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All Journal Natural Science: Journal of Science and Technology KOVALEN: Jurnal Riset Kimia JKPK (Jurnal Kimia dan Pendidikan Kimia) KAIBON ABHINAYA : JURNAL PENGABDIAN MASYARAKAT Jurnal ABDINUS : Jurnal Pengabdian Nusantara Jurnal Riset Sains dan Kimia Terapan
Husain Sosidi
Analytical Chemistry, Chemistry Department, Tadulako University
Humanities Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Economics, Econometrics & Finance Education Environmental Science Industrial & Manufacturing Engineering

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Adsorbsi Ion Logam Cu (II) Menggunakan Biomassa Daun Genjer (Limnocharis flava): Adsorption of Cu (II) Ions by Biomass of Genjer Leaves (Limnocharis flava) Helni Febriani; Dwi Juli Puspitasari; Ruslan; Husain Sosidi
KOVALEN: Jurnal Riset Kimia Vol. 7 No. 2 (2021): Edisi Agustus
Publisher : Chemistry Department, Mathematics and Natural Science Faculty, Tadulako University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/kovalen.2021.v7.i2.14009

Abstract

The adsorption of Cu (II) ions by Genjer (Limnocharis flava) biomass has been carried out. This research aims to determine the optimum pH of the plant and the contact time between the metal ion Cu (II) with the plant that produces the highest absorption, as well as knowing the best adsorbent mass for absorption between Cu (II) metal ions and genjer plants. The study used a completely randomized design (CRD) with variables of pH, contact time, and adsorbent mass. The testing of the absorption of the Genjer leaves biomass against Cu (II) was carried out with Atomic Adsorption Spectrophotometric (AAS). The results showed that the optimum absorption produced was 83.34% at pH 4, and 91.54% with the highest contact time of 30 minutes, and 82.04% with an adsorbent mass of 1 gram. Keywords: Limnocharis flava, pH, contact time, adsorbent mass, adsorption, Cu (II) ion
Pembuatan Konsentrat Protein Ampas Kelapa (Cocos nucifera L.) Bebas Lemak pada Berbagai Konsentrasi NaOH: Production of Fat-Free Coconut Pulp (Cocos nucifera L.) Protein Concentrates at Various NaOH Concentrations Ulayya Kasio; Syaiful Bahri; Husain Sosidi; Khairuddin; Ni Ketut Sumarni; Ahmad Ridhay
KOVALEN: Jurnal Riset Kimia Vol. 7 No. 3 (2021): Edisi Desember
Publisher : Chemistry Department, Mathematics and Natural Science Faculty, Tadulako University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/kovalen.2021.v7.i3.14235

Abstract

Coconut pulp contains up to 18.2% protein which is one of the wastes from coconut oil processing. Protein from coconut pulp can be used in the manufacture of protein concentrates which are widely used in the food industry. The purpose of this research is to determine the concentration of NaOH that can produce the yield and protein content of coconut pulp protein concentrate. Coconut pulp protein was extracted with NaOH at various concentrations of 0.5, 1, 1.5, 2, and 2.5 M, then continued with salting out using salt (NH4)2SO4 with a saturation of 65%. The crude protein content of coconut pulp protein concentrate was determined by the Kjeldahl method. The results showed that the use of 0.5 M NaOH resulted in the highest protein content of coconut pulp protein concentrate, which was 71.30% with a yield of 14.42%.
Penggunaan Karbon Aktif dari Tandan Kosong Kelapa Sawit Teraktivasi NaOH pada Penyerapan Ion Pb(II): Utilization of NaOH-Activated Carbon from Oil Palm Empty Fruit Bunches on Pb(II) Ion Absorption Minda M; Husain Sosidi; Ni Ketut Sumarni; Hardi Ys.; Ruslan; Nov Irmawati Inda; Moh. Mirzan
KOVALEN: Jurnal Riset Kimia Vol. 8 No. 1 (2022): April Edition
Publisher : Chemistry Department, Mathematics and Natural Science Faculty, Tadulako University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/kovalen.2022.v8.i1.15847

Abstract

Oil palm empty fruit bunches (OPEFB) are plantation waste that has the potential to be used as activated carbon. The main component of OPEFB is lignocellulosic which can be a source of activated carbon and utilized for Pb2+ ion adsorption. The use of activated carbon activated by NaOH still requires optimization, especially in determining the contact time and optimum adsorption pH. This study aims to determine the effect of pH and contact time on the adsorption of Pb2+ and to determine the efficiency of the adsorbent on the adsorption of Pb2+. In this study, activated carbon from OPEFB was carbonized at 300oC for 1 hour, followed by activation using NaOH 0.5%. The results showed that the use of pH 5 and a contact time of 90 minutes had a relatively higher Pb2+ adsorption than other conditions. However, the use of variations in pH and contact time had no significant effect on the adsorption of Pb2+ ions. Adsorbents with variations in pH 4, 5, 6, 7, and 8 were able to absorb Pb2+ of 99.73%, 99.86%, 99.74%, 99.79%, and 99.80%, respectively. Adsorbents with variations in contact time of 30, 60, 90, 120, and 150 minutes were able to absorb Pb2+ of 99.28%, 99.40%, 99.48%, 99.44%, and 99.48%, respectively.
Penurunan Kadar Chemical Oxygen Demand (COD) pada Limbah Cair Industri Tahu Menggunakan Arang Aktif dari Pelepah Kelapa Sawit (Elaeis guenensis Jacq.) : Reducing Chemical Oxygen Demand (COD) Levels in Tofu Industrial Liquid Waste Using Activated Charcoal from Palm Oil (Elaeis guenensis Jacq.) Mid-ribs Khairuddin; Ruslan Ruslan; Muh.Ricky Arisandi M. Tahili; Dwi Juli Puspitasari; Indriani; Husain Sosidi; Prismawiryanti; Moh. Mirzan
KOVALEN: Jurnal Riset Kimia Vol. 8 No. 2 (2022): August Edition
Publisher : Chemistry Department, Mathematics and Natural Science Faculty, Tadulako University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/kovalen.2022.v8.i2.15966

Abstract

Oil palm midribs (Elaeis guenensis Jacq.) are one of the wastes from oil palm plantations. The high carbon element composition in the palm midribs has the potential to be used as charcoal or activated carbon. Activated carbon can reduce COD levels in tofu industrial wastewater. This study aims to determine the effect of activated carbon mass and contact time on decreasing COD levels in tofu industrial wastewater. Palm midrib charcoal was activated using HCl 1N with the independent variable of activated charcoal mass (1, 3, 5, 7, and 9 grams) and contact times (30, 60, 90, 120, and 150 minutes), while the dependent variable was the percentage decrease COD levels. Activated charcoal from the palm midribs was in accordance with SNI 06-3730-1995 concerning the Quality Standard of Activated Charcoal. The effect of the adsorbent mass showed that the mass increase in activated charcoal was directly proportional to the percentage decrease in COD levels in the tofu industrial wastewater, while the optimum contact time of activated charcoal was obtained at 60 minutes with a decrease in COD levels of 82.13%.
Analisis Kadar Kadmium (Cd) dalam Bawang Merah Lokal Palu (Allium cepa L. var. aggregatum) pada Berbagai Lokasi dan Umur Tanam: Analysis of Cadmium (Cd) in Palu Local Shallots (Allium cepa L. var. aggregatum) at Various Locations and Planting Ages Eka Lindawati; Khairuddin Khairuddin; Nurhaeni; Ruslan; Ahmad Ridhay; Husain Sosidi; Erwin Abdul Rahim; Syamsuddin
KOVALEN: Jurnal Riset Kimia Vol. 9 No. 1 (2023): April Edition
Publisher : Chemistry Department, Mathematics and Natural Science Faculty, Tadulako University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/kovalen.2023.v9.i1.16287

Abstract

The local Palu shallot (Allium cepa L. var. aggregatum) plant is one of the leading products in the Central Sulawesi region. Shallots can experience a decrease in quality if they are contaminated with heavy metals, such as cadmium (Cd) in amounts that exceed the threshold. This study aims to determine the effect of planting age on cadmium levels in local Palu shallots cultivated in Oloboju Village and Solove Village, Biromaru District, Sigi Regency. The research variables used were the planting age which consisted of 4 levels (age 40, 50, 60, and 70 days), and the planting location which consisted of 2 levels (Solove Village and Oloboju Village). Cd levels were analyzed using an Atomic Absorption Spectrophotometer (AAS). Cadmium levels in shallot roots at two planting locations decreased with increasing planting age, from 101.34 - 107.18 mg/kg at 40 days of age to 1.68-3.78 mg/kg at 70 days of age. Shallot bulbs at two locations had lower cadmium levels than roots, namely 0.01-0.04 mg/kg. The results of the study found that planting time had a significant effect on cadmium levels in the roots of shallots, but planting age and planting location had no significant effect on cadmium levels in local Palu shallot bulbs with levels that met the SNI (Indonesian national standard) quality requirements
Isotermal Adsorpsi Ion Tembaga (II) Menggunakan Arang Tongkol Jagung (Zea mays L.) Teraktivasi Kalium Permanganat: Isothermal Adsorption of Copper (II) Ions Using Charcoal from Corn Cobs (Zea mays L.) Activated by Potassium Permanganate Lisma Habiba; Nov Irmawati Inda; Prismawiryanti; Husain Sosidi; Ni Ketut Sumarni; Dwi Juli Puspitasari; Moh. Mirzan; Jusman
KOVALEN: Jurnal Riset Kimia Vol. 9 No. 1 (2023): April Edition
Publisher : Chemistry Department, Mathematics and Natural Science Faculty, Tadulako University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/kovalen.2023.v9.i1.16292

Abstract

Corn cobs which generally only become waste can be processed into activated carbon and used for the absorption of heavy metals, such as copper(II) ions. This study aims to determine the morphology of corn cobs charcoal after activation, determine the isothermal adsorption model of copper (II) metal ions on corncob-activated carbon, and then determine the adsorption capacity of copper (II) metal ions on corncob-activated carbon. The morphology of the corncob-activated charcoal obtained was analyzed using Scanning Electron Microscopy (SEM). Isothermal adsorption of copper (II) ions was carried out with various concentrations of copper (II) ions of 5, 10, 20, 50, and 100 ppm. The results of the analysis using SEM showed that the surface shape of the corncob-activated charcoal is regular and has pores with a pore diameter obtained in the range between 1.08-1.26 m and 1.38-1.59 m. The mechanism of adsorption of copper (II) ions by corncob-activated charcoal using KMnO4, following the Freundlich isothermal model with a value of R2 0.9993 with an adsorption capacity of 51 x 10-4 mmol/L. The utilization of activated carbon from corn cobs that are activated by potassium permanganate is very effective for adsorbing copper metal ion pollutants through an adsorption mechanism on the surface of activated carbon.
Pengelolaan Alat-Alat dan Bahan Kimia Laboratorium IPA SMA di MGMP Kimia Kabupaten Donggala : Pengelolaan Alat-Alat dan Bahan Kimia Laboratorium IPA SMA di MGMP Kimia Kabupaten Donggala Dwi Juli Puspitasari; husain Sosidi; prismawiryanti prismawiryanti
KAIBON ABHINAYA : JURNAL PENGABDIAN MASYARAKAT Vol. 5 No. 2 (2023)
Publisher : Universitas Serang Raya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30656/ka.v5i2.5698

Abstract

One of the problems that often arise in the world of education is the lack of learning resources, educational facilities and their use in assisting the learning process. The teacher's lack of knowledge in the use, maintenance and storage of equipment and chemicals makes the laboratory not utilized as a learning resource. The purpose of this service is to provide knowledge and skills to chemistry teachers regarding the management of chemical equipment and materials at the chemistry MGMP in Donggala district a. Community service activities were carried out at the MGMP Chemistry SMA Donggala Regency. Service activities are carried out by understanding of the provision of material regarding the management of equipment and chemicals, then followed by material on safety and work safety in the laboratory. Furthermore, carrying out field practice in the chemical laboratory in the form of guidance and assistance in the management of chemical equipment and materials. This activity is expected to increase understanding in chemistry learning as well as an increase in teacher quality which has a positive impact on improving student achievement.
Sintesis dan Karakterisasi Polivinil Alkohol (PVA) Terlapis Polieugenol: Synthesis And Characterization of Polyvinyl Alcohol (PVA) Coated with Polyeugenol Rahim, Erwin Abdul; Ridhay, Ahmad; Sitti Nur Halizah; Indriani; Sosidi, Husain; Khairuddin; Inda, Nov Irmawati; Nurakhirawati; Mirzan, Moh.; Amar, Aini Auliana
KOVALEN: Jurnal Riset Kimia Vol. 10 No. 1 (2024): April Edition
Publisher : Chemistry Department, Mathematics and Natural Science Faculty, Tadulako University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/kovalen.2024.v10.i1.17088

Abstract

A study has been conducted on materials containing polyvinyl alcohol (PVA) coated with poly eugenol. This research aims to explore the synthesis process and properties of PVA coated with poly eugenol. Characterization of PVA includes tensile strength measurement and surface observation using SEM. Additionally, the antioxidant activity of PVA was also tested using the DPPH method. In this study, PVA films were obtained by dissolving PVA in a water solvent. The characterization results indicate that the tensile strength ranges from 25.56 to 271.10 Mpa, elongation reaches 315.20 to 320%, and the young modulus ranges from 4.05 to 6.27 Mpa. Surface observation with SEM shows a smooth surface without pores. The antioxidant activity test shows IC50 values ranging from 84.11 to 175.37 ppm.
Spesiasi dan Bioavailabilitas Merkuri dalam Sedimen Teluk Palu Pasca Gempa dan Tsunami dengan Metode Diffusive Gradient in Thin Film (DGT): Speciation and Bioavailability of Mercury in Palu Bay Sediments Post Earthquake and Tsunami Using the Diffusive Gradient in Thin Film (DGT) Method Sosidi, Husain; Khairuddin; Dwiyana, Putri; Ruslan, Ruslan
KOVALEN: Jurnal Riset Kimia Vol. 10 No. 2 (2024): August Edition
Publisher : Chemistry Department, Mathematics and Natural Science Faculty, Tadulako University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/kovalen.2024.v10.i2.17264

Abstract

Speciation and bioavailability of mercury in the sediments of Palu Bay after the earthquake and tsunami were conducted using fractionation and Diffusion Gradient in Thin Films (DGT). This method has been conducted using sediment samples from the estuary of the Pondo River, Palu. Heavy metal speciation of mercury ions was conducted by looking at the distribution of mercury ions in various species by sequential extraction and heavy metal bioavailability of mercury ions. This method was conducted by looking at the migration of mercury ions from sediments into the seawaters using a Diffusive Gradient in Thin Films (DGT). The speciation of mercury ions concentration with sequential extraction as EFLE (easily, freely, leachable, exchangeable) fraction is about < 0.0005 ppm, the oxidizable fraction is about < 0.0005 ppm and the resistant fraction is between < 0.0005 ppm to 0.0063 ppm. The results of DGT experiments to study the migration of mercury ions from sediments into the seawaters during 3 days of immersion is between 0.01003 ppm and 0.01748 ppm. The availability of mercury ions concentration in the sediments allows for the migration of mercury ions into water.
Studi Variasi Suhu dan Kosentrasi Larutan Asam Sitrat terhadap Karakteristik Silika Daun Tebu menggunakan Metode Leaching Abustiana, Rahma Lolita; Mirzan, Muhamad; Sosidi, Husain; Khairuddin; Ridhay, Ahmad; Jusman
Jurnal Riset Sains dan Kimia Terapan Vol. 11 No. 1 (2025): Jurnal Riset Sains dan Kimia Terapan, Volume 11 Nomor 1, Juni 2025
Publisher : Program Studi Kimia Universitas Negeri Jakarta

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21009/JRSKT.111.04

Abstract

Telah dilakukan penelitian tentang studi variasi suhu dan konsentrasi larutan asam sitrat terhadap karakteristik silika daun tebu menggunakan metode leaching dengan 3 variasi suhu 60ºC, 80ºC, 100ºC dan 3 variasi konsentrasi 8%, 10%, 12%. Metode yang dilakukan ialah preparasi daun tebu, sintesis silika daun tebu menggunakan metode leaching dengan asam sitrat, dan pembakaran daun tebu hasil leaching asam sitrat. Pengujian dilakukan untuk memperoleh silika murni. Tujuan dari penelitian ini adalah untuk mengetahui variasi suhu dan konsentrasi larutan asam sitrat terhadap karakteristik silika daun tebu yang diperoleh dengan metode leaching. Hasil penelitian diperoleh 3 analisis yaitu, untuk analisis XRD menunjukan didapatnya hasil struktur silika yang masih amorf. Analisis FTIR menunjukan gugus fungsi yang terbentuk yaitu -OH, Si-O-Si dan Si-O. Analisis SEM menunjukan bahwa semakin tinggi suhu leaching yang diberikan terhadap sampel maka ukuran butir semakin merata.
Co-Authors Abd. Rahman Abustiana, Rahma Lolita Ahmad Ridhay Aini Auliana Amar Arianto Buchari Buchari Darmawati Darmawati Dwi Juli Puspitasari Dwi Juli Pusptasari Dwi Juli Pusptasari Dwiyana, Putri Eka Lindawati Erwin Abdul Rahim Fitra Langgeng Mangesti Hardi Ys. Helni Febriani Indra Noviandri Indriani Indriani Jusman Jusman, Jusman Khairuddin Khairuddin Khairuddin Krisma Meylin Lasampa Lisma Habiba Minda M Mirzan, Muhamad Moh. Mirzan Moh. Mirzan Moh. Rifki Saputra Muh.Ricky Arisandi M. Tahili Musafira Musafira Ni Ketut Sumarni Nov Irmawati Inda Nurakhirawati Nurhaeni Prismawiryanti Prismawiryanti Ramli, Aksar Ruslan Ruslan Ruslan Ruslan Ruslan Sitti Nur Halizah Sutomo Eka Putra Syaiful Bahri Syamsuddin Syamsuddin Ulayya Kasio Wiranto Wengkau Yul Uca Sali Putri