbesar 576,2 nm. Partikel relatif stabil dalam larutan berdasarkan Uji Zeta-Potential (-15,1 mV sampai -17,8 mV) dan stabilitas moderat (-20,8 mV sampai -25,1 mV). Simpulan: Penambahan pelarut organik methanol pada pelarut air meningkatkan kelarutan CaOH dan meningkatkan pembentukan fasa vaterite. peningkatan jumlah air menurunkan jumlah fasa vaterite, meningkatkan ukuran partikel dan nilai zeta potensial. namun pada penambahan 15% air dan seterusnya menurunkan ukuran partikel CaCO3. KATA KUNCI CaCO3, fine bubble diffuser, FTIR, PSA, zeta potential
Comparison of bond strength between self-adhered and conventional composites Putra, Adria Permana; Karlina, Elin; Febrida, Renny
Padjadjaran Journal of Dentistry Vol 22, No 3 (2010): November 2010
Publisher : Faculty of Dentistry Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (132.68 KB) | DOI: 10.24198/pjd.vol22no3.15805

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Bond strength towards dentine is a critical factor for composite restoration success. The purpose of this research was to obtain data on self-adhered composite bond strength to tooth dentine. This research was an experimental laboratory research that used 10 third molar teeth as samples. The teeth were prepared by thinning its mesial part until it reaches dentine layer. The sample was divided into two groups, each consisting of 5 teeth. In group I was applied self-adhered composite with Fusio® Liquid Dentine brand, whereas group II was applied conventional composite with Ivoclar Te-Econom Flow®. The applied composite had a cylindrical shape with 6 mm diameter. The sample was then placed on the test arm. The shear bond strength test method then conducted on Universal Testing Machine (UTM). Obtained data was tested using Two-tails Independent t-Test (α = 0,05). The results showed the average of self-adhered composite bond strength to dentine is 1,8878 ± 0,2859 MPa and conventional composite for 4,43552 ± 0,49472 MPa. The data showed that the self-adhered composite bond strength to dentine is smaller than conventional composite. From this research can be concluded that there was bond strength difference between the self-adhered composite with conventional composites towards the tooth dentine.
Comparison of nanocomposite colour particle stability after immersion in black tea and green tea Pramudiyanti, Nindya; Febrida, Renny; Usri, Kosterman
Padjadjaran Journal of Dentistry Vol 27, No 1 (2015): March 2015
Publisher : Faculty of Dentistry Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24198/pjd.vol27no1.26687

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Introduction: Restorations using composite resins have to meet several requirements, one of which is stable against discoloration. Unfortunately discoloration may happen to this kind of restoration, and one of the causes is the tea habit. This research was to compare the color stability of nano particle composite after soaked in black tea and green tea. Methods: The research method was a laboratory experiment using nano particle composite as samples. It was conducted to 15 samples in cylindrical shape with diameter of 7 mm and thickness of 2 mm. Samples were divided in to 3 groups, each group consists of 5 samples. The first group soaked in black tea, the second group soaked in green tea and the last one soaked in mineral water for 7 days. Color measurements were obtained by using spectrophotometer (CIE lab system) and color differences (∆E) were estimated. For statistical evaluation, analysis of variance (ANOVA) was used with 5% error level. Results: There are differences in color stability of nano composite after soaked in black tea and green tea. The value of color differences after soaked in black tea is 2,669 and green tea is 3,062. Conclusion: The stability of nano particle composite color is better at soaking with black tea compared with immersion with green tea.
Influence of alcohol-containing mouthwash and alcohol-free mouthwash towards the hybrid composite restoration materials surface hardness Munawar, Adlina Hasna; Febrida, Renny; Nurdin, Denny
Padjadjaran Journal of Dentistry Vol 25, No 3 (2013): November 2013
Publisher : Faculty of Dentistry Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (204.685 KB) | DOI: 10.24198/pjd.vol25no3.15574

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Mouthwash is widely used by the community to maintain oral health. Beside the benefit provided, both alcohol-containing mouthwash and alcohol-free mouthwash have negative effects on the composite resin restorative materials, which can affect the surface hardness. One of composite types is hybrid type which is superior in physical and mechanical properties as a restorative material. The aim of this study was to determined the effect of alcohol-containing mouthwash and alcohol-free mouthwash towards the surface hardness of hybrid composite restorative material. This study used 15 disc-shaped specimens of hybrid composite with the size of 6 mm diameter and 4 mm thickness and divided into three treatment groups immersion, in the alcohol-containing mouthwash (A), alcohol-free mouthwash (B), and artificial saliva (C) as control for 12 hours, which surface hardness was further tested using Vickers hardness test. The mean of hardness values of group: A 24.9 VHN; B: 27.2 VHN; and C: 28.4 VHN. The results of statistical tests One-Way ANOVA showed there were significant differences in the hardness values among the three treatment groups (p<0,05). From this study concluded that both alcohol-containing mouthwash and alcohol-free mouthwash were decreasing the surface hardness of hybrid composite restorative material.
Setting time evaluation of injectable carbonate apatite cement using various sodium carboxymethylcellulose (Na CMC) concentration Cahyanto, Arief; Permatasari, Indah; Febrida, Renny
Padjadjaran Journal of Dentistry Vol 30, No 2 (2018): July 2018
Publisher : Faculty of Dentistry Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (183.605 KB) | DOI: 10.24198/pjd.vol30no2.18321

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Introduction: The injectable calcium phosphate cement has the advantage to be used in the bone defect with the limited access which supports a minimally invasive surgical technique. These Injectability properties of calcium phosphate cement can be modified by adding a sodium carboxymethylcellulose (Na CMC). The aim of this present study is to investigate the setting time of injectable bone cement based on CO3Ap using various Na CMC concentration. Methods: Vaterite (a polymorph of CaCO3) and Dicalcium Phosphate Anhydrous (DCPA) as powder phase mixed with 0.2 mol/L Na2HPO4 solution containing 1% polyethylene glycol (PEG) and various concentration of Na CMC as followed 0.5%, 1%, 1.5%, and 2%, respectively. Each concentration groups was consisting of 5 samples from total 20 samples. Powder and liquid phase was mixed with a spatula at a liquid to powder (L/P) ratio of 0.4. The setting time of CO3Ap cement was evaluated according to the modification method standardized by ISO 1566 for dental zinc phosphate cement using a custom fabricated Vicat needle apparatus. The cement was maintained at 37ºC and 100% relative humidity as a standard requirement. Results: The mean value of setting time cement was as followed 0.5% Na CMC 35:06 minutes, 1% Na CMC 38:48 minutes, 1.5% Na CMC 40:06 minutes, and 2% Na CMC 41:30 minutes. The result is statistically significant (p<0.05) with the group of 0.5% Na CMC compared to others group. Conclusion: Increasing the concentration of Na CMC could prolong the setting time of CO3Ap cement.
Comparison of brittleness and flowability between Cipetir Gutta-Percha and commercial Gutta-Percha Usri, Kosterman; Faza, Yanwar; Sanjaya, Arya; Viona, Nona; Djustiana, Nina; Karlina, Elin; Febrida, Renny; Cahyanto, Arief
Padjadjaran Journal of Dentistry Vol 34, No 1 (2022): March
Publisher : Faculty of Dentistry Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24198/pjd.vol34no1.38869

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Introduction: Gutta-Percha (GP) is a standard endodontic filling material found in pure form in the Cipetir area, Indonesia. However, a study comparing physical properties (brittleness and flowability) between pure GP and commercially used GP has not been found. Therefore, this study aims to test the brittleness and flowability of Cipetir GP compared to commercial GP. Methods: This study was quasi-experimental. Forty samples were prepared for each material and test, according to ANSI/ADA specification-GP cones-no 78 in 2006. The first step began by making a sample of Cipetir GP using moulds from a cuvette, commercial GP (Inline #80), and gypsum stone. The second step was to test the brittleness (Crease Recovery Tester) and flowability (according to ADA No. 78 of 2000) of Cipetir GP and commercial GP. Results: The brittleness test of Cipetir GP showed unbroken samples, and the commercial GP showed four broken samples. The Fisher's Exact test showed a p-value of 0.087, which means there was no significant difference in brittleness between Cipetir GP and commercial GP. At the same time, the average value of flowability of Cipetir GP and commercial GP were 6.46 mm and 0.19 mm, respectively. The unpaired t-test showed a p-value<0.05, which means there was a significant difference in the flowability between Cipetir GP and commercial GP. Conclusions: There is a brittleness similarity between Cipetir GP and commercial GP, while the flowability value of Cipetir GP is higher than commercial GP. Those initial findings showed that the Cipetir GP might become an excellent candidate to be an alternative endodontic filling.
PENDEKATAN BIOMIMETIK PADA BIDANG KEDOKTERAN GIGI: TINJAUAN PUSTAKA Gempita, Gema; Febrida, Renny
PREPOTIF : JURNAL KESEHATAN MASYARAKAT Vol. 9 No. 2 (2025): AGUSTUS 2025
Publisher : Universitas Pahlawan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31004/prepotif.v9i2.47522

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Tinjauan pustaka ini membahas pendekatan biomimetik dalam bidang kedokteran gigi yang bertujuan untuk meniru dan menggantikan struktur alami pada area kraniofasial. Penelitian yang intensif selama beberapa dekade telah menghasilkan pengembangan biomaterial dan teknik inovatif untuk mendukung proses tersebut. Temuan menunjukkan bahwa material berbasis alami atau yang menyerupai struktur biologis memiliki hasil klinis yang lebih baik dan potensi lebih tinggi untuk aplikasi klinis. Oleh karena itu, pengembangan biomaterial biomimetik memerlukan pendekatan interdisipliner yang melibatkan kedokteran, bioteknologi, dan ilmu komputasi. Di masa depan, pengembangan jaringan gigi yang sepenuhnya diregenerasi, seperti enamel, dentin, pulpa, dan sementum, dengan karakteristik nanostruktur yang menyerupai jaringan gigi alami, menjadi salah satu harapan utama dalam kemajuan bidang ini.