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All Journal Proceeding Seminar LPPM UMP Tahun 2014 KOVALEN: Jurnal Riset Kimia Chemistry Indonesian Journal of Chemical Research Hydrogen: Jurnal Kependidikan Kimia Hydrogen: Jurnal Kependidikan Kimia Jurnal Inovasi Pengabdian Masyarakat Pendidikan
Laily Nurliana
Program Studi Pendidikan Bahasa dan Sastra Indonesia, Fakultas Keguruan dan Ilmu Pendidikan, Universitas Muhammadiyah Purwokerto Jl Raya Dukuh Waluh, PO BOX 202 Purwokerto 53182 Telp. (0281) 636751 ext 230
Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Education Engineering Environmental Science Social Sciences Other

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The Synthesis of Methyl Ester Nitrate from Ketapang Seed Oil (Terminalia catappa L.) Nurliana, Laily; Ritonga, Halimahtussaddiyah; Feronika, Yulita; Musta, Rustam
Hydrogen: Jurnal Kependidikan Kimia Vol. 12 No. 6 (2024): December 2024
Publisher : Universitas Pendidikan Mandalika

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33394/hjkk.v12i6.13537

Abstract

The synthesis of methyl ester nitrate (MEN) from ketapang oil (Terminalia catappa L.) have been carried out. This study aims to determine the yield and the characteristics of MEN. In this study, ketapang seed oil was obtained from the soxhlet extraction process followed by an evaporation process to separate the oil from the solvent. MEN can be produced from ketapang seed oil by esterification to convert all of FFA became ester, followed by transesterification that intended to produce ester from triglycerides and nitrationthat is reaction of esther and HNO3 to create MEN. Evaporated oil is esterified using methanol with a mole ratio of oil: methanol (1: 6), then the transesterification process using methanol with a mole ratio (1:15) gives a yield of 86%. The transesterification product was then nitrated using HNO3 and H2SO4 for 4 hours with a yield of 83%. Characterization of methyl ester using GC-MS characterization showed the presence of methyl palmitoleate (C17H32O2), methyl palmitate (C19H34O2), methyl oleate (C19H36O2), methyl 13-octadecanoic (C19H36O2), methyl stearate (C19H38O2), and methyl 18-nonadecanoic (C21H42O2). Characterization MEN using a FTIR spectrophotometer showed the presence of a C-ONO2 group at wave number 1550 cm-1, NO2 group at wave number 1365 cm-1 and a C-N group at wave number 1118 cm-1. It shows that MEN can be synthesized from ketapang seed oil.
Identifikasi dan Uji Aktivitas Antioksidan Senyawa Metabolit Sekunder Ekstrak Tanaman Cleome viscosa L: Identification and Antioxidants Activity Tests of Secondary Metabolite Compounds of Clome viscosa L. Plant Extracts Imran; Nurliana, Laily; Natsir, Muh.; Nohong; Kadir, La Ode Abd; Rudi, La; Ruslan; Azis, Thamrin
KOVALEN: Jurnal Riset Kimia Vol. 9 No. 1 (2023): April Edition
Publisher : Chemistry Department, Mathematics and Natural Science Faculty, Tadulako University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/kovalen.2023.v9.i1.16340

Abstract

Cleome viscosa L. has been used empirically by people on the island to treat diseases that have clinical symptoms such as malaria (fever, sweating, chills, and muscle aches). The purpose of this study was to determine the class of secondary metabolites and antioxidant activity. The extraction was carried out using the maceration method, while the fractionation was carried out using the separating funnel. The secondary metabolites found in the Cleome viscosa L. plant extract are alkaloids, flavonoids, steroids, terpenoids, tannins, and saponins. Antioxidant test conducted by DPPH method showed that the positive control of ascorbic acid and methanol extract obtained IC50 values of 3.86 ppm and 37.4 ppm, respectively.
Co-Authors Andraysno, Andraysno Astam, Amal Desy Kurniawati Feronika, Yulita Halulanga, Muh. Mahatir Imran Imran Imran Kadir, La Ode Abd La Ode Kadidae, La Ode La Rudi Muh. Natsir, Muh. Musta, Rustam Nohong Nursin, Nursin Risnawaty Risnawaty Ritonga, Halimahtussaddiyah Ritonga, Halimatussaddiyah Ruslan Sabarwati, Sitti Hadijah Siti Fathonah THAMRIN AZIS