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All Journal Reaktor International Journal of Science and Engineering (IJSE) International Journal of Renewable Energy Development TEKNIK METANA Jurnal Ilmu Lingkungan JURNAL TEKNOLOGI KIMIA DAN INDUSTRI IPTEK The Journal for Technology and Science Prosiding Seminar Nasional Sains Dan Teknologi Fakultas Teknik Seminar Nasional Teknik Kimia Kejuangan Journal of Engineering and Technological Sciences Majalah Ilmiah MOMENTUM Science and Technology Indonesia Indonesia Journal of Halal Abdimas UNWAHAS : Jurnal Pengabdian Masyarakat UNWAHAS Jurnal Profesi Insinyur Indonesia Bulletin of Chemical Reaction Engineering & Catalysis
Luqman Buchori
Departemen Teknik Kimia, Fakultas Teknik, Universitas Diponegoro Jl Prof Sudharto, SH, Tembalang, Semarang, 50275, Telp/fax: (024)7460058
Religion Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Civil Engineering, Building, Construction & Architecture Computer Science & IT Control & Systems Engineering Economics, Econometrics & Finance Education Electrical & Electronics Engineering Energy Engineering Environmental Science Industrial & Manufacturing Engineering Materials Science & Nanotechnology Medicine & Pharmacology Physics Social Sciences Transportation

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Utilizing Shear Factor Model and Adding Viscosity Term in Improving a Two-Dimensional Model of Fluid Flow in Non Uniform Porous Media Bindar, Yazid; Makertihartha, IGBN; Supardan, M. Dani; Buchori, Luqman
Journal of Engineering and Technological Sciences Vol 39, No 2 (2007)
Publisher : ITB Journal Publisher, LPPM ITB

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (436.337 KB) | DOI: 10.5614/itbj.eng.sci.2007.39.2.3

Abstract

In a packed bed catalytic reactor, the fluid flow phenomena are very complicated because the fluid and solid particle interactions dissipate the energy. The governing equations  were developed in the  forms of  specific  models. The shear factor  model was introduced in the momentum equation for covering the effect  of  flow  and  solid  interactions  in  porous  media.   A  two  dimensional numerical  solution  for  this  kind  of  flow  has  been  constructed  using  the  finite volume  method.  The  porous  media  porosity  was  treated  as  non-uniform distribution  in  the  radial  direction.  Experimentally,  the  axial  velocity  profiles produce  the  trend  of  having  global  maximum  and  minimum  peaks  at  distance very close to the wall. This trend is also accurately picked up by the numerical result. A more comprehensive shear factor formulation results a better velocity prediction than other correlations do. Our derivation on the presence of porous media leads to an additional viscosity term. The effect of this additional viscosity term was investigated numerically. It is found that the additional viscosity term improves  the  velocity  prediction  for  the  case  of  higher  ratio  between  tube  and particle diameters
OPTIMASI PROSES POLIMERISASI CNSL DENGAN FORMALDEHID UNTUK APLIKASI COATING FURNITURE Budi, Faleh Setia; Buchori, Luqman
Jurnal Ilmu Lingkungan Vol 11, No 1 (2013): April 2013
Publisher : School of Postgraduate Studies, Diponegoro Univer

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (389.456 KB) | DOI: 10.14710/jil.11.1.10-15

Abstract

PENGAMBILAN MINYAK KEDELAI DARI AMPAS TAHU SEBAGAI BAHAN BAKU PEMBUATAN BIODIESEL Buchori, Luqman; Sasongko, Setia Budi; Anggoro, Didi Dwi; Aryanti, Nita
Jurnal Ilmu Lingkungan Vol 10, No 2 (2012): Oktober 2012
Publisher : School of Postgraduate Studies, Diponegoro Univer

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (764.317 KB) | DOI: 10.14710/jil.10.2.49-53

Abstract

ABSTRAK Kedelai adalah komoditi terbesar setelah padi di Indonesia. Kebutuhannya mencapai 2,3 juta ton per tahun. Dari jumlah tersebut 50% dikonsumsi berupa tempe, 40% berupa tahu, dan 10% berupa minyak kedelai. Dari produksi tahu, dihasilkan limbah ampas tahu. Dalam penelitian ini, lemak pada ampas tahu diekstraksi untuk mendapatkan minyak kedelai yang dijadikan bahan baku biodiesel. Hasil ekstraksi kemudian dianalisa untuk dibandingkan dengan standar bahan baku biodiesel. Penelitian ini bertujuan untuk menghitung berat lemak yang terekstrak dari ampas tahu terhadap lama waktu ekstraksi dan jenis solven yang digunakan, serta mengetahui komposisi minyak ampas tahu tersebut. Hasil penelitian menunjukan bahwa waktu ekstraksi dan jenis solven mempengaruhi jumlah lemak yang dapat terekstrak. Benzene merupakan solven yang dapat mengekstrak minyak lebih baik daripada solven toluene dan n-heksane. Solven benzene memiliki waktu optimum lima jam untuk mengekstrak lemak yang terdapat di dalam ampas tahu. Dari hasil analisa, diketahui bahwa kadar FFA minyak kedelai yang menggunakan solven benzene sebesar 4,8%, lebih kecil daripada menggunakan solven toluene (5,4%) dan n-heksan (5,8%). Sedangkan bilangan penyabunan diperoleh 184,22 mgKOH/gr untuk benzene, 193,55 mgKOH/gr untuk toluene dan 184,22 mgKOH/gr untuk n-heksan. Kandungan posfor yang didapat sebesar 0,19 untuk benzene, 0,23 untuk toluene dan 0,12% untuk n-heksan. Nilai ini masih dalam kategori besar sehingga harus melewati pretreatment terlebih dahulu sebelum melewati proses transesterifikasi menjadi biodiesel. Kata Kunci: ampas tahu; biodiesel; kedelai; minyak kedelai; transesterifikasi ABSTRACT Soybeans are the largest commodity after rice in Indonesia. Needs to reach 2.3 million tons per year. Of this amount 50% is consumed in the form of tempeh, 40% in the form of knowing, and 10% of soybean oil. From tofu production, tofu waste generated. In this study, fat on tofu extracted for soybean oil used as biodiesel feedstock. The results are then analyzed for compared to standard biodiesel feedstock. This study aimed to calculate the weight of fat extracted from the tofu waste to extraction time and the type of solvent and determines the composition of the oil tofu. The results showed that the extraction time and the type of solvent affects the amount of fat that can be extracted. Benzene is a solvent that can extract oil better than the solvents toluene and n-hexane. Benzene had five hours optimum to extract the fat in the tofu. From the analysis, it is known that the FFA content of soybean oil using benzene was 4.8%, smaller than toluene (5.4%) and n-heksane (5.8%). While these numbers obtained by saponification 184.22 mgKOH/gr for benzene, 193.55 mgKOH/gr for toluene and 184.22 mgKOH/gr for n-heksane. The content of phosphorus of 0.19 for benzene, 0.23 for toluene and 0.12% for n-heksane. This value is still in the major categories that must be passed before pretreatment process trough transesterification into biodiesel. Keywords: tofu waste; biodiesel; soybean; soybean oil; transesterification
PEMBUATAN BIODIESEL DARI MINYAK GORENG BEKAS DENGAN PROSES CATALYTIC CRACKING Buchori, Luqman; Widayat, Widayat
TEKNIK Volume 28, Nomor 2, Tahun 2007
Publisher : Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (395.817 KB) | DOI: 10.14710/teknik.v28i2.2116

Abstract

Crude oil is a source of energy which is not be renewable. This fact motivates so much countries ineconomizing on fuel. Many researches have been done to gets another fuel substitute the crude oil.Biodiesel is represented as fuel instead of diesel fuel, and it is produced from vegetable oil. In the otherside, ex-cooking oil is waste-product from food industry, restaurant and household which is potential tobe alternative fuels because of the high contents of carbon and hydrogen atoms. Commonly the biodieselmade from vegetable oil by esterification and transesterification process. But if using esterification andtransesterification process to ex-cooking oil material, it is not economically feasible because the processmakes another reaction between alkaly catalist and oil to produce soap. One of biodiesel process iscatalytic cracking of the ex-cooking oil. This research is aimed to analyze zeolite catalist size effect(0.125mm; 0.3375mm; 0.425mm; 0.85mm; 1.18mm), and acid concentration on the product (2N; 3N;4N). This result shows that at 4N acid concentration and 0.125 mm zeolite catalist size is optimal whichcan reach diesel specification.
Sintesa Metil Ester Sulfonat dari Minyak Jarak Pagar (Jathropa Curcas Oil) dan Aplikasinya pada Proses Enhanced Oil Recovery (EOR) Nugroho, Amin; Buchori, Luqman
METANA Vol 15, No 1 (2019): Juni 2019
Publisher : Universitas Diponegoro

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (1009.911 KB) | DOI: 10.14710/metana.v15i1.22666

Abstract

Konsumsi minyak bumi mengalami peningkatan dari tahun ke tahun, sementara produksinya cenderung mengalami penurunan. Produksi minyak bumi dapat ditingkatkan dengan oil recovery. Sejak tahun 1980, teknik Enhanced Oil Recovery (EOR) dengan menggunakan surfaktan sebagai penginjeksi (surfactant flooding) merupakan salah satu teknik yang paling berhasil untuk meningkatkan produksi minyak. Surfaktan dapat dibuat dari bahan alami, salah satunya dari minyak jarak pagar. Tujuan dari percobaan ini adalah untuk mengkaji pengaruh waktu reaksi dan pengaruh penambahan metanol terhadap metil ester sulfonat (MES, surfaktan) yang dihasilkan dalam operasi sulfonasi. Surfaktan yang diperoleh kemudian diaplikasikan dalam proses EOR. Proses pembuatan MES dari minyak biji jarak dilakukan melalui 2 tahapan yaitu proses esterfikasi dan transesterifikasi dengan katalis batu dolomite. Metil ester (ME) yang diperoleh kemudian disulfonasi untuk mendapatkan MES. Konsentrasi surfaktan anionik dalam produk dianalisa dengan spektrofotometer. Hasil penelitian menunjukkan bahwa MES yang memiliki kandungan surfaktan anionik paling tinggi diperoleh pada waktu reaksi 90 menit dan penambahan metanol dengan konsentrasi 40%wt yaitu sebesar 55,464 mg/L. Uji kompatibilitas didapatkan larutan berwarna keruh (koloid), sedangkan tegangan antarmukanya sebesar 17,71 dyne/cm dan tegangan antarmuka pada suhu 80oC adalah 26,57 dyne/cm. Petroleum consumption has increased from year to year, while production tends to decline. Petroleum production can be increased by oil recovery. Since 1980, the Enhanced Oil Recovery (EOR) technique using surfactants as injectors (surfactant flooding) is one of the most successful techniques for increasing oil production. Surfactants can be made from natural ingredients, one of them from jatropha oil. The purpose of this experiment was to examine the effect of reaction time and the effect of adding methanol to methyl ester sulfonate (MES, surfactant) produced in sulfonation operations. The surfactants obtained are then applied in the EOR process. The process of MES production from castor oil is carried out through 2 stages, namely esterfication and transesterification with dolomite catalyst. Methyl esters (ME) were obtained then sulfonated to obtain MES. The concentration of anionic surfactants in the product was analyzed by a spectrophotometer. The results showed that the MES which had the highest anionic surfactant content was obtained at the reaction time of 90 minutes and the addition of methanol with a concentration of 40% wt was 55.464 mg/L. Compatibility test obtained colloidal colored solution (colloid), while surface tension was 17.71 dyne/cm and surface tension at 80oC was 26.57 dyne/cm.
Effect of Temperature on Plasma-Assisted Catalytic Cracking of Palm Oil into Biofuels Istadi, I.; Riyanto, Teguh; Buchori, Luqman; Anggoro, Didi Dwi; Saputra, Roni Ade; Muhamad, Theobroma Guntur
International Journal of Renewable Energy Development Vol 9, No 1 (2020): February 2020
Publisher : Center of Biomass & Renewable Energy, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.14710/ijred.9.1.107-112

Abstract

Plasma-assisted catalytic cracking is an attractive method for producing biofuels from vegetable oil. This paper studied the effect of reactor temperature on the performance of plasma-assisted catalytic cracking of palm oil into biofuels. The cracking process was conducted in a Dielectric Barrier Discharge (DBD)-type plasma reactor with the presence of spent RFCC catalyst. The reactor temperature was varied at 400, 450, and 500 ºC. The liquid fuel product was analyzed using a gas chromatography-mass spectrometry (GC-MS) to determine the compositions. Result showed that the presenceof plasma and catalytic role can enhance the reactor performance so that the selectivity of the short-chain hydrocarbon produced increases. The selectivity of gasoline, kerosene, and diesel range fuels over the plasma-catalytic reactor were 16.43%, 52.74% and 21.25%, respectively, while the selectivity of gasoline, kerosene and diesel range fuels over a conventional fixed bed reactor was 12.07%, 39.07%, and 45.11%, respectively. The increasing reactor temperature led to enhanced catalytic role of cracking reaction,particularly directing the reaction to the shorter hydrocarbon range. The reactor temperature dependence on the liquid product components distribution over the plasma-catalytic reactor was also studied. The aromatic and oxygenated compounds increased with the reactor temperature.©2020. CBIORE-IJRED. All rights reserved
Biofuels Production from Catalytic Cracking of Palm Oil Using Modified HY Zeolite Catalysts over A Continuous Fixed Bed Catalytic Reactor Istadi, I.; Riyanto, Teguh; Buchori, Luqman; Anggoro, Didi D.; Pakpahan, Andre W. S.; Pakpahan, Agnes J.
International Journal of Renewable Energy Development Vol 10, No 1 (2021): February 2021
Publisher : Center of Biomass & Renewable Energy, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.14710/ijred.2021.33281

Abstract

The increase in energy demand led to the challenging of alternative fuel development. Biofuels from palm oil through catalytic cracking appear as a promising alternative fuel. In this study, biofuel was produced from palm oil through catalytic cracking using the modified HY zeolite catalysts. The Ni and Co metals were impregnated on the HY catalyst through the wet-impregnation method. The catalysts were characterized using X-ray fluorescence, X-ray diffraction, Brunauer–Emmett–Teller (BET), Pyridine-probed Fourier-transform infrared (FTIR) spectroscopy, and Scanning Electron Microscopy (SEM) methods. The biofuels product obtained was analyzed using a gas chromatography-mass spectrometry (GC-MS) method to determine its composition. The metal impregnation on the HY catalyst could modify the acid site composition (Lewis and Brønsted acid sites), which had significant roles in the palm oil cracking to biofuels. Ni impregnation on HY zeolite led to the high cracking activity, while the Co impregnation led to the high deoxygenation activity. Interestingly, the co-impregnation of Ni and Co on HY catalyst could increase the catalyst activity in cracking and deoxygenation reactions. The yield of biofuels could be increased from 37.32% to 40.00% by using the modified HY catalyst. Furthermore, the selectivity of gasoline could be achieved up to 11.79%. The Ni and Co metals impregnation on HY zeolite has a promising result on both the cracking and deoxygenation process of palm oil to biofuels due to the role of each metal. This finding is valuable for further catalyst development, especially on bifunctional catalyst development for palm oil conversion to biofuels.
Peningkatan Kuantitas dan Kualitas Produk UKM Wingko Babat di Kota Semarang dengan “Modified Oven” Luqman Buchori; Didi Dwi Anggoro; Dyah Hesti Wardhani
Prosiding Seminar Nasional Teknik Kimia "Kejuangan" 2016: Prosiding SNTKK 2016
Publisher : Seminar Nasional Teknik Kimia Kejuangan

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Abstract

Wingko babat merupakan makanan oleh-oleh khas Kota Semarang yang banyak diminati oleh para wisatawan. Proses pembuatan wingko babat meliputi beberapa tahap yaitu tahap pencampuran bahan baku, pencetakan, pemasakan, pendinginan dan pengemasan. Namunpada proses pemasakan, bahan yang dimasak tidak bisa merata. Hal ini disebabkan distribusi api atau panas tidak merata sehingga produk yang dihasilkan terkadang ada yang gosong. Kuantitas produk atau jumlah bahan yang dimasak tidak bisa maksimal karena proses pemasakan lama. Akibatnyasulit memenuhi permintaan pasar. Untuk mengatasi permasalahan ini perlu dilakukan perbaikan sistem pemasakan bahan wingko babatdengan cara mendesain ulang peralatan masaknya yaitu dengan rancang bangun alat masak bahan wingko babat.Alat ini dinamakan modified oven. Alat ini terdiri dari lima bagian utama yaitu (1) saluran pipa, (2) modified oven, (3)lubangtempat keluarnya api, (4) lubang sirkulasi udara, dan (5) penyangga. Hasil aplikasi alat ini menunjukkan peningkatan kuantitas dan kualitas produk. Kapasitas produksi meningkat 75% per harinya.Penggunaan bahan bakar untuk sekali masak menurun 50%. Omset produksi naik menjadi hampir 75% dan keuntungan UKM meningkat 2 kali lipat. Hasil pemasakan dapat seragam sehingga produk wingko yang dihasilkan tidak sampai gosong. Tekstur produk lembut dan proses pemasakan menjadi lebih cepat. Kualitas produk wingko menjadi lebih terjaga dan dapat memenuhi permintaan pasar khususnya pada musim wisatawan.
Pengaruh Metode Pembuatan Katalis Metal/Zeolit Y Terhadap Karakterisasi dan Aktivitasi Katalis Didi Dwi Anggoro; Luqman Buchori
Prosiding Seminar Nasional Teknik Kimia "Kejuangan" 2018: PROSIDING SNTKK 2018
Publisher : Seminar Nasional Teknik Kimia Kejuangan

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Abstract

Utilizing Shear Factor Model and Adding Viscosity Term in Improving a Two-Dimensional Model of Fluid Flow in Non Uniform Porous Media Yazid Bindar; IGBN Makertihartha; M. Dani Supardan; Luqman Buchori
Journal of Engineering and Technological Sciences Vol. 39 No. 2 (2007)
Publisher : Institute for Research and Community Services, Institut Teknologi Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.5614/itbj.eng.sci.2007.39.2.3

Abstract

In a packed bed catalytic reactor, the fluid flow phenomena are very complicated because the fluid and solid particle interactions dissipate the energy. The governing equations  were developed in the  forms of  specific  models. The shear factor  model was introduced in the momentum equation for covering the effect  of  flow  and  solid  interactions  in  porous  media.   A  two  dimensional numerical  solution  for  this  kind  of  flow  has  been  constructed  using  the  finite volume  method.  The  porous  media  porosity  was  treated  as  non-uniform distribution  in  the  radial  direction.  Experimentally,  the  axial  velocity  profiles produce  the  trend  of  having  global  maximum  and  minimum  peaks  at  distance very close to the wall. This trend is also accurately picked up by the numerical result. A more comprehensive shear factor formulation results a better velocity prediction than other correlations do. Our derivation on the presence of porous media leads to an additional viscosity term. The effect of this additional viscosity term was investigated numerically. It is found that the additional viscosity term improves  the  velocity  prediction  for  the  case  of  higher  ratio  between  tube  and particle diameters
Co-Authors . Widayat Amin Nugroho Anggun Kurniawan Anindita Indriana Aprilina Purbasari Ardian D. Yudhistira Arum Sakti Prasetyo Astrilia Damayanti B Budiyono Berkah Fajar Bintang Ayu Kalimantini Boby Gusman Irianto Samosir Budiyono Budiyono Chusnul Khotimah Dewi Fatmawati Didi D. Anggoro Didi D. Anggoro Didi Dwi Anggoro Dinda Labibah Ubay Dyah Hesti Wardhani Dyah Hesti Wardhani Fachmy Adji Pangestu Setiawan Faleh Setia Budi Faleh Setia Budi Fegi Yuliandri Fradriyan Aulia Giveni Christina Silaen H Hadiyanto Hantoro Satriadi Hargono Hargono Harum Nissaulfasha Herawati Oktavianty Heri Cahyono Heru Susanto I Nyoman Widiasa I. Istadi I.G.B Ngurah Makertihartha Indro Sumantri Inshani Utami Istikhoratun, Titik JD Ryan Christy S Khonsa Syahidah Kusmiyati Kusmiyati Laeli Kurniasari M. Dani Supardan M. Dani Supardan M. Djaeni Maria Augustine Graciafernandy Meitiandari Mutiara Muhamad, Theobroma Guntur Muhammad Ulil Absori Nadia Taradissa Maheswari Ndaru Okvitarini Ngadi, Norzita Nita Aryanti Norzita Ngadi Nur Hidayati Nurjati Solikhin Nurul Aishah Aishah Nurushofa, Faustina Alda Okryreza Abdurrachman P Purwanto Pakpahan, Agnes J. Pakpahan, Andre W. S. Pratama, Pambudi Pajar Purwanto Purwanto Purwanto Purwanto Putri Diliyan Shakti Ratnawati Ratnawati Resti Nur Utami Riko Rikardo Putra Riyanto, Teguh Rizki Andre Handika Roikhatus Solikhah Salsabila, Unik Hanifah Saputra, Roni Ade Setia Budi Sasongko Setiadi, Iqfan Dwi Silviana Silviana Siswo Sumardiono Suherman Suherman Suherman Suherman Sulardjaka, S Teguh Riyanto Teuku Irfan Maulana Titik Istirokhatun Udin Mabruro Wahyu Fitriani Widayat Widayat Widayat Yayuk Astuti Yazid Bindar Yazid Bindar Yudha Duta Utama