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Optimization Approach of Microwave Assisted Extraction Anthocyanins Pigments Butterfly Pea Flowoers (Clitoria Ternatea L.) Using OFAT (One-Factor-At-a-Time) Method Aththobarani, Muhammad Daffa'; Priyanto, Anugerah Dany; Putra, Andre Yusuf Trisna; Wicaksono, Luqman Agung; Erliyanti, Nove Kartika; Panjaitan, Renova; Pujiastuti, Caecilia; Triani, Nova
AGRITEPA: Jurnal Ilmu dan Teknologi Pertanian Vol 12 No 1 (2025)
Publisher : UNIVED Press, Dehasen University Bengkulu

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.37676/agritepa.v12i1.8268

Abstract

Optimization of anthocyanin pigment extraction from butterfly pea flowers (Clitoria ternatea L.) is an important focus to increase the efficiency of obtaining valuable active compounds. This study marks an initial approach in the application of Microwave-Assisted Extraction (MAE) using 0.75% aquadest-tartaric acid solvent, with the hope of producing more stable anthocyanins. The main objectives of this study were to identify the effect of the solvent-material ratio, extraction duration, and MAE power level on anthocyanin levels (mg/L) through the One-Factor-At-a-Time (OFAT) method. The results showed that the optimal treatment was obtained at condition P17, with a solvent-material ratio of 1:15, an extraction time of 15 minutes, and an MAE power of 450 watts, which produced an anthocyanin level of 33.89 ± 0.47 mg/L. These findings confirm that increasing the solvent-material ratio to the optimal point contributes to increasing anthocyanin recovery. However, excessive MAE time and power can cause pigment degradation. The optimal ratio variables were found to be in the range of 1:15 to 1:25, extraction time 9–15 minutes, and MAE power 270–450 watts. This study is expected to be the basis for further optimization using the Response Surface Methodology (RSM) method which allows for deeper analysis of the interactions between variables.
The Effectiveness of Sodium Hydroxide Precipitation in Impurity Removal during NaCl Recovery from Bittern Waste Water Puspitasari, Indah Maharani; Putra, Andreansyah Brilliant; Pujiastuti, Caecilia; Panjaitan, Renova
G-Tech: Jurnal Teknologi Terapan Vol 9 No 4 (2025): G-Tech, Vol. 9 No. 4 October 2025
Publisher : Universitas Islam Raden Rahmat, Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.70609/g-tech.v9i4.8082

Abstract

Recovery of sodium chloride (NaCl) from bittern, a by-product of salt production, is often hindered by impurities such as Mg²⁺ and Ca²⁺, which reduce NaCl purity. This study evaluated the effect of sodium hydroxide (NaOH) concentration and stirring time on NaCl recovery, using NaOH concentrations of 4.6 until 8.02 N and stirring durations of 20 until 60 minutes at a constant stirring speed of 300 rpm. The process involved NaOH addition, stirring, filtration of precipitates, and NaCl crystallization. Parameters such as impurity levels, pH, NaCl purity, and recovery percentage were analyzed. Results indicated that higher NaOH concentrations and longer stirring times generally decreased impurity levels and improved NaCl recovery. Optimal conditions 5.8 N NaOH and 50 minutes stirring yielded an impurity level of 0.0359%, NaCl purity of 89.61%, and a recovery rate of 85.57%. This study presents a novel approach by optimizing NaOH concentration and stirring time parameters to effectively minimize divalent ion contamination, thereby enhancing NaCl recovery from bittern. The findings have direct applicability in improving the efficiency of salt recovery processes in coastal salt industries, contributing to more sustainable salt production systems.
Penentuan Konstanta Isoterm Freundlich dan Kinetika Adsorpsi Karbon Aktif Terhadap Asam Asetat Setyorini, Dwi; Arninda, Andi; Syafaatullah, Achmad Qodim; Panjaitan, Renova
Eksergi Vol 20 No 3 (2023)
Publisher : Prodi Teknik Kimia, Fakultas Teknik Industri, UPN "Veteran" Yogyakarta

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31315/e.v20i3.10835

Abstract

Karbon aktif merupakan salah satu adsorben yang paling sering digunakan. Salah satu senyawa yang dapat diserap yaitu asam asetat. Untuk mengetahui kinerja adsoben lebih lanjut, maka diperlukan studi kinetika berdasarkan persamaan isotherm Freundlich. Isoterm Freundlich mampu menunjukkan jenis adsopsi apakah secara kimisorpsi atau fisisorpsi dan berlangsung secara multilayer. Studi kinetika pseudo first orde dan pseudo second orde dimaksudkan untuk mengetahui mekanisme dan karakteristik adsorpsi yang berlangsung. Penelitian ini bertujuan untuk mengetahui konstanta isotherm Freundlich dan kinetika adsorpsi karbon aktif terhadap asam asetat. Konsentrasi asam asetat yang digunakan untuk mengetahui konstanta freundlich yaitu 0,5M, 0,25M, 0,125M, 0,0625M, 0,03125M dengan lama waktu kontak selama 10 menit. Sedangkan kinetika adsorpsi dilakukan dengan menggunakan asam asetat yang berkonsentrasi 0,5 M dengan waktu adsorpsi 2 menit, 4 menit, 6 menit, 8 menit dan 10 menit. Kemudian filtrat di titrasi dengan NaOH 0,1N. Ukuran karbon aktif yang digunakan antara lain 180 mess, 420 mess dan 600 mess.  Data yang diperoleh dianalisis dengan persamaan freundlich, pseudo first orde dan pseudo second orde. Data analisis yang didapatkan nilai konstanta freundlich yaitu sebesar 50,00342 dan memenuhi kinetika orde dua yang artinya, proses adsorpsi dipengaruhi lebih dari satu faktor.
Pemanfaatan lahan tidur untuk budidaya serai wangi di Kosagrha Lestari Medokan Ayu Selatan, Rungkut Susilowati, Susilowati; Djarwatiningsih, Djarwatiningsih; Panjaitan, Renova; Putra, Sandy Buana; Wahyusi, Kindriari Nurma; Pujiastuti, Caecilia; Moenandar, Siswanto
SELAPARANG: Jurnal Pengabdian Masyarakat Berkemajuan Vol 8, No 1 (2024): March
Publisher : Universitas Muhammadiyah Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31764/jpmb.v8i1.21616

Abstract

AbstrakKeberadaan lahan tidur di daerah pemukiman dapat menjadi sumber permasalahan bagi warga karena menjadi sarang hewan liar yang tentunya mengganggu kenyamanan masyarakat setempat. Lahan tidur di wilayah Kosagrha Lestari merupakan lahan milik pemerintah kota yang telah lama terbengkalai, ditumbuhi oleh rerumputan liar serta penuh dengan sampah-sampah seperti sampah sisa bangunan, sampah plastik dan botol-botol. Tim Pengabdian kepada Masyarakat (PkM) dari Universitas Pembangunan Nasional “Veteran” Jawa Timur (UPNVJT), dalam program pengabdian kepada masyarakat, bekerjasama dengan Kelompok Tani Kosagrha Lestari memanfaatkan lahan tidur tersebut menjadi lahan budidaya tanaman serai wangi. Pendekatan program pengabdian yang dilakukan adalah melakukan aksi (action) yang kemudian diikuti dengan diskusi tanya jawab dalam forum resmi (talk show). Hasil dari pengabdian masyarakat dengan metode pendekatan yang dilakukan adalah bahwa masyarakat memiliki ketertarikan dan kepercayaan lebih terhadap program yang sebelumnya terbukti berhasil dilakukan. Teknik budidaya yang disarankan dapat diaplikasikan pada lahan tidur di Kosagrha dan menghasilkan lahan budidaya serai wangi yang tumbuh dengan baik. Kata kunci: lahan tidur; pupuk kandang; serai wangi; teknik budidaya Abstract Unused land in residential areas can be a problem source for residents because it becomes a nest for wild animals, which disturbs the local community's comfort. The idle land in the Kosagrha Lestari area, which belongs to the government, has been neglected for a long time, overgrown with weeds and full of rubbish such as building waste, plastic waste, and bottles. The community servise team of UPNVJT collaborated with the Kosagrha Lestari Farmers Group in a community service program, utilizing that idle land to become citronella cultivation land. The service program's approach was taking action followed by a question-and-answer discussion in an official forum (talk show). The results of this community service activity using the approach method were that the community had more interest and trust in a program with successful evidence. The cultivation technique suggested could be applied to the unused land in Kosagrha and generate a well-cultivated land of citronella. Keywords: unused land; manure; citronella; cultivation technique