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All Journal Reaktor International Journal of Renewable Energy Development TEKNIK METANA JURNAL KIMIA SAINS DAN APLIKASI JURNAL TEKNOLOGI KIMIA DAN INDUSTRI Prosiding Seminar Nasional Sains Dan Teknologi Fakultas Teknik Jurnal Kimia dan Kemasan Majalah Ilmiah MOMENTUM ALCHEMY Jurnal Penelitian Kimia Indonesian Journal of Chemistry Jurnal Inovasi Teknik Kimia Jurnal Pasopati : Pengabdian Masyarakat dan Inovasi Pengembangan Teknologi Jurnal Teknik Kimia Indonesia Jurnal Kimia dan Kemasan Jurnal Pengabdian Vokasi Jurnal Profesi Insinyur Indonesia International Journal of Renewable Energy Development Bulletin of Chemical Reaction Engineering & Catalysis
Aprilina Purbasari
Departemen Teknik Kimia, Fakultas Teknik, Universitas Diponegoro
Aerospace Engineering Agriculture, Biological Sciences & Forestry Automotive Engineering Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Civil Engineering, Building, Construction & Architecture Computer Science & IT Control & Systems Engineering Earth & Planetary Sciences Education Electrical & Electronics Engineering Energy Engineering Environmental Science Industrial & Manufacturing Engineering Languange, Linguistic, Communication & Media Law, Crime, Criminology & Criminal Justice Materials Science & Nanotechnology Transportation

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Journal : Bulletin of Chemical Reaction Engineering

 1 
Preparation and Characterization of Zeolite Membrane for Bioethanol Purification Aprilina Purbasari; Titik Istirokhatun; Ariestya Meta Devi; Lulluil Mahsunnah; Heru Susanto
Bulletin of Chemical Reaction Engineering & Catalysis 2013: BCREC Volume 8 Issue 1 Year 2013 (June 2013)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.8.1.4062.47-53

Abstract

The use of bioethanol as an alternative fuel with a purity of more than 99.5% wt has prompted research on bioethanol purification. One of the promising methods used for bioethanol purification is pervaporation membrane. This research is aimed to prepare and characterize zeolite membranes for pervaporation membrane. The membrane preparation consisted of two stages, namely support preparation and zeolite deposition on the support. In support preparation, α- alumina and kaolin with specific composition (50:30; 40:40; 50:30) was mixed with additives and water. After pugging and aging process, the mixture became paste and extruded into tubular shape. The tube was then calcined at temperature of 1250 °C for 3 hours. After that, zeolite 4A was deposited on the tubes using clear solution made of 10 %wt zeolite and 90 %wt water and heated at temperature of 80 °C for 3 hours. Furthermore, the resulting zeolite membranes was washed with deionized water for 5 minutes and dried in oven at temperature of 100 °C for 24 hours. Characterization of zeolite membranes included mechanical strength test, XRD, and SEM. In the mechanical strength test, the membrane sample with α- alumina:kaolin = 50:30 (membrane A) has the highest mechanical strength of 46.65 N/mm2. Result of XRD analysis for the membrane A indicated that mullite and corundum phases were formed, which mullite phase was more dominant. Meanwhile the result of SEM analysis shows that zeolite crystals have been formed and covered the pores support, but the deposition of zeolite has not been optimal yet. The performance examination for bioethanol purification showed that the membrane could increase the purity of bioethanol from 95% to 98.5% wt. © 2013 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0)
Co-Authors . Suherman Afiatin Afiatin Afri Yenni Agnesia Permatasari Alice Pramashinta Andri Cahyo Kumoro Anissa Ardanti Wulandari Ariestya Meta Devi Arif Fajar Utomo Aulia Beta Safira Ayyubi, Shalahudin Nur Budi Ismadi Budiyono Budiyono Darmaji, Timothius Adrian Christantyo Dessy Ariyanti Dessy Ariyanti Didi Dwi Anggoro Ekky Febri Ariani Erwan Adi Saputro Faleh Setia Budi Fikri Mudzakir Marasabessy Hafsah Fajrin Aprilianti Hamzah, Fazlena Hapsari, Farida Diyah Hargono Hargono Heny Kusumayanti Heny Kusumayanti Herry Santosa Heru Susanto Kristinah Haryani Laeli Kurniasari Lesdantina, Dina Lukman Atmaja Lulluil Mahsunnah Luqman Buchori M. Djaeni Machmud Lutfi H Margaretha Praba Aulia Mira Amalia Hapsari Muhammad Adi Irawan Muslim, Aristianto Nita Aryanti Nita Aryanti Noer Abyor Handayani Noer Abyor Handayani Nungki Primastuti Pratama, Pambudi Pajar Pratiwi, Wahyu Zuli Purwanto Purwanto Purwanto Purwanto Pury Diana Shintawati Raizka Kharisma Mediani Ratnawati Ratnawati Restu Kusumawardani Rini Kusumawati Samadhi, T Walmiki Saputra, Erwan Adi Sary, Cindy Nella Setia Budi Sasongko Shalahudin Nur Ayyubi Silviana Silviana Silviana Silviana Siswo Sumardiono Slamet Priyanto Sri Rukiyawati Suherman Suherman Titik Istirokhatun Tjokorde Walmiki Samadhi Tjokorde Walmiki Samadhi Tjokorde Walmiki Samadhi Tkokorde Walmiki Samadhi Tutuk Djoko Kusworo Vitus Dwi Yunianto Vitus Dwi Yunianto Budi Ismadi Wei Gao Wisnu Jati N Wulandari Dharsono Y. Saptiana Oktari Yazid Bindar Yazid Bindar Yustina Linasari