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All Journal International Journal of Renewable Energy Development JURNAL KIMIA SAINS DAN APLIKASI Alchemy : Journal of Chemistry Jurnal Kimia Riset Science and Technology Indonesia Jurnal Penelitian Pendidikan IPA (JPPIPA) Indonesian Journal of Chemistry Communications in Science and Technology Chemistry Indonesian Journal of Chemical Research Kumawula: Jurnal Pengabdian Kepada Masyarakat Sains dan Matematika Indonesian Journal of Chemical Science and Technology PROFICIO: Jurnal Pengabdian Masyarakat Jurnal Pijar MIPA Unesa Journal of Chemistry Molekul: Jurnal Ilmiah Kimia
Pirim Setiarso
Universitas Negeri Surabaya
Agriculture, Biological Sciences & Forestry Humanities Astronomy Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Decision Sciences, Operations Research & Management Economics, Econometrics & Finance Education Energy Engineering Environmental Science Materials Science & Nanotechnology Mathematics Physics Social Sciences Other

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Fabrication of Carbon Paste Electrode Modified with Bentonite Nanoparticles and Titanium Dioxide Nanoparticles for Analysis of Methyl Parabens by Cyclic Voltammetry Hizbullah, Ahmad Jihad; Setiarso, Pirim
Jurnal Pijar Mipa Vol. 19 No. 1 (2024): January 2024
Publisher : Department of Mathematics and Science Education, Faculty of Teacher Training and Education, University of Mataram. Jurnal Pijar MIPA colaborates with Perkumpulan Pendidik IPA Indonesia Wilayah Nusa Tenggara Barat

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/jpm.v19i1.5949

Abstract

Cosmetics are products of several substances or ingredients with a predetermined time limit. Efforts to extend the time limit of cosmetic use are made by adding preservatives. One preservative that is often used is methylparaben. Methylparaben has been tested using spectrophotometry, voltammetry, and HPLC. In this study, electrode modification was carried out in the voltammetry test to obtain a low detection limit. The purpose of this study was to determine the effect of the working electrode composition of carbon paste, bentonite nanoparticles, titanium dioxide nanoparticles, and paraffin on the best response in the analysis of methylparaben by cyclic voltammetry, knowing the optimum measurement conditions of pH with the best electrode composition in the analysis of methylparaben by cyclic voltammetry. FTIR characterized bentonite nanoparticles to determine vibrations and functional groups, and XRD was performed to determine the phase and particle size. The electrode was made from a mixture of carbon, bentonite nanoparticles, titanium dioxide nanoparticles, and paraffin. The best electrode composition was added with titanium dioxide nanoparticles to obtain a higher peak current. XRD characterization of bentonite nanoparticles showed an average particle size of 43.8155 nm. The result of determining the best electrode composition is 3:2:3:2 with an anodic peak current of 9.6.10-4 A. The best methylparaben measurement at pH seven solution conditions. The latest research shows that carbon paste electrodes modified with bentonite and titanium dioxide nanoparticles can be used for methylparaben analysis.
Cyclic Voltammetry Method for Analysis of Phosphate Concentration in Water Agustin, Qomariyah; Setiarso, Pirim
Jurnal Pijar Mipa Vol. 19 No. 1 (2024): January 2024
Publisher : Department of Mathematics and Science Education, Faculty of Teacher Training and Education, University of Mataram. Jurnal Pijar MIPA colaborates with Perkumpulan Pendidik IPA Indonesia Wilayah Nusa Tenggara Barat

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/jpm.v19i1.6090

Abstract

Phosphate is a nontoxic element but a limiting element for productivity. Several methods have been established to analyze the phosphate concentration in water. This study aims to analyze phosphate concentration in water using the voltammetry method using cyclic voltammetry. Cyclic voltammetry is an electroanalytical method that measures the current outcome of oxidation-reduction reactions in response to the potential. The current outcome is directly proportional to the phosphate concentration in the solution. The calibration curve was formed from the KH2PO4 standard solution using concentrations of 0.1 mg/L, 0.2 mg/L, 0.4 mg/L, 0.8 mg/L, and 1.6 mg/L. The voltammogram showed that the analyte does not have an anode peak current (Ipa), which means that the analyte solution did not have an oxidation reaction, so the cathode peak current (Ipc) value was used. Based on the calibration curve, the linear regression graph with a straight-line equation is y = -0,00000645632x - 0,000208737 with R2 of 0,99737. Meanwhile, this cyclic voltammetry method was validated by calculating the LOD and LOQ values; the results are 0.1034 mg/L and 0.3134 mg/L, respectively. Hence, based on the analysis of phosphate concentration in water samples, this method works satisfactorily and is suitable for routine analysis because of its advantages.
Potential Analysis of Quercetin and Its Derivatives as Inhibitors of Hendra Virus (HeV) Rosyiidah, Nur Anisa; Setiarso, Pirim; Sanjaya, I Gusti Made
Indonesian Journal of Chemical Science and Technology (IJCST) Vol. 7 No. 1 (2024): JANUARY 2024
Publisher : Universitas Negeri Medan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24114/ijcst.v7i1.56448

Abstract

This study aims to determine the inhibitory potential of quercetin and its derivatives on the activity of Hendra virus (HeV) 6BK6 protein with its comparator N-Acetyl-D-[1-13C] Glucosamine. This research was carried out using the molecular docking method in order to obtain information related to binding affinity values, inhibition constants, and amino acid residues in the ligand-receptor hydrogen bonds. It was found that the compound quercetin 3-O-xyloside had the lowest binding affinity among the other compounds, namely -6.92 kcal/mol with an inhibition constant of 8.44 µM. In addition, there are four types of amino acid residues in the ligand-receptor hydrogen bonds including ASP304 (1,90 Ã…), SER301 (2,47 Ã…), ARG191 (3,18 Ã…), and MET188 (4.34 Ã…). In this case it can be concluded that the compound quercetin 3-O-xyloside has been shown to have the potential to inhibit the activity of the HeV 6BK6 protein.
The Effect of Ultrasonication on the Quality of Keratin Extraction Based on Ionic Liquid from Duck Feather Perdana, Senja Salzanabila Putri; Kusumawati, Nita; Basukiwardojo, Maria Monica Sianita; Setiarso, Pirim; Djalilah, Gina Noor; Rahmawati, Khofifatul
Communications in Science and Technology Vol 10 No 2 (2025)
Publisher : Komunitas Ilmuwan dan Profesional Muslim Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21924/cst.10.2.2025.1785

Abstract

This study investigates the effect of ultrasonic-assisted extraction (UAE) and solvent extraction (SE) on keratin recovery from duck feathers using sodium sulfide-based ionic liquids under different pH conditions. The results showed that SE at acidic pH (pH=3) achieved the highest yield (92%), whereas UAE showed lower recovery (28%) under mildly acidic conditions (pH=5). Spectroscopic and electrophoretic analyses using FTIR confirmed the β-sheet structure with characteristic peaks at 3400 cm−1 (O–H and N–H stretching) and 1660 cm−1 (C=O stretching). Sodium Dodecyl Sulfate Polyacrylamide Gel Electrophoresis analysis (SDS-PAGE) revealed protein bands in the 15–25 kDa range, typical of β-keratin, with higher intensity in SE. Morphological analysis using SEM revealed finer and more homogeneous particles for UAE, while SE produced denser aggregates. Thermal analysis revealed two main degradation stages, occurring at 0–100 °C and 250–500 °C, with UAE samples exhibiting lower residual mass (5.46%) than SE (8.65%). Particle size analysis showed UAE samples had larger but more uniformly distributed particles. XRD results confirmed semi-crystalline structures, with UAE increasing amorphous content and SE maintaining crystallinity. These findings highlight the complementary advantages for tailoring keratin properties toward diverse applications.
PENDAMPINGAN MANAGEMEN USAHA PUPUK CAIR PADA PETERNAK SAPI PERAH DUSUN BRAU BATU Hayati, Nur; Kusumawati, Nita; Setiarso, Pirim; Monica, Maria; Sanjaya, I Gusti Made; Samik, Samik
Jurnal Pengabdian Masyarakat FKIP UTP Vol 7 No 1 (2026): PROFICIO : Jurnal Abdimas FKIP UTP
Publisher : FKIP UNIVERSITAS TUNAS PEMBANGUNAN SURAKARTA

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.36728/jpf.v7i1.6053

Abstract

Kota Batu merupakan bagian dari Provinsi JawaTimur. Dusun Brau terletak di Kecamatan Bumiaji Kota Batu pada ketinggian 1000 mdpl, suhu rata-rata harian 18-25 °C dengan bentang wilayah berupa perbukitan dengan kontur tanah yang subur. Ketersediaan pakan hijauan yang memadai sebagian besar warga Dusun Brau Desa Gunungsari menyandarkan penghasilan untuk kebutuhan hidupnya dengan membudidayakan sapi perah. Hasil utama budidaya sapi perah adalah produk susunya, dengan salah satu hasil samping berupa limbah peternakan yaitu kotoran sapi. Pada tahun 2023, tim PKM telah melatihkan kepada warga usaha untuk meningkatkan nilai ekonomi kotoran sapi dengan menjadikannya pupuk cair. Selama satu tahun ke belakang, hasil pembuatan pupuk cair digunakan oleh warga untuk sawah atau kebun mereka. Dengan mempertimbangkan kemampuan warga yang masih kurang dalam menghasilkan produk yang siap jual, tim PKM telah menyusun skala prioritas yang harus segera diupayakan penyelesaiannya melalui program PKM Kebijakan Fakultas MIPA Tahun 2024 ini, yaitu: 1) banyaknya pupuk cair yang mampu dihasilkan oleh warga; 2) pupuk cair masih dimanfaatkan secara pribadi; dan 3) rendahnya pengetahuan mitra mengenai managemen usaha pupuk cair. Solusi dari permasalahan tersebut adalah melakukan introduksi pengemasan dan labelling produk pupuk cair. Kata Kunci: Brau; limbah peternakan; dan pengemasan produk
PELATIHAN PEMBUATAN BATIK ECOPRINT UNTUK PEMBEKALAN KEWIRAUSAHAN SISWA SMAN 1 REJOSO, NGANJUK Sari Edi Cahyaningrum; Pirim Setiarso; Fitriari Izzatunissa Muhaimin; Nurhadi; Yetty Tinari; Diah Kenthiri Esa Prastika
Jurnal Pengabdian Masyarakat FKIP UTP Vol 7 No 2 (2026): PROFICIO : Jurnal Abdimas FKIP UTP
Publisher : PROFICIO

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.36728/.v7i2.6569

Abstract

Batik ecoprint adalah teknik batik yang menggunakan bahan-bahan alami seperti daun, bunga, dan batang tumbuhan untuk menciptakan motif pada kain. Teknik ini berbeda dengan batik tradisional yang menggunakan lilin (malam) untuk membuat motif, ecoprint memanfaatkan pigmen warna alami dari tumbuhan untuk mentransfer warna ke serat kain. Proses ini menghasilkan motif yang unik, organik, dan ramah lingkungan. Perbedaan Batik Ecoprint dengan Batik Tradisional: Pewarna: Batik tradisional menggunakan malam (lilin) untuk membuat motif dan pewarna kimia, sedangkan batik ecoprint menggunakan bahan alami seperti daun, bunga, dan batang tumbuhan. Pada tahap desain ini tim PKM melakukan perancangam awal program pelatihan, merancang materi pelatihan dan merancang evaluasi pelatihan secara konseptual yang nantinya akan dijadikan dasar dalam tahapan pengembangan. Langkah-langkah kegiatan yang akan dilakukan untuk memecahkan masalah yang dialami mitra adalah sebagai berikut, yakni pemberian pelatihan terhadap guru yang telah diidentifikasi sebelumnya. Pemberian pelatihan ini dilakukan di sekolah,Tahap implementasi pelatihan dilakukan secara tahap muka dan penugasan. Tahap evaluasi dilakukan dengan mengevaluasi hasil penugasan kepada peserta terkait pembuatan batik ecoprint. Hasil PKM ini memberikan dampak yang bermakna bagi siswa SMAN 1 Rejoso Nganjuk. Kegiatan pelatihan ecoprint ini berhasil dilaksanakan dengan baik dan mencapai tujuan yang ditetapkan. Antusiasme siswa dalam kegiatan ini membuktikan bahwa metode pembelajaran langsung (experiential learning) sangat efektif. Kegiatan ini tidak hanya melatih keterampilan seni tetapi juga sukses menanamkan nilai-nilai cinta lingkungan dan potensi kewirausahaan. Kegiatan ini mendukung SDGs 4,8 dan 9
Co-Authors A'yun, Qurrota Agustin, Qomariyah Andianita, Tri Dyah Anggraini Putri, Dhea Ashabul Kahfi Ashabul Kahfi, Ashabul Ayu Ilfiana Buchari Buchari Cahyani, Sinta Anjas Diah Kenthiri Esa Prastika Didin Mujahidin Dina Kartika Maharani Eka Candra Saputra Elsa Rishda Hariningtias ERLITA PUTRI, PUPUT Estiningtyas, Indri Wasa Fachrirakarsie, Fadlurachman Faizal Fajrin, Aisyah Rahmatul Fatihah, Vita Ayu Febriyana, Andini Fitriari Izzatunissa Muhaimin Gina Noor Djalilah Hafidha, Qonita Arky Harsono, Rifanda Viantiano Hery Widijanto Hizbullah, Ahmad Jihad I GUST MADE SANJAYA Ihda Shoumi Nurdini Indah Tri Wahyuni Indah, Rahmalia Indra Noviandri INGGRIANI, FIRMA Khoiriyah, Nuril Kurniawan, Muhammad Ridho Hafid Lenny Yuanita Maria Monica Sianita Maria Monica Sianita Basukiwardojo MAY LUKMANA, KUMININGSIH Monica, Maria Mulyono, Dymarda Indra Santoso Nafisatus Zakiyah Naulia, Kaila Nerry Puspita Sari Nita Kusumawati Nita Kusumawati Nur Hayati Nurhadi Nuril Khoiriyah Nurzulla, Weka Firda Rizki Perdana, Raga Agung Perdana, Senja Salzanabila Putri Putra, Ananta Adita Eka Putri, Marinda Mayliansarisyah Rahayu, Nunik Tri Rahmawati, Khofifatul RAIDAH RUSNADI, WINDA Ramadanti, Awanda Halida Rhamdiyah, Fastabiqul Khairati Rimbi Rodiyana Sova Riska Nur Safitri, Riska Nur Rosyiidah, Nur Anisa Safitri, Rizka Dwi Samik Samik Samik Samik Sanjaya, IGM Sari Edi Cahyaningrum Sinta Anjas Cahyani Supari Muslim Supari Muslim Suyatno Sutoyo Taufik Hidayatulloh Tukiran Tukiran Wachid, Rochman Wahono Widodo Yetty Tinari Zahro, Nafisatuz Zakiyah, Nafisatus