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All Journal JURNAL KIMIA SAINS DAN APLIKASI Jurnal Bahan Alam Terbarukan PROSIDING SEMINAR KIMIA Jurnal Kimia Mulawarman ALCHEMY Jurnal Penelitian Kimia JURNAL ATOMIK Jurnal Bahan Alam Terbarukan
Noor Hindryawati, Noor
Jurusan Kimia, Fakultas Matematika Dan Ilmu Pengetahuan Alam, Universitas Mulawarman
Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Energy Engineering Environmental Science Materials Science & Nanotechnology

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Journal : JURNAL ATOMIK

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Mini Review: Citrus sinensis Sebagai Bioreduktor Dalam Green Synthesis Nanopartikel Hiyahara, Irfan Ashari; Hindryawati, Noor; Syaima, Husna; Akbar, Muhammad Marion; Duratulhikmah, Nur Fadhilah; Putra, Narundana Perdana; Wulandari, Siti Aprilia; Larasati, Zarra Udyani; Rahayuningsih, Rahayuningsih; Indriani, Isah Waliah
JURNAL ATOMIK Vol 8 No 1 (2023)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

Green synthesis is an eco-friendly approach that provides a viable alternative to traditional physical and chemical methods for the production of nanoparticles. This technique employs non-toxic and safe materials, such as plants, microorganisms, algae, bacteria, yeast, and fungi, to generate stable and less toxic nanoparticles. Citrus sinensis, commonly known as sweet orange, is a plant that contains various active compounds. These bioactive compounds can be extracted and used as bioreductants in green synthesis of nanoparticles. This mini review aimed to provide an overview of the current state of research on the utilization of Citrus sinensis as a bioreductant in the production of nanoparticles. A systematic search strategy was employed to identify research articles that met the criteria of discussing green synthesis of nanoparticles with Citrus sinensis as a bioreductant. The nanoparticles produced using Citrus sinensis extract can be either metal nanoparticles or metal oxide nanoparticles. The review highlights the distribution of nanoparticles produced with Citrus sinensis extract, their applications, and the extraction process of Citrus sinensis commonly employed in green synthesis of nanoparticles. Hopefully this review serves as a useful reference for researchers and practitioners who are interested in employing the Citrus sinensis plant as a bioreductant in the green synthesis of nanoparticles.
CORRELATION OF Pb METAL ION LEVELS ON PROTEIN CONCENTRATION IN CRUSH CONSTRUCTION (Gafrarium tumidium) TAKEN IN THE COAST OF BONTANG, EAST KALIMANTAN Corebima, Damianus Develistur; Kartika, Rudi; Hindryawati, Noor
JURNAL ATOMIK Vol 5 No 2 (2020)
Publisher : Jurusan Kimia FMIPA UNMUL

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Research on the correlation of Pb metal ion levels to protein content in crush clams (Gafrarium tumidium) taken at the coast of the East Kalimantan Rhino Estuary has been conducted. This study aims to determine the levels of Pb metal ions and protein levels in blood clams based on the size and location of different samples. Correlation of Pb metal ion levels and protein in blood clams was tested using the Least Square method and Pearson product moment. Analysis of Pb metal ion levels using SSA (Atomic Absorption Spectrophotometer) and protein content analysis using the Kjeldahl method. In this study, the Pb metal ion level was obtained at the public port of Tanjung Limau, PPI Tanjung Limau and beach Lallo Sekangat with an average of 0.7474 mg/L, 0.5513 mg/L, and 0.2804 mg/L respectively. Crush clam protein content at Tanjung Limau, PPI Tanjung Limau and beach Lallo Sekangat with an average of 19.6544%, 14.6902%, and 10.9135% respectively. The correlation of Pb metal levels to protein levels in crush clams (Gafrarium tumidium) was stated positively with coefficient correlation results was strong (r = 0.7910).
Daya Antibakteri Ekstrak Metanol Buah Okra (Abelmoschus esculentus (L.) Moench) puah, Siti Mar; Astuti, Winni; Hindryawati, Noor
JURNAL ATOMIK Vol 6 No 2 (2021)
Publisher : Jurusan Kimia FMIPA UNMUL

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ABSTRACT Phytochemical test and antibacterial activity of methanol extract of Okra (Abelmoschus esculentus (L.) Moench) fruit have been carried out. Extraction using maceration method. The methanol extract of Okra fruit contains phenolic secondary metabolites, alkaloids and steroids. Antibacterial activity opposes the agar diffusion method against the bacteria Salmonella typhi and Steprococcus mutans. The Minimum Inhibitory Concentration Value of Okra fruit methanol extract against Salmonella typhi bacteria at a concentration of 0.625-1.25% and against Streptococcus mutans bacteria 1.25% -2.5%. Okra fruit methanol extract has antibacterial activity with wide variations. Keywords : Abelmoschus esculentus (L.) Moench, antibacterial activity, secondary metabolites, Minimum Inhibitory Concentration (MIC).
SINTESIS DAN KARAKTERISASI NANOPARTIKEL PERAK TERMODIFIKASI KITOSAN MENGGUNAKAN REDUKTOR NaBH4 Az Zahra, Upi Fathimah; Hindryawati, Noor; Panggabean, Aman Sentosa
JURNAL ATOMIK Vol 9 No 2 (2024)
Publisher : Jurusan Kimia FMIPA UNMUL

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/ja.v9i2.1406

Abstract

The research about synthesis of chitosan-modified silver nanoparticles using NaBH4 reducing agents has been carried out. This research aims to determine the optimum AgNO3 concentration, optimum pH and optimum stirring time. The chitosan-modified silver nanoparticles obtained were then characterized using a UV Vis Spectrophotometer, Particle Size Analyzer and Transmission Electron Microscopy instruments. The results of measurements using a UV-Vis Spectrophotometer, the synthesis of chitosan-modified silver nanoparticles was obtained was obtained at the optimum condition of AgNO3 concentration of 3x10-3 M, pH 4 and the optimum stirring time was 2 hours. The formation of AgNPs is characterized by the presence of typical absorption peaks at maximum wavelengths of 402 nm-434 nm. Keywords: Silver Nanoparticles, Chitosan, NaBH4
OPTIMASI PEMBENTUKAN NANOPARTIKEL PERAK DENGAN BIOREDUKTOR DARI EKSTRAK DAUN TAHONGAI ( Kleinhovia hospita Linn.) -, Rahayuningsih; Hindryawati, Noor; Syaima, Husna
JURNAL ATOMIK Vol 9 No 2 (2024)
Publisher : Jurusan Kimia FMIPA UNMUL

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/ja.v9i2.1397

Abstract

The synthesis of Silver Nanoparticles was carried out by bottom-up method by reducing Ag+ ions to Ag0 using Tahongai leaves (Kleinhovia hospital Linn) which contain secondary metabolites such as alkaloids, flavanoids and phenolics as bioreductors that reduce AgNO3 solution as a precursor. The purpose of this study was to determine whether tahongai leaves can be used as a bioreductor in the synthesis of silver nanoparticles. The concentration variation of tahongai leaf extract bioreductor was 25 %; 50 %; and 75 %. Changes in silver nanoparticles can be marked by changes in the color of the solution and by UV-Vis Spectrophotometer absorption. The results of this study showed a change in color of AgNO3 solution from clear to brownish yellow which indicates the formation of silver nanoparticles, and through UV-Vis Spectrophotometer analysis showed absorption at wavelengths of 420 to 430 which indicates relatively stable nanoparticles so it can be concluded that tahongai leaf extract can be used as a bioreductor for the synthesis of silver nanoparticles.
ANALISIS KADAR LOGAM Pb, Mn dan KANDUNGAN PROTEIN PADA DAGING UDANG WINDU (Penaeus sp.) YANG DIAMBIL DIPERAIRAN SUNGAI DONDANG KECAMATAN MUARA JAWA Octavianus, Riyan; Kartika, Rudi; Hindryawati, Noor
JURNAL ATOMIK Vol 3 No 1 (2018)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

Research on metal concentration of Pb, Mn and protein content in windu shrimp’s meat (Penaeus sp.) analysis in Dondang river, Muara Jawa have been done. This research is aimed to determine the concentration of heavy metal Pb, Mn and concentration of protein inside windu shrimp based by size and different sampling location. Concentration of heavy metal Pb, Mn and protein are correlated using Least Square method. Concentration of heavy metal Pb and Mn are analyzed by using AAS (Atomic Absorption Spectrophotometry) and concentration of protein are analyzed by using Kjeldahl method. Result of this research is the concentration heavy metal Pb and Mn in sampling point 1 in average concentration are 0.556 mg/L and 0.463 mg/L, sampling point 2 are 0.790 mg/L and 0.738 mg/L, sampling point 3 are 0.876 mg/L and 0.905 mg/L. Concentration of protein in windu shrimp in sampling point 1 in average are 23.4928%, sampling point 2 are 28.1701% and sampling point 3 are 29.1622%. Correlation of concentration of heavy metal Pb and Mn to the concentration of protein in windu shrimp (penaeus sp.) with R = 0.791; r = 0.948.
ETHANOL PRODUCTION FROM TUBER GANYONG (Canna Edulis Kerr.) BY Saccharomyces cerevisiae WITH THE ADDITION OF Spirulina Sp. Sukanadi, I Putu; Kartika, Rudi; Hindryawati, Noor
JURNAL ATOMIK Vol 2 No 2 (2017)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

This study demonstates the potential of starch tuber ganyong (Canna edulis Kerr.) as a substance for making ethanol by Saccharomyces cerevisiae with microalgae addition of Spirulina sp. as a source of nutrients in the fermentation process of ethanol has been carried out. The study also aims to determine the amount of nutrient concentration and fermentation time was used to generate the optimum ethanol content. Hydrolysis process by enzymatic is done through a liquification phase with α-amylase and saccharification phase with gluko-amylase. Furthermore the process of fermentation stage with the variation of the time (132 hours, 156 hours, 180 hours and 204 hours) using the yeast Saccharomyces cerevisiae with the addition of Spirulina sp. as a nutrient in the variation of Spirulina sp. concentrations (0,6 % (w/v), 1,2 % (w/v) and 1,8 % (w/v)). The result showed the sugar reducing after of hydrolysis was obtained with amount of 0,527 %, increased from the initial state with amount of 0,351 %. The highest ethanol content be found on the increase nutrient with amount of 1,2 % (w/v) by is time of fermentation to180 hours.
ADSORPTION OF FE METAL ION IN SOLUTION USING NATURAL ZEOLITE ACTIVATED BY KOH Palentin, Ersa Rizkita; Hindryawati, Noor; Gunawan, Rahmat
JURNAL ATOMIK Vol 4 No 2 (2019)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

Adsorbtion of Fe metal ion in solution using natural zeolite activated by KOH has been conducted. Natural zeolite was characterized using X-Ray Flourescence (XRF), X-Ray Diffraction (XRD) and surface area test. The XRF analysis results showed a decreasing SiO2 composition in natural zeolite activated by KOH 1.5 M. XRD analysis results showed the type of natural zeolite activated by KOH was mordenite with the chemical compound Ca2.5Na2Al7Si41O96.24H2O. The surface area of natural zeolite was 75.041 m2/g and after activation with KOH 1.5 M was 126.908 m2/g. The optimum conditions for the adsorption of Fe ions was at pH 4 with % adsorption was 96.24% at a 90 minutes the % adsorption was 98.3%.
ACTIVATON AND CHARACTERIZATION OF NATURAL ZEOLITE USING NaOH Sumarni, Sumarni; Hindryawati, Noor; Alimuddin, Alimuddin
JURNAL ATOMIK Vol 3 No 2 (2018)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

A study on the activation of natural zeolite using NaOH and it’s application for adsorption Rhodamin B from waste liquid woven Samarinda has been conducted. The activation process was conducted by several steps namely, sample preparation and activation stage using NaOH with ultrasonic assisted, then characterized using X-Ray Flourescence (XRF), X-Ray Diffraction (XRD). The XRF analysis result showed that indicates a decrease of SiO2 54.359% in natural zeolite after activation with 6 M NaOH. The XRD analysis result showed the type of natural zeolite activated NaOH was mordenit with chemical compound Ca2.5Na2Al7.Si41O96.24H2O. The optimum condition on the adsorpsi of Rhodamin B from waste liquid woven Samarinda using activated zeolite at 6 M NaOH 60 minutes and with persen adsorpsi was 87.487 % and on the adsorbent weight of 1.25 gram with persen adsorption 82.311 %.
Sintesis Silika Dari Abu Sekam Padi Termodifikasi 2-Merkaptobenzotiazol untuk Adsorpsi Ion Logam Cd2+ dan Cr6+ Syukri, Irma; Hindryawati, Noor; Subagyono, R.R. Dirgarini Julia Nurlianti
JURNAL ATOMIK Vol 2 No 2 (2017)
Publisher : Jurusan Kimia FMIPA UNMUL

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Abstract

A study on the adsorption of Cd2+ ion using silica gel modified with 2-mercaptobenzothiazole (MBT) from rice husk ash has been conducted. The modification of silica gel with MBT was conducted by several steps namely, sample preparation, synthesis of sodium silicate and modification of silica using MBT through a sol gel method. The XRF result showed that silica gel contained 98.98 % SiO2 . The FTIR spectrum of silika MBT showed the persence of Si-OH, Si-O, Si-O-Si and –SH groups. The surface area of silica gel and silica MBT were 163 m2/g and 30 m2/g, respectively. The adsorption capacity of Cd2+ ion was 0.42 mg/g and the adsorption percentage was 69.40%. The presence of Cr6+ ion decreased the adsorption capacity of silica MBT over Cd2+ ion.
Co-Authors -, Rahayuningsih Abdul Aziz Adhaina, Karina Aditya, Adrian Maulana Ahmad, Atika Aulia Akbar, Muhammad Marion Alimuddin Alimuddin Aman Sentosa Panggabean Apriliana, Nina Arief, M. Syaiful Ashari, Irfan Audi Zahid Iswaradi Az Zahra, Upi Fathimah Bergita, Angela Br Ginting, Survina Osalia Chairul Saleh Corebima, Damianus Develistur Daniel -, Daniel Daniel Daniel Duratulhikmah, Nur Fadhilah Elean, Samuel Erwin Erwin Eva Marliana, Eva Gaanty Pragas Maniam, Gaanty Pragas Hariati, Hariati Hariati, Hariati Helbianurramdan, Helbianurramdan Hiyahara, Irfan Ashari Husna Syaima Indriani, Isah Waliah Kusmiaty, Prilianda Laksono, Annuary Larasati, Zarra Udyani Laurentha, Nantha Mid, Arsy Aprilia Muhammad Marion Akbar N. S, R. R. Dirgarini Julia N., R.R. Dirgarini N., R.R. Dirgarini Julia Nanang Tri Widodo Octavianus, Riyan Octavianus, Riyan Oktaviani, Reka Palentin, Ersa Rizkita Pasuluran, Nirwanto Prastiwi, Mela puah, Siti Mar Putra, Narundana Perdana Putri, Rinda Anisyah Putriani, Elsa Avrilia Rahayuningsih Rahayuningsih, Rahayuningsih RAHMAT GUNAWAN Rahmat Gunawan Rakhmad, Rakhmad Ratna Kusuma Ronaldy, Igo Marsat Rudi Kartika, Rudi Saputra, Herdian Sari, Ermalia Lintang Sari, Helbyarti Mawar Setiawan, M. Pratsojo Soerja Koesnarpadi Subagyono, Dirgarini Julia Nurlianti Subagyono, R.R. Dirgarini Julia Nurlianti Subagyono, R.R. Dirgarini Julia Nurlianti Subagyono, RR Dirgarini Julia Nurlianti Subagyono, RR Dirgarini Julia Nurlianti Sukanadi, I Putu Sumarni Sumarni Syukri, Irma Syukri, Irma Tandirerung, Edman Tanjung, Faisal Teguh Wirawan Teguh Wirawan, Teguh Tika Widyastuti Wahyuni Ramadhani Wilsoma, Wilsoma Winanti, Renita Anggun Winni Astuti, Winni Wulandari, Duwi Devi Wulandari, Siti Aprilia Yuli Yana