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INDONESIA
JURNAL ATOMIK
Published by Universitas Mulawarman
ISSN : 25490052     EISSN : 25490052     DOI : -
Core Subject : Science, Social, Engineering,
Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Energy Environmental Science
Jurnal Atomik (JA) is published twice a year (March and August) by Department of Chemistry, Faculty of Mathematics and Natural Sciences, Mulawarman University. Jurnal Atomik is a media for graduate students of Department of Chemistry to publish their research articles in Chemistry field including Analytical Chemistry, Inorganic Chemistry, Physical Chemistry, Organic Chemistry, and Biochemistry. The research articles that be submitted to Jurnal Atomik have to be approved by Editorial Board and in accordance with the rules of writing approved by Editor of Jurnal Atomik.
Arjuna Subject : -
Articles 10 Documents
 1 
Search results for , issue "Vol 10 No 1 (2025)" : 10 Documents clear
Pembuatan Arang Aktif Kulit Buah Tarap (Artocarpus odoratissimus B.) dan Komposit Fe3O4-Arang Aktif Kulit Buah Tarap Sebagai Adsorben Logam Kadmium (Cd) Fradita, Windiy Mira; Koesnarpadi, Soerja; Wirawan, Teguh
JURNAL ATOMIK Vol 10 No 1 (2025)
Publisher : Jurusan Kimia FMIPA UNMUL

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/ja.v10i1.1411

Abstract

Tarap (Artocarpus odoratissimus B.) is a species of the genus Artocarpus and belongs to the Moraceae family. In its use, fruit cores, skins, and leaves can become metal adsorbents. This research aims to determine the characteristics and adsorption capacity of tarap fruit skin, which can be an alternative to dealing with cadmium (Cd) metal pollution. Making activated charcoal adsorbent tarap fruit peel was carbonated at a temperature of 450ºC for 1 hour and activated using 2 M HCl, while the Fe3O4-activated charcoal composite tarap fruit peel was made using the coprecipitation method from FeSO4.7H2O and FeCl3.6H2O with a mole ratio of 1:1 and then combined with tarap fruit peel activated charcoal to adsorb cadmium metal using the batch method, which is separated using an external magnet and analyzed using an Atomic Absorption Spectrophotometer. The results of FT-IR characterization on both adsorbents contained C-O and O-H groups and on the Fe3O4-activated charcoal composite of tarap fruit peel, there were Fe-O groups. The XRD difactogram shows that there is a Fe3O4 diffraction pattern with relatively small intensity in the Fe3O4-activated charcoal composite of tarap fruit peel. The results of VSM analysis show that the Fe3O4-activated charcoal composite of tarap fruit peel is paramagnetic. The optimum conditions for the adsorption of cadmium metal on activated charcoal from tarap fruit peel were at pH 7 with a contact time of 60 minutes and on the Fe3O4-activated charcoal composite from tarap fruit peel at pH 6 with a contact time of 45 minutes. The maximum adsorption capacity of activated charcoal from tarap fruit peel is 11.1316 mg/g and for the Fe3O4-activated charcoal composite tarap fruit peel is 22.9510 mg/g.
PEMBUATAN DAN KARAKTERISASI MEMBRAN ELEKTRODA SELEKTIF ION Cu(II) MENGGUNAKAN IONOFOR Na2S SEBAGAI SENSOR KIMIA Rosyada, Amrina; Arif, Moh. Syaiful; Panggabean, Aman Sentosa
JURNAL ATOMIK Vol 10 No 1 (2025)
Publisher : Jurusan Kimia FMIPA UNMUL

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/ja.v10i1.1418

Abstract

Preparation and characterization of Cu(II) ion selective electrode membranes based on polyvinyl chloride (PVC) using sodium sulfide (Na2S) as the ionophore has been done. The use of PVC polymer functions as a material that strengthens the properties of the membrane mixed with Na2S to form a homogeneous membrane and can reduce the risk of leaks in the membrane used. However, PVC has stiff properties, so a plasticizer in the form of DOP was needed to reduce intermolecular forces and make the membrane elastic. The preparation was carried out with the composition Na2S : PVC : DOP, namely 6 : 3 : 1. The membrane was doped with CuSO4 solution for 7 days and the Cu2+ ESI performance was measured to increase the optimal conductivity of the membrane, it is done by doping the membrane, namely by inserting 1 M Cu2+ dopant metal. The ESI Cu2+ performance results show a solution composition of 1:2 CuSO4:KNO3 and works well in the composition range 10-5 - 10-1 M, with a Nernst factor value of 28.9 mV/decade and a detection limit of 1.01×10-5 M. The response time of ESI Cu2+ was 10-60 seconds and can be used for 3 days. ESI Cu2+ works in the pH range 4-6 and the presence of interfering ions Cd2+, Zn2+, Cl-, NO3- and SO42- does not affect the performance of ESI Cu2+.
AKTIVITAS AMILASE PENDEGRADASI PATI MENTAH DARI BAKTERI AIR SUNGAI KARANG MUMUS Adawiyah, Rabiatul; Astuti, Winni; Pratiwi, Djihan Ryn
JURNAL ATOMIK Vol 10 No 1 (2025)
Publisher : Jurusan Kimia FMIPA UNMUL

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/ja.v10i1.1409

Abstract

Raw starch degrading amylase (RSDA) is an enzyme that can degrade raw starch into glucose without going through the gelatinization process. This research was conducted to isolate RSDA producing bacteria originating from the Karang Mumus River in Samarinda City. Bacterial isolation was carried out using the spread plate method. Screening for RSDA producing bacteria using nutrient media containing raw starch. The results of bacterial isolation obtained 14 single colonies of bacteria. A total of 5 bacterial colonies out of 14 bacteria were able to produce RSDA. Then the RSDA enzyme from the 5 bacteria was tested for amylase activity quantitatively using the dinitrosalicylic acid (DNS) method. Then, of the 5 bacteria, 1 bacterium with the colony code KM 5 had the highest activity, namely 0,332 U/mL.
UJI AKTIVITAS ANTIOKSIDAN KOMBINASI ESKTRAK METANOL DAUN REMEK DAGING (Hemigraphis colorata W.Bull) DAN DAUN KRATOM (Mitragyna speciosa Korth) Aina, Nur; Saleh, Chairul; Marliana, Eva
JURNAL ATOMIK Vol 10 No 1 (2025)
Publisher : Jurusan Kimia FMIPA UNMUL

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/ja.v10i1.1483

Abstract

Antioxidant activity test of a combination of methanol extracts of meat remek leaves (Hemigraphis colorata w. bull) and kratom leaves (Mitragyna speciosa Korth) using the 1,1-diphenyl-2-picrylhydrazyl (DPPH) silencing method with vitamin C as a positive control was analysed by UV-Vis spectrophotometry. The methanol extract of remek leaves contains flavonoids, triterpenoids/steroids and phenolic compound while the methanol extract of kratom leaves contains triterpenoids, flavonoids, alkaloids, saponins and phenolic. The combination of the two extracts gave the highest % inhibition in the 1:1 ratio. The IC50 values of methanol extracts of meat remek leaves, kratom leaves are 70.61; 33.43 ppm indicating antioxidant activity in the strong and very strong categories and the combination is 38.08 indicating the combination index is strong antagonis
PENENTUAN STATUS MUTU AIR MENGGUNAKAN METODE INDEKS PENCEMARAN PADA SUNGAI SANGA-SANGA Rahmadi, Mohammad Zulfian; Sitorus, Saibun; Pagoray, Henny; Widodo, Nanang Tri
JURNAL ATOMIK Vol 10 No 1 (2025)
Publisher : Jurusan Kimia FMIPA UNMUL

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/ja.v10i1.1417

Abstract

Pencemaran Sungai Sanga-Sanga dapat disebabkan oleh buangan sektor pemukiman maupun sektor industri pertambangan Penggunaan indeks kualitas air dapat mempermudah penentuan kualitas air sungai serta mempermudah juga dalam pemberian informasi kepada pihak yang membutuhkan. Tujuan penelitian ini adalah untuk mengkaji kualitas air Sungai Sanga-Sanga ditinjau dari parameter fisika, kimia dan biologi serta menentukan status mutu Sungai Sanga-Sanga dengan metode Indeks Pencemaran. Penelitian ini merupakan penelitian deskriptif kuantitatif yang bersifat ex-post facto dengan menggunakan metode Indeks Pencemaran untuk menentukan status mutu air Sungai Sanga-Sanga. Status mutu air Sungai Sanga-Sanga berdasarkan Indeks Pencemaran berada pada kondisi tercemar ringan.
PENGARUH WAKTU PENYANGRAIAN TERHADAP AKTIVITAS ANTIOKSIDAN PADA KOPI DARI BIJI KURMA (Phoenix dactylifera L.) Yana, Yuli; Ulfa, Elis Diana; Nandita, Septika Tri
JURNAL ATOMIK Vol 10 No 1 (2025)
Publisher : Jurusan Kimia FMIPA UNMUL

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/ja.v10i1.1488

Abstract

Biji kurma biasanya dibuang sebagai limbah yang tidak termanfaatkan. Berdasarkan hasil survey kurma merk Golden Valley merupakan kurma yang banyak digemari masyarakat. Aktivitas antioksidan pada biji kurma dapat dimanfaatkan sebagai kopi non-kafein. Penelitian ini bertujuan untuk mengetahui potensi biji kurma sebagai kopi yang kaya akan antioksidan dengan variasi waktu dan massa pada proses penyangraian. Pada penelitian ini biji kurma yang digunakan sebanyak 200 gram dan dilakukan variasi waktu dan massa penyangraian yang berbeda-beda yaitu 30, 45, & 60 menit. Ekstrak kopi biji kurma kemudian dianalisis kandungan senyawa fitokimia dan aktivitas antioksidannya menggunakan metode DPPH. Hasil penelitian fitokimia menunjukkan bahwa ekstrak kopi biji kurma memiliki senyawa metabolit sekunder golongan triterpenoid, fenolik, flavonoid, dan tanin. Hasil penelitian menunjukkan bahwa waktu penyangraian berpengaruh terhadap aktivitas antioksidan ekstrak kopi biji kurma. Semakin lama waktu penyangraian semakin tinggi aktivitas antioksidan ekstrak kopi biji kurma. Hasil penelitian menunjukkan kopi biji kurma dengan waktu penyangraian 60 menit memiliki nilai IC50 sebesar 21,715 ppm yang termasuk dalam kategori antioksidan sangat kuat. Hasil uji panelis menunjukkan tingkat kesukaan tertinggi yaitu 85,5% pada sampel kopi biji kurma dengan waktu penyangraian 60 menit.
AKTIVITAS ANTI-Staphylococcal SECARA IN VITRO EKSTRAK DIKLOROMETANA DARI RIMPANG TEMU KUNCI (Boesenbergia rotunda) TERHADAP Staphylococcus aureus ATCC 25923 Matutu, Deni Ari; Hairani, Rita; Ruga, Ritbey
JURNAL ATOMIK Vol 10 No 1 (2025)
Publisher : Jurusan Kimia FMIPA UNMUL

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/ja.v10i1.1404

Abstract

The rhizome of temu kunci (Boesenbergia rotunda) is one of the plants used by the local people in Indonesia as a traditional medicine. This study aimed to identify the secondary metabolite compounds contained in the dichloromethane extract with phytochemical screening and investigate its antibacterial activity against test bacteria Staphylococcus aureus ATTC 25923 was carried out by agar diffusion method with modification where tetracycline as a positive control and ethanol as a negative control. The phytochemical screening showed the dichloromethane extract contains secondary metabolites such as alkaloids, flavonoids, phenolics and triterpenoids. With 1 mg/mL of dichloromethane extract revealed its antibacterial activity against S. aureus with inhibitory zone value of 15.0 ± 0.0 mm while its MIC value of the extract was 0.031 ± 0.0 mg/mL toward of tested bacteria. In addition, tetracycline as a positive control at 0.5 μg/mL exhibited its antibacterial potential with an inhibitory zone value of 22.0 ± 0.0 mm and its MIC value of 0.016 ± 0.577 µg/mL.
ADSORPSI ION LOGAM Pb2+ DENGAN ARANG AKTIF MAHKOTA NANAS (Ananas comosus (L.) Merr) TERMODIFIKASI KITOSAN Arsyakia, Tarisa; Koesnarpadi, Soerja; Lianasari, Ika Yekti
JURNAL ATOMIK Vol 10 No 1 (2025)
Publisher : Jurusan Kimia FMIPA UNMUL

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/ja.v10i1.1436

Abstract

Pineapple (Ananas comosus (L.) Merr) is one of the most widely produced plants in Indonesia. Pineapple crown can be classified as solid waste that has an impact on the environment. Another problem of environmental pollution is heavy metals such as lead. In this study, modification was carried out by adding chitosan to the activated charcoal prepared from pineapple crown powder waste. The purpose of this study was to determine the characterization of chitosan-modified pineapple crown activated charcoal using Fourier Transform Infrared (FTIR) and Scanning Electron Microscopy (SEM), determine the optimum adsorption conditions based on variations in pH, contact time and concentration of Pb2+ metal and determine the percent absorption and adsorption capacity. The results of FT-IR characterization of pineapple crown charcoal, chitosan and chitosan-modified activated charcoal indicated the presence of O-H (streching), N-H, C-H (streching), C=C aromatic and C-H (bending) groups, and in pineapple crown charcoal and chitosan-modified pineapple crown activated charcoal also indicated C-O-C groups while chitosan indicated C-N groups. In the results of SEM characterization, pineapple crown charcoal has a smooth, chitosan has a rough and chitosan-modified activated charcoal has a slightly rough surface and is still tightly bound to each other. The optimum conditions for adsorption of chitosan-modified activated charcoal on Pb2+ metal ions at pH 4 with a contact time of 60 minutes and a concentration of 75 mg/L. The results of the adsorption capacity test at each pH variation, contact time and concentration of Pb2+ metal ions were 2.4154 mg/g, 14,89 mg/g and 15,1732 mg/g.
ELEKTRODEKOLORISASI LIMBAH CAIR INDUSTRI SARUNG TENUN SAMARINDA MENGGUNAKAN ELEKTRODA PbO2/Pb DARI AKI BEKAS Ramadani, Desi Fidyah; Wirawan, Teguh; Widodo, Nanang Tri
JURNAL ATOMIK Vol 10 No 1 (2025)
Publisher : Jurusan Kimia FMIPA UNMUL

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/ja.v10i1.1413

Abstract

Electrodecolorization of liquid waste from the Samarinda woven sarong industry using PbO2/Pb electrode has been conducted. The purpose of this study was to decolorize woven sarong wastewater samples using the electrodecolorization method using lead dioxide (PbO2) as the anode and lead (Pb) as the cathode. Electrodecolorization is carried out by varying working potential, Na2SO4 electrolyte concentration, time and electrode distance. The dye concentration was determined using a UV-Vis spectrophotometer. The research results showed that the optimum conditions for electrodecolorization of woven sarong wastewater samples were using PbO2/Pb electrodes, namely with a working potential of 6 volts, a Na2SO4 electrolyte concentration of 0.25 M, a time of 60 minutes, and a distance of 1 cm. The percentage of decolorization of Samarinda woven sarong wastewater samples using PbO2/Pb electrodes, at maximum conditions was 98,75%.
ADSORPSI ZAT WARNA DIREK HITAM MENGGUNAKAN ARANG AKTIF DARI MAHKOTA NANAS (Ananas comosus (L) Merr) TERMODIFIKASI KITOSAN Putri, Raisya Karina; Yusuf, Bohari; Widodo, Nanang Tri
JURNAL ATOMIK Vol 10 No 1 (2025)
Publisher : Jurusan Kimia FMIPA UNMUL

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/ja.v10i1.1433

Abstract

Consumption of pineapple fruit (Ananas comosus (L) Merr) results in solid waste of about 45-65%, especially the pineapple crown. On the other hand, the textile industry uses dyes such as recolors that can cause pollution in the aquatic environment. This study aims to use activated charcoal from chitosan-modified pineapple crown as an adsorbent for direct dyes. The steps taken are characterizing activated charcoal, chitosan and chitosan-modified activated charcoal using Fourier Transform Infrared (FT-IR) and Scanning Electron Microscopy (SEM), optimizing with variations in mass, contact time and pH, and determining the maximum adsorption capacity. Preparation of pineapple crown activated charcoal carbonated at 400oC for 1 hour. Activated using 2% NaOH and then modified with chitosan. The chitosan-modified pineapple crown activated charcoal was used to adsorb the dye direct black and analyzed using a UV-Vis spectrophotometer. The results of FT-IR characterization of pineapple crown activated charcoal, chitosan and chitosan-modified pineapple crown activated charcoal indicated the presence of O-H, C-H (stretching), C=O and C-H (bending) groups, and in chitosan and chitosan-modified activated charcoal also indicated the appearance of overlapping N-H (amine), C-N (amide) and C-O-C groups. The results of SEM characterization of pineapple crown activated charcoal show that the surface has a smooth texture, chitosan has a rough and irregular texture surface and chitosan-modified pineapple crown activated charcoal has small clumps of various sizes and shapes. The results of the optimum conditions of adsorption of chitosan-modified pineapple crown activated charcoal on black rec dye occurred at a mass of 0.25 grams, contact time for 20 minutes and pH 7 with a maximum adsorption capacity of 11,6472 mg/g following the Langmuir isotherm.

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