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Journal : Jurnal Fisika Unand

Potensi Ekstrak Kulit Buah Naga Merah (Hylocereus polyrhizus) sebagai Bioreduktor Untuk Biosintesis Nanopartikel Hawa Aritma Sunarko Putri; Rahmi Oktarini; Syuaibatul Islamiyah; Sri Redjeki; Rachmad Ramadhan Yogaswara
Jurnal Fisika Unand Vol 13 No 4 (2024)
Publisher : Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jfu.13.4.497-503.2024

Abstract

One type of antioxidant that is usually found in plants such as fruit, skin, leaves, and others is flavonoids. In addition, flavonoids can be used for the formation of nanoparticles (NPs) as a bioreductor. The purpose of this study was to examine the utilization of red dragon fruit peel extract as a bioreductor in the synthesis of zinc oxide nanoparticles from zinc nitrate precursors using the biosynthesis method. Red dragon fruit peel was macerated to obtain flavonoids. Zinc nitrate was used as a precursor to make ZnO NPs. UV-VIS spectrophotometric analysis showed that the total flavonoids contained in the extract were 5.6 x 10-4 mg QE/g. By FTIR test, ZnO nanoparticles are known to contain OH groups characterized by a peak in the 3374.10 cm-1 region. XRD results show that ZnO nanoparticles have a hexagonal wurtzite shape. SEM-EDX results show that the ZnO nanoparticles formed have a size of 157-174 nm and contain the constituent composition of 69.41% zinc and 29.35% oxygen. ZnO nanoparticles have anticancer effects that can be used in anticancer drugs, which can efficiently suppress synergistic cytoxicity in leukemia cell lines under UV irradiation. 
Biosintesis Nanopartikel ZnO Menggunakan Ekstrak Daun Tanaman Jagung (Zea Mays L.) Adeningrum, Della Arista; Rosa, Aulia; Wahyusi, Kindriari Nurma; Yogaswara, Rachmad Ramadhan
Jurnal Fisika Unand Vol 14 No 2 (2025)
Publisher : Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jfu.14.2.160-166.2025

Abstract

ZnO nanoparticles can be synthesized using the biosynthesis method using corn plant leaf extract (Zea Mays L.) as a bioreductant. The aim of this research is to examine the effect of variations in Zinc Nitrate Hexahydrate precursor concentration and calcination temperature on the yield, as well as the characterization of ZnO nanoparticles. Corn plant leaves are extracted to obtain flavonoid compounds. The resulting extract is mixed with the precursor solution then calcined to obtain ZnO nanoparticles.  The highest yield was produced in a sample with a precursor concentration of 0.1M with a calcination temperature of 300˚ C of 22.6082%. SEM-EDX results on samples with a precursor concentration of 0.3 M and a calcination temperature of 700˚C show various particle morphologies and sizes of ZnO nanoparticles, namely 91 nm; 97 nm; 109 nm; 435nm; and 973 nm, and the composition of ZnO nanoparticles consists of 76.43% Zn atomic weight and 23.57% O ​​atomic weight. at a calcination temperature of 700˚ C shows a pure ZnO sample with an element composition of 80.3% Zn atomic weight and 19.7% O atomic weight. The size of the crystal diameter for XRD analysis on samples with a precursor concentration of 0.3M with calcination temperatures of 300 ˚C and 700˚ C were 40.8564 nm and 31.7203 nm, respectively. Both samples have the same crystal system, namely hexagonal zincite.
Sintesis Kristalin Selulosa Berbahan Limbah Pelepah Pisang Rahmawati, Ayu; Faidah, Lutfatin; Ramadhan Yogaswara, Rachmad
Jurnal Fisika Unand Vol 14 No 4 (2025)
Publisher : Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jfu.14.4.332-338.2025

Abstract

Nanocrystalline cellulose (CNC) was successfully synthesized from banana sheath waste and demonstrated promising potential for applications in biocomposites, sustainable materials, and biomedical fields. This study aimed to produce CNC through an environmentally friendly chemical process while investigating the effects of bleaching temperature and acid concentration on CNC yield and properties, in accordance with ISO/TS 20477:2017. The process involved delignification using 17% NaOH at 100°C for 1.5 hours to remove lignin, followed by bleaching with 10% H₂O₂ for 1.5 hours at various temperatures (70°C–90°C) to enhance cellulose purity. Acid hydrolysis using H₂SO₄ at concentrations of 10%–30% was conducted at 45°C for 40 minutes to break down amorphous regions and form nanocrystalline structures. Chesson-Datta analysis revealed cellulose, hemicellulose, and lignin contents of 80.32%, 5.257%, and 3.26%, respectively. Optimal conditions were found at 80°C bleaching temperature and 10% acid concentration, yielding 2.5606 g of CNC. SEM-EDX analysis showed smooth fibrous morphology with 63.55% carbon and 35.83% oxygen content, while XRD analysis indicated particle sizes ranging from 8.76 to 24.12 nm, with an average of 14.25 nm.
Potensi Ekstrak Kulit Buah Naga Merah (Hylocereus polyrhizus) sebagai Bioreduktor Untuk Biosintesis Nanopartikel Putri, Hawa Aritma Sunarko; Oktarini, Rahmi; Islamiyah, Syuaibatul; Redjeki, Sri; Yogaswara, Rachmad Ramadhan
Jurnal Fisika Unand Vol 13 No 4 (2024)
Publisher : Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jfu.13.4.497-503.2024

Abstract

One type of antioxidant that is usually found in plants such as fruit, skin, leaves, and others is flavonoids. In addition, flavonoids can be used for the formation of nanoparticles (NPs) as a bioreductor. The purpose of this study was to examine the utilization of red dragon fruit peel extract as a bioreductor in the synthesis of zinc oxide nanoparticles from zinc nitrate precursors using the biosynthesis method. Red dragon fruit peel was macerated to obtain flavonoids. Zinc nitrate was used as a precursor to make ZnO NPs. UV-VIS spectrophotometric analysis showed that the total flavonoids contained in the extract were 5.6 x 10-4 mg QE/g. By FTIR test, ZnO nanoparticles are known to contain OH groups characterized by a peak in the 3374.10 cm-1 region. XRD results show that ZnO nanoparticles have a hexagonal wurtzite shape. SEM-EDX results show that the ZnO nanoparticles formed have a size of 157-174 nm and contain the constituent composition of 69.41% zinc and 29.35% oxygen. ZnO nanoparticles have anticancer effects that can be used in anticancer drugs, which can efficiently suppress synergistic cytoxicity in leukemia cell lines under UV irradiation. 
Co-Authors A.R Yelvia Sunarti Achmad Chumaidi, Achmad Achmad Rizaldi Adeningrum, Della Arista Adrian Gunawan, Adrian Afida Kartika Sari Ahmad Rizky Safrudin Anggara, Ikhwan Rifki anggraini, putri anggraini Anita Karlina AR Yelvia Sunarti Ardiansyah, Mochammad Rifqi Awildan El Fath AYU RAHMAWATI Bambang Wahyudi Bellani Yunfa Winata Billah, Mu’tasim Billah, Mu’tasim Daud, Daud Dhining Ayu Elsa Rosyidah Eristya Maya Safitri Erliyanti, Nove Kartika Erwan Adi Saputro Faidah, Lutfatin Farha, Ayu Shafira Fariana, Nida Fransisca Asteria Nandra Febiola Hamzah Fansuri Handi Ramadhan Hawa Aritma Sunarko Putri Ibadurrahman, Muhammad Watsieq Jiwantara, Dhebby Mas Ketut Sumada Khairunnisa Khairunnisa Kindriari Nurma Wahyusi Kusumawati, Yuly L.Urip Widodo, Yohandrik Novel Karaman Laksminingsih, Arieanthi Luckyana Aini Luckyana Aini Mardiansyah, Yuda Eka Melita, Lusia Nada Merry Jhoe Stefanny Mohd Hafiz Dzarfan Othman Mohd Jumain Jalil Mu'tasim Billah Muhammad Ashfal Ashfiya Muhammad Hakam Muhammad, Fitrah Guna Mutasim Billah Mu’tasim Billah Nandini , Atika Naufal Alkautsar Maulana Nerissa Arviana Nerissa Arviana Ni Ketut Sari Nuha, Farhah Kamilatun Nuraini, Adila Silmi Nurul Widji Triana Oktarini, Rahmi Prihardani, Fitri Pusfitasari, Memik Dian Putri, Hawa Aritma Sunarko Rahmi Oktarini Rensa Arnas Yunarwan Reva Edra Nugraha Rieswana, Yuried Diilan Rina Yulianti Rohmad Taufiqi Romalawati, Meiswita Rosa, Aulia Sa'adah, Tantri Nailis Sani Shanti Larissa Silvana Dwi Nurherdiana Sintha Soraya Santi Sri Redjeki Sri Redjeki Suprihatin Suprihatin Susilowati Syafsir Akhlus Syuaibatul Islamiyah Tahan Aprijal Simamora Tantri Nailis Sa'adah Tikat Deri Agratiyan Tsabitah Nabilah Khairunnisa Wahyu Arif Dharmawan Yesi Nabila Zahro Herazi Zuhdi, Farhan Muhammad