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All Journal International Journal of Renewable Energy Development Urania Jurnal Ilmiah Daur Bahan Bakar Nuklir Jurnal Bahan Alam Terbarukan Seminar Nasional Teknik Kimia Kejuangan Journal of Engineering and Technological Sciences Jurnal Rekayasa Proses
Wahyudi Budi Sediawan
Departemen Teknik Kimia, Fakultas Teknik, Universitas Gadjah Mada, Jl. Grafika No.2 Yogyakarta 55281, Indonesia, Telp.(+62274) 561176
Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Energy Engineering Environmental Science Materials Science & Nanotechnology

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Pemodelan Dekomposisi Ammonium Carbamate pada Tekanan Tinggi di Pabrik Urea Sunarya, Rahmat; Sediawan, Wahyudi Budi; Hidayat, Muslikhin
Prosiding Seminar Nasional Teknik Kimia "Kejuangan" 2023: PROSIDING SNTKK 2023
Publisher : Seminar Nasional Teknik Kimia "Kejuangan"

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Abstract

Urea acts as a nitrogen-based fertilizer to boost crop production and prevent a worldwide hunger crisis. Considering ways to make urea production in existing plants more environmentally friendly, a detailed study has been conducted on the high-pressure stripper, in which the equipment uses intensive energy to decompose ammonium carbamate. The mathematical model was prepared using the two-film theory. The UNIQUAC and Redlich-Kwong equations of state have been used to express nonideality in the NH3-CO2-H2O-urea system under high pressure and temperature circumstances. Due to the lack of transport properties in extreme conditions, the properties were estimated using a theoretical method. The present study obtained the mass-transfer coefficient in dimensionless form  and . Moreover, the heat-transfer coefficient was calculated using the Chilton-Colburn analogy. The proposed model result matches what is expected with the commercial plant data. Furthermore, with less than 5% relative deviations, the model deserves significant consideration for any practical use in high-pressure stripper simulation
Sintesis Asil Gliserol Melalui Reaksi Esterifikasi Asam Oleat dengan Gliserol Husada, Caesar Purnama; Sulistyo, Hary; Sediawan, Wahyudi Budi
Prosiding Seminar Nasional Teknik Kimia "Kejuangan" 2023: PROSIDING SNTKK 2023
Publisher : Seminar Nasional Teknik Kimia "Kejuangan"

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Abstract

Acyl glycerol derivatives from oleic acid, especially monoacylglycerol (MAG) and diacylglycerol (DAG), are products that is widely used in the food, lubricant, and cosmetic industries. Acyl glycerol can be obtained through esterification reaction of glycerol with fatty acids.  This study aims to determine the effect of temperature on the conversion and amount of acyl glycerol produced. This research was conducted using a batch system with temperature variations of 80°C, 100°C, and 120°C with HCl 1%wt as catalyst and 1:1 reactant mole ratio (glycerol: oleic acid) for 2 hours reaction time. Samples were taken every 10 minutes, then the samples were analyzed using Thin Layer Chromatography (TLC) to determine the fraction of the product produced. The experimental results showed that increasing the temperature will produce higher conversions and acyl glycerols. The highest conversion of oleic acid occurred at 120°C (43.016%), with mole percentage of 1,796% monoacylglycerol (MAG), 3,820% diacylglycerol (DAG), and 5,813% triacylglycerol (TAG).
Sintesis Surfaktan Non-ionik Berbasis Asam Palmitat Melalui Reaksi Esterifikasi dengan Gliserol Purbaningdyah, Emma; Sulistyo, Hary; Sediawan, Wahyudi Budi
Prosiding Seminar Nasional Teknik Kimia "Kejuangan" 2023: PROSIDING SNTKK 2023
Publisher : Seminar Nasional Teknik Kimia "Kejuangan"

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Abstract

Esterification of glycerol using the fatty acids is one of methods that is widely used in the conversion of glycerol to synthesize products containing monoacylglycerol (MAG) and diacylglycerol (DAG). Among the various types of surfactants, monoacylglycerol (MAG) and diacylglycerol (DAG) are the most widely used of non-ionic surfactants in many industries such as food, pharmacy and cosmetic. This study aims to determine the effect of temperature on the conversion of palmitic acid and the concentration fraction of products. This research was conducted in a batch system with the temperature variations of 80°C, 100°C and 120°C; using 1% HCl catalyst concentration of palmitic acid mass, and reactant mole ratio of 1:1 (glycerol: palmitic acid). Samples were taken every 10 min during 120 min of reaction, to be analyzed by Thin Layer Chromatography (TLC) to determine the concentration fraction of products. The experimental results showed that increasing temperature enhanced the products formation, thus, increased the fraction concentration of products. However, the highest conversion of palmitic acid (80.14%) was obtained at 120°C, with concentration fraction of 1.67% monoacylglycerol (MAG), 10.96% diacylglycerol (DAG) and 6.01% triacylglycerol (TAG).
Co-Authors Amelia, Shinta Astrilia Damayanti Devi Yuni Susanti Fikrah Dian Indrawati Sawali Hary Sulistyo Husada, Caesar Purnama Indra Perdana Moh. Azhar Afandy Muslikhin Hidayat Mustikaningrum, Mega Nugraheni, Prihati Sih Nurwidyaningrum, Kristanti Nuryoto Purbaningdyah, Emma Retno Ambarwati Sigit Lestari Sarto Soeriyadi, Alexander H. Sunarya, Rahmat Teguh Ariyanto Ustadi, Ustadi Wiratni Budhijanto Zahrul Mufrodi, Zahrul