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All Journal Jurnal Pengajaran MIPA AGRIVITA, Journal of Agricultural Science Unnes Science Education Journal Indonesian Journal of Chemistry Diklabio: Jurnal Pendidikan dan Pembelajaran Biologi Canrea Journal: Food Technology, Nutritions, and Culinary Journal Journal of Vocational Education Studies (JOVES) Didaktika: Jurnal Kependidikan Jurnal Pengabdian Isola IJIS Edu : Indonesian Journal of Integrated Science Education
Ratnaningsih Eko S.
Universitas Pendidikan Indonesia
Agriculture, Biological Sciences & Forestry Humanities Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Decision Sciences, Operations Research & Management Education Engineering Languange, Linguistic, Communication & Media Mathematics Social Sciences Other

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Journal : Jurnal Pengajaran MIPA

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SINTESIS 4,10,16,22-TETRAMETOKSIKALIKS[4]ARENA DARI MINYAK ADAS (Synthesis of 4,10,16,22-Tetramethoxycalix[4]Arene from Anise Oil) Sardjono, Ratnaningsih Eko
Jurnal Pengajaran MIPA Vol 2, No 1 (2001): JPMIPA: Volume 2, Issue 1, 2001
Publisher : Faculty of Mathematics and Science Education, Universitas Pendidikan Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.18269/jpmipa.v2i1.34900

Abstract

One kind of calixarenes, i.e. 4,10,16,22-tetramethoxycalix[4]arene (4), has been synthesized from anethole (1), which was isolated from anise oil. The synthesis of 4 was carried out via acid-catalyzed procedure. The reaction route consists of three stages, i.e. (i) oxidation of 1 with KMnO4 at 40oC for 15 minutes, (ii) reduction p-anisaldehyde (2) with NaBH4 at 76oC for 3 hours, and  (iii) cyclotetramerization of p-anisilalcohol (3) with AlCl3 at 20oC for 2 hours. Oxidation of 1 produced 2 in 77%, whereas reduction of 2 gave 3 in 55 %. The cyclotetramerization of 3 yielded 4 in 95 %.
Co-Authors Ade Elvia Ahmad Nur F. Ahmad Nur F. Ahmad Nur F. Amelinda Pratiwi Amelinda Pratiwi Asep Kadarohman Asep Kadarohman Asep Kadarohman Asep Suryatna Binar Kurnia Prahani Budiman Anwar Candrawati, Emilia Cecep Jaenudin Ede Kadarusman Ede Kadarusman Ede Kadarusman Emilia Candrawati Emilia Candrawati Fandi Ahmad Fitri Khoerunnisa Florentina Maria Titin Supriyanti Galuh Yuliani Gebi Dwiyanti Gebi Dwiyanti Gebi Dwiyanti Hokcu Suhanda Iis Rosliana Ijang Rohman Iqbal Musthapa Lela Lailatul K. Lela Lailatul K. Lela Lailatul K. Lusia Narsia Amsad MADE ASTAWAN Mellyta Uliyandari Uliyandari Mustapha, Iqbal Nenden Nataliawati Nia Kurniawati Nur Indah Sari Putri, Sastia Prama Rafidha Irdiani Ramdhani, Rizal Pauzan S, Liliasari Satwika Trianti Ngandoh Siti Aisyah Siti Aisyah Supriyanti, F.M Titin Tryas, Anisha Ayuning Tuszie Widyanti Tutik Wresdiyati Wahyu Sopandi Wawan Wahyu Wawan Wahyu Yendi Yusi Riksa Yustiana, Yusi Riksa