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Indonesian Journal of Chemistry

ijc
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Published by Universitas Gadjah Mada

ISSN : 14119420 EISSN : 24601578 DOI : -

Core Subject : Science, Engineering,

Chemical Engineering, Chemistry & Bioengineering Chemistry

Indonesian Journal of Chemistry is an International, peer-reviewed, open access journal that publishes original research articles, review articles, as well as short communication in all areas of chemistry including applied chemistry. The journal is accredited by The Ministry of Research, Technology and Higher Education (RISTEKDIKTI) No : 21/E/KPT/2018 (in First Rank) and indexed in Scopus since 2012. Since 2018 (Volume 18), Indonesian Journal of Chemistry publish four issues (numbers) annually (February, May, August and November).

Arjuna Subject : -

Articles 1,981 Documents

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Synthesis and Characterization of Titania-Rice Husk Silica Composites as Photocatalyst Posman Manurung; Rudy Situmeang; Ediman Ginting; Indra Pardede
Indonesian Journal of Chemistry Vol 15, No 1 (2015)
Publisher : Universitas Gadjah Mada

This article describes the synthesis of titania-silica composites by a sol-gel method using a mixture of silica of rice husk and titanium butoxide sols. Microstructures were examined at calcination temperature in the range of 500 to 700 °C, with temperatures interval of 50 °C. The sintered catalysts were subsequently tested for photodegradation of methylene blue (MB) under ultraviolet and sunlight rays. Physical characteristics were analyzed using X-ray diffraction (XRD), scanning electron microscopy (SEM)/energy dispersive X-ray spectroscopy (EDS), and Brunauer-Emmett-Teller (BET). The XRD results did not show the presence of silica crystal phase in each sample. The results showed that the highest BET surface area of samples was obtained at the temperature of 650 °C. In sample calcined 500 °C, the activity of the catalyst on MB was relatively similar in both sunlight and ultraviolet rays.

Retracted-Enhanced X-Ray Absorption Property of Gold-Doped Single Wall Carbon Nanotube Alimin Alimin; Narsito Narsito; Indriana Kartini; Sri Juari Santosa
Indonesian Journal of Chemistry Vol 15, No 3 (2015)
Publisher : Universitas Gadjah Mada

Enhanced X-ray absorption property of single wall carbon nanotube (SWCNT) through gold (Au) doping (Au@SWCNT) has been studied. Mass attenuation coefficient of SWCNT increased 5.2-fold after Au doping treatment. The use of ethanol in the liquid phase adsorption could produce Au nanoparticles as confirmed by the X-ray Diffraction (XRD) patterns. The possibility of gold nanoparticles encapsulated in the internal tube space of SWCNT was observed by transmission electron microscope technique. A significant decrease of nitrogen uptakes and upshifts of Radial Breathing Mode (RBM) of Au@SWCNT specimen suggest that the nanoparticles might be encapsulated in the internal tube spaces of the nanotube. In addition, a decrease intensity of XRD pattern of Au@SWCNT at around 2θ ≈ 2.6° supports the suggestion that Au nanoparticles are really encapsulated into SWCNT.

Theoretical Study on the Extraction of Alkaline Earth Salts by 18-Crown-6: Roles of Counterions, Solvent Types and Extraction Temperatures Saprizal Hadisaputra; Lorenz R Canaval; Harno Dwi Pranowo; Ria Armunanto
Indonesian Journal of Chemistry Vol 14, No 2 (2014)
Publisher : Universitas Gadjah Mada

The roles of counterions, solvent types and extraction temperatures on the selectivity of 18-crown-6 (L) toward alkaline earth salts MX2 (M = Ca, Sr, Ba; X = Cl-, NO3-) have been studied by density functional method at B3LYP level of theory in gas and solvent phase. In gas phase, the chloride anion Cl- is the preference counterion than nitrate anion NO3-. This result is confirmed by the interaction energies, the second order interaction energies, charge transfers, energy difference between HOMO-LUMO and electrostatic potential maps. The presence of solvent reversed the gas phase trend. It is found that NO3- is the preference counterion in solvent phase. The calculated free energies demonstrate that the solvent types strongly change the strength of the complex formation. The free energies are exothermic in polar solvent while for the non polar solvent the free energies are endothermic. As the temperature changes the free energies also vary where the higher the temperatures the lower the free energy values. The calculated free energies are correlated well with the experimental stability constants. This theoretical study would have a strong contribution in planning the experimental conditions in terms of the preference counterions, solvent types and optimum extraction temperatures.

CHEMICALLY CHITOSAN MODIFIED WITH METHYL METHACRYLATE AND ITS EFFECT ON MECHANICAL AND THERMAL PROPERTIES OF POLYPROPYLENE COMPOSITES Faisal Amri Tanjung; Salmah Husseinsyah; Kamarudin Hussin; Iqmal Tahir
Indonesian Journal of Chemistry Vol 13, No 2 (2013)
Publisher : Universitas Gadjah Mada

Effects of methyl methacrylate on the properties of chitosan-filled polypropylene (PP) composites has been investigated. Mechanical and thermal properties of the composites were analyzed according to ASTM D 638-91, thermogravimetry analysis (TGA) and differential scanning calorimetry (DSC). The results showed that tensile strength of PP composites decreased upon the addition of chitosan, while Young's modulus improved. At a similar filler loading, the treated PP/chitosan composites were found to have higher tensile strength and Young's modulus as compared with the untreated composites. Thermal analysis results showed that thermal stability and crystallinity of the treated composites were higher than the untreated ones. Scanning electron microscopy (SEM) and Fourier transforms infrared (FTIR) studies revealed less detached filler from matrix on tensile surface of the treated composites as an evidence of enhanced filler-matrix interfacial adhesion due to formation of ester-bridge between the chitosan and the methyl methacrylate.

PHOSPHATE AND NITRATE REMOVAL FROM DRINKING WATER SOURCES USING ACRYLAMIDE-FERRIHYDRITE GEL Barlah Rumhayati; Chasan Bisri; Heni Kusumawati; Faridah Yasmin
Indonesian Journal of Chemistry Vol 12, No 3 (2012)
Publisher : Universitas Gadjah Mada

Phosphate and nitrate ions removal from drinking water has been conducted using acrylamide-ferrihydrite gel. The gel was prepared by mixing the ferrihydrite paste and acrylamide gel solution followed by casting at temperature 42-46 °C for at least one hour. The effect of pH and concentration of phosphate and nitrates to the percent of removal were investigated. Desorption efficiency was also investigated using sulphuric acid at various concentration. As a result, phosphate and nitrate could be removed optimally at pH 5. The solution concentration of nitrate for optimum removal was 10 mg/L NO3-, whilst phosphate could be removed optimally at concentration of 0.3 mg/L PO43-. The analytes could be desorbed from the gel using H2SO4 0.3 M. In application, phosphate and nitrate in the drinking water sources could be removed up to 70%.

Computer-Aided Drug Repurposing: A Cyclooxygenase-2 Inhibitor Celecoxib as a Ligand for Estrogen Receptor Alpha Enade Perdana Istyastono; Florentinus Dika Octa Riswanto; Sri Hartati Yuliani
Indonesian Journal of Chemistry Vol 15, No 3 (2015)
Publisher : Universitas Gadjah Mada

A cyclooxygenase-2 (COX-2) inhibitor celecoxib has been previously reported to have cytotoxic activities towards gastric, prostate, ovarian, colon and breast cancer cell lines. This article reports that the cytotoxic activities of celecoxib could be resulted from its activity as a potent ligand for estrogen receptor alpha (ERα). Aided by molecular docking simulations, an in silico test to examine whether celecoxib is a ligand for estrogen receptor alpha (ERα) was performed followed by in vitro test employing cytotoxic assay using 3-[4,5-dimethylthiazol-2-yl]-2,5-diphenyltetrazolium bromide (MTT) method. The compound was extracted from Celebrex®. Measured by using UV spectrophotometric method at 255.5 nm, it was identified that the content of celecoxib was 102.15 mg/271.48 mg capsule content. The in silico test indicated that celecoxib is a potent ligand for ERα. This finding was confirmed experimentally by an in vitro test that celecoxib has a comparable activity as an ERα ligand to tamoxifen, a drug of choice for breast cancer treatment.

Simulation of Pollutant Gas Dispersion on Case Study of Lontar 3 Coal Fired Power Plant in Addition into 1 x 660 MW Capacity in Kemiri, Tangerang District, Banten Province Eko Sugiharto; Taufik Abdillah Natsir; Abdul Rozaq
Indonesian Journal of Chemistry Vol 14, No 3 (2014)
Publisher : Universitas Gadjah Mada

Air quality simulation has been performed for additional capacity of Banten 1 x 600 MW Coal Fired Power Plant toward air quality degradation in its surrounding environment. The simulation was based on pollutant gas dispersion calculated using Gaussian Plume equation. The research has involved climate secondary data on Cengkareng climatology Station for last 10 years. Besides, the primary data has also been taken in 7 point sampling locations to determine initial ambient air quality of existing 1 x 600 MW Coal Fired Power Plant. The data of existing 1 x 600 MW coal fired power plant has been taken from Adipala Steam Power Plant while the gas pollutant dispersion simulation has been done well using Gaussian Plume equation. The result showed that gas emission for NO2, and TSP parameter in all scenarios and SO2 gas parameter in several scenarios were exceeding the Threshold Limit Value. Thus, a technology is needed to minimize produced emission gas. The increase of gas pollutant in all sampling locations was not significantly increasing and those gas pollutants were not generally exceeding the Threshold Limit Value permitted by the government regulation.

QUINOLIN-6-AMINES: SYNTHESIS AND BIOLOGICAL EVALUATION Hament Panwar; Nidhi Chaudhary; Ranjana Dubey; Tilak Ram
Indonesian Journal of Chemistry Vol 13, No 3 (2013)
Publisher : Universitas Gadjah Mada

Some novel 2-{(chloromethoxy)methyl}thio-N-substituted phenyl-[1,2,4]triazolo[1,5-a] quinolin-6-amines have been derived from 5-bromocoumarin. All the synthesized compounds have been characterized by elemental and spectral (I.R., 1H-NMR, Mass) analysis and evaluated for their antimicrobial, insecticidal and anthelmintic activities.

SYNTHESIS 7-O-CARBOXYMETHYL-3’,4’-DIMETHOXYISOFLAVONE Andi Hairil Alimuddin; Sabirin Matsjeh; Chairil Anwar; Mustofa Mustofa
Indonesian Journal of Chemistry Vol 12, No 3 (2012)
Publisher : Universitas Gadjah Mada

Synthesis of 7-O-carboxymethyl-3',4'-dimethoxyisoflavone from 7-hydroxy-3',4'-dimethoxyisoflavone derived from eugenol had been done. 7-hydroxy-3',4'-dimethoxyisoflavone was first converted into 7-O-ethoxycarbonylmethyl-3',4'-dimethoxyisoflavone via substitution of hydroxyl group at 7-O position by ethyl-2 chloro acetate through bimolecular nucleophilic substitution reaction (SN2). Hydrolysis of ester group of 7-O-ethoxycarbonylmethyl-3',4'-dimethoxyisoflavone using KOH produce 7-O-carboxymethyl-3',4'-dimethoxyisoflavone in 93.4% yield as a white solid with melting point of 155-159 °C.

Synthesis and Characterization of Alumina Precursors Derived from Aluminum Metal through Electrochemical Method Eva Marlina Ginting; Nurdin Bukit
Indonesian Journal of Chemistry Vol 15, No 2 (2015)
Publisher : Universitas Gadjah Mada

This study investigated the use of the electrochemical method to prepare alumina (a-Al2O3) from aluminum metal. The a-Al2O3 precursor was calcined at 110 °C for six hours and then characterized using Fourier Transform Infrared (FTIR) spectroscopy, Particle Size Analysis (PSA), X-Ray Diffraction spectroscopy (XRD), and Scanning Electron Microscopy (SEM). To study transformation of the precursor into α-Al2O3, three samples were sintered at 400, 800, and 1200 °C, respectively and they were characterized. The most interesting result obtained was the transition of AlOOH and β-Al(OH)3 into γ-Al2O3 at low temperatures (400 to 800°C), followed by transformation of γ-Al2O3 into a-Al2O3 at high temperature (1200 °C). The overall results obtained demonstrated that electrochemical method is a potential alternative for production of α-Al2O3, which can be achieved in practically pure phase at sintering temperature at 1200 °C.

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