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Fabrication of fine particle powder from Teak (Tectona Grandis) leaves as a textile dyeing with environmentally friendly technology Budianto, Arif; Dewi, Diah L.; Rahayu, Susi; Kurniawidi, Dian W.; Akhyar, Halil; Alaydrus, Alfina T.
ORBITA: Jurnal Pendidikan dan Ilmu Fisika Vol 10, No 1 (2024): May
Publisher : Universitas Muhammadiyah Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31764/orbita.v10i1.22509

Green technology for eco-friendly dyes in textile industries has been required in recent decades. An innovation was established by producing textile dyes from natural sources. This research aims to identify fine particle powder's characteristics and analyze the color changes applied to the textile. The mechanical thermal was utilized to produce natural dyes. Three main stages were conducted to obtain dye powder: mordant, coloring, and fixation. The dye powder was examined for water content, phytochemical tests, FTIR, SEM-EDX, and color using the Android-based Color Analyzer and Color Grab applications. The results show that the water content of 7.21% meets the SNI 01-3709-1995 standard. So, the powder can be stored for a long time because it does not quickly spoil. In addition, the phytochemical test resulted in alkaloids, flavonoids, and tannins. This revealed that teak leaf powder can be a suitable textile dye. After that, SEM-EDX examination illustrated that the powder had a round, flat, elongated morphology, a sharp edge texture, and an irregular position. Meanwhile, the EDX signified that the recognized chemical elements did not damage the environment, and the powder diameter ranges from 0.5-8.5 μm. The powder size complied with the fine particle powder category. To analyze the color from the dye powder application, there were color changes during each dyeing process. During all stages, from making the powder to applying the powder to the fabric, environmentally friendly technology was utilized. Therefore, this research can promote new opportunities for innovation and development of highly competitive products towards a more environmentally friendly and sustainable textile industry.

MENDUKUNG NTB DALAM PROGRAM NZE 2050 DENGAN EDUKASI 6R (REFUSE, REDUCE, REUSE, RECYCLE, RETHINK, and ROT) UNTUK SAMPAH PLASTIK DI SMA N 2 SELONG, LOMBOK TIMUR Putraji, L.M. Guguh; Ardianto, Teguh; Budianto, Arif; Hudha, L. Sahrul; Rahayu, Susi; Kurniawidi, Dian W.
Jurnal Pepadu Vol 5 No 4 (2024): Jurnal PEPADU
Publisher : Universitas Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/pepadu.v5i4.6052

Sampah secara umum dihasilkan dari kegiatan manusia sehari-hari. Dari berbagai jenis sampah, sampah plastik merupakan sampah non-organik yang paling banyak dihasilkan, tidak dapat diurai secara alamiah, dan memiliki dampak bagi kesehatan maupun lingkungan. Kabupaten Lombok Timur, memproduksi sampah terbanyak setiap harinya di Provinsi Nusa Tenggara Barat. Usaha mengurangi sampah perlu didukung oleh kesadaran masyarakat untuk mengurangi sampah dan memilah sampah sehingga dapat mengurangi beban pengelolaan sampah yang dilakukan oleh pemerintah daerah, terlebih setelah pemerintah propinsi NTB menggaungkan program Net Zerowaste Emission Tahun 2050. SMA N 2 Selong merupakan salah satu sekolah di wilayah Selong Lombok Timur yang diharapkan mampu menjadi pionir dalam edukasi pengembangan kesadaran diri sehingga memiliki peran yang sangat stategis untuk mengedukasi masyarakat. Oleh karena itu, untuk mengatasi permasalahan sampah perlu dilakukan edukasi pemilahan sampah plastik di lingkungan sekolah. Bahkan perlu diperkenalkan manfaat mendaur ulang sampah karena hal ini akan menunjukkan animo generasi muda dalam mewujudkan program zero waste di lingkungan SMA N 2 Selong, dan nantinya diharapkan pada generasi muda di seluruh wilayah Lombok Timur. Kegiatan ini diikuti oleh siswa kelas X, XI dan XII sejumlah 54 siswa terpilih dan hampie seluruh guru SMA N 2 Selong dengan respon Sangat Memuaskan.

Synthesis of nanochitosan from oyster pearl shell (Pinctada maxima) as renewable energy candidate Rahayu, Susi; Alawiyah, Geby; Kurniawidi, Dian W.; Ardianto, Teguh; Budianto, Arif; Alaa, Siti; Syamsuddin, Syamsuddin
Acta Chimica Asiana Vol. 7 No. 2 (2024)
Publisher : The Indonesian Chemical Society, Chapter Nusa Tenggara and The University of Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/aca.v7i2.205

The increase in energy needs must be balanced by environmentally friendly technological innovations. Chitosan polymer is one of the technological innovations of energy materials that are being developed by many developed countries. This research aimed to identify the potential of oyster pearl shell waste as a source of electrolyte polymers. The study was conducted experimentally by synthesizing chitosan nanoparticles from chitosan using the ionic gelation method. Chitosan is obtained through the isolation method from Pinctada maxima oyster pearl shell waste. The isolation method is carried out by three processes: deproteination, demineralization, and deacetylation. Several characterizations were carried out to analyze the material from the synthesis, including a proximate test, FTIR analysis, and PSA analysis. Isolated chitosan was identified to have a deacetylation degree that reached 88.63% with the formation of OH and NH2 functional groups. In general, the proximate tets data has shown that the obtained chitosan already meets the Indonesian standard SNI 7949:2013. PSA analysis resulted in differences in size distribution, PDI, and zeta potential between chitosan and chitosan nanoparticles. The results were obtained by the average distribution of chitosan particle size of 52.043 μm and chitosan nanoparticle size of 2.3365 μm—the analysis of the potential zeta of chitosan -3.9 mV and chitosan nanoparticle -21,6 mV. Thus, changes in the size of the chitosan material affect its potential PDI and zeta values. The change of these two values is a good indicator of the initial data and the potential of the material as an energy material. Therefore, chitosan polymer is an electrolyte material that can be used as a candidate for environmentally friendly renewable energy materials

Isolasi Kitosan dari Cangkang Kerang Mutiara (Pinctada maxima) Menggunakan Deasetilasi Dengan Gelombang Mikro Rahayu, Susi; Destrianingtyas, Aulia Safitri; Ridho Illahi, Ramadian; Kurniawidi, Dian W.
Kappa Journal Vol 8 No 2 (2024): Agustus
Publisher : Universitas Hamzanwadi

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29408/kpj.v8i2.27166

Kitosan merupakan biopolimer turunan dari hasil deasetilasi kitin, yang berkembang pesat di dunia medis saat ini. Kitosan salah satu material yang memiliki sifat anti mikroba, biokompatibel, dan biodegradable sehingga aman bagi tubuh manusia. Penelitian ini dilakukan untuk mengidentifikasi pengaruh daya gelombang mikro terhadap karakteristik kitosan. Pembuatan kitosan dengan mengisolasi kitosan dari cangkang kerang Mutiara (Pinctada maxima sp) melalui proses deproteinasi, demineralisasi, dan deasetilasi. Kitosan di analisis gugus fungsi, derajat deasetilasi, rendemen, berat molekul, dan struktur kristalnya. Pada tahapan deasetilasi mengunakan NaOH 60%. Hasil penelitian menunjukkan bahwa pemberian gelombang mikro dengan daya high selama 5 menit memperoleh nilai derajat deasetilasi tertinggi 83,40%, rendemen akhir sebesar 8,2%, dan berat molekul 222.185,94 Da, serta memiliki derajat kristalinitas sebesar 59,09%. Derajat deasetilasi kitosan meningkat seiring dengan naiknya daya gelombang mikro sedangkan berat molekul yang dihasilkan berbanding terbalik dengan derajat deasetilasi.

Synthesis and Characterization of TiO2/CaTiO3 Perovskite Composite Derived from Pinctada maxima Shell Waste Kurniawidi, Dian W.; Rahayu, Susi; Budianto, Arif; Saputra, Kormil; Agista, Wida Puteri; Suprayogi, Thatit; Marlina, Resti
Science and Technology Indonesia Vol. 10 No. 3 (2025): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26554/sti.2025.10.3.924-942

This study has succeeded in synthesizing and characterizing TiO2/CaTiO3 perovskite composites using calcium carbonate (CaCO3) from shellfish waste (Pinctada maxima). Synthesis was carried out through the coprecipitation method with variations in the molar ratio of CaCO3:TiO2 and calcination temperatures (700oC, 800oC, and 900oC). Characterization was carried out using FTIR, DTA-TG, XRD, SEM-EDS, BET and UV-Vis. The results of the analysis showed that the calcination temperature affected the powder color, crystal structure, thermal properties and particle size. The DTA-TG analysis shows that increasing the calcination temperature up to 900oC significantly reduces mass loss to 51.88%, with minimal thermal events, indicating the formation of a thermally stable and well-crystallized TiO2/CaTiO3 structure. At a temperature of 900oC, a more perfect CaTiO3 was formed with the whitest powder color, the anatase and brookite phases of TiO2 were still detected, while the calcite phase was still found at a temperature of 700oC. The morphology of the samples showed agglomeration with increasingly uniform particle sizes at higher calcination temperatures. Complementary BET analysis confirms that the composite possesses a mesoporous structure with a specific surface area of 11.42 m2/g and a pore size distribution of 3-5 nm, making it suitable for adsorption and photocatalytic applications. UV-Vis analysis showed an increase in the band gap value along with the increase in the TiO2 ratio. This is also confirmed by the presence of Urbach energy which tends to increase with increasing TiO2 ratio.

INFLUENCE OF COMPOSITION AND LYOPHILIZATION TIME ON PHYSICAL PROPERTIES OF HA/Cs/Coll/ HYDROXYPROPYL METHYLCELLULOSE BIOCOMPOSITES FOR BONE SCAFFOLDS Purnaning, Dyah; Hurnah, Hurnah; Taufik S, Ahmad; Rahayu, Susi; Kurniawidi, Dian W.; Hadi, Kasnawi Al
Indonesian Physical Review Vol. 8 No. 2 (2025)
Publisher : Universitas Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/ipr.v8i2.474

Biomaterial implants are one of the alternatives to replace damaged organs in the body system temporarily (scaffolding) or permanently. Bone biomaterial implants can be obtained through the manufacture of HA/Cs/Coll (HA/Cs/Coll) biocompositeses with the addition of Hydroxypropyl Methylcellulose (HPMC) matrix. The objective is to evaluate how variations in material composition and lyophilization time affect the physical properties of the biocomposites, including density, compressive strength, Youngâ€™s modulus, and surface morphology. The manufacture ofÂ biocomposites uses the mechanical thermal method for mixing materials and the freeze drying method for the biocomposites drying process. Composition ratios of HA:Cs/Coll were varied at 3:7, 5:5, and 7:3, while lyophilization durations were set at 24, 48, and 72 hours. Characterizations were performed through density measurements, mechanical testing using a Tensilon machine, and surface morphology analysis using a digital microscope. The results showed that the comparison of biocomposites with a ratio of 7:3 had the highest density of 0.150 gr/cmÂ³, compressive strength of 0.046 MPa, and young modulus of 0.3 MPa. Meanwhile, the biocomposites that was lyophilized for 48 hours showed the best balance between a density of 0.145 gr/cmÂ³, a compressive strength of 0.08 MPa, and a young modulus of 0.17 MPa. Morphological analysis revealed improved porosity and surface uniformity with longer freeze-drying times. Based on this, the resulting HA/Cs/Coll biocompositese has potential as an implant material but further research is needed to improve its mechanical properties by increasing the concentration of the binder, namely HPMC.

MENDUKUNG NTB DALAM PROGRAM NZE 2050 DENGAN EDUKASI 6R (REFUSE, REDUCE, REUSE, RECYCLE, RETHINK, and ROT) UNTUK SAMPAH PLASTIK DI SMA N 2 SELONG, LOMBOK TIMUR Putraji, L.M. Guguh; Ardianto, Teguh; Budianto, Arif; Hudha, L. Sahrul; Rahayu, Susi; Kurniawidi, Dian W.
Jurnal Pepadu Vol 5 No 4 (2024): Jurnal PEPADU
Publisher : Universitas Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/pepadu.v5i4.6052

Sampah secara umum dihasilkan dari kegiatan manusia sehari-hari. Dari berbagai jenis sampah, sampah plastik merupakan sampah non-organik yang paling banyak dihasilkan, tidak dapat diurai secara alamiah, dan memiliki dampak bagi kesehatan maupun lingkungan. Kabupaten Lombok Timur, memproduksi sampah terbanyak setiap harinya di Provinsi Nusa Tenggara Barat. Usaha mengurangi sampah perlu didukung oleh kesadaran masyarakat untuk mengurangi sampah dan memilah sampah sehingga dapat mengurangi beban pengelolaan sampah yang dilakukan oleh pemerintah daerah, terlebih setelah pemerintah propinsi NTB menggaungkan program Net Zerowaste Emission Tahun 2050. SMA N 2 Selong merupakan salah satu sekolah di wilayah Selong Lombok Timur yang diharapkan mampu menjadi pionir dalam edukasi pengembangan kesadaran diri sehingga memiliki peran yang sangat stategis untuk mengedukasi masyarakat. Oleh karena itu, untuk mengatasi permasalahan sampah perlu dilakukan edukasi pemilahan sampah plastik di lingkungan sekolah. Bahkan perlu diperkenalkan manfaat mendaur ulang sampah karena hal ini akan menunjukkan animo generasi muda dalam mewujudkan program zero waste di lingkungan SMA N 2 Selong, dan nantinya diharapkan pada generasi muda di seluruh wilayah Lombok Timur. Kegiatan ini diikuti oleh siswa kelas X, XI dan XII sejumlah 54 siswa terpilih dan hampie seluruh guru SMA N 2 Selong dengan respon Sangat Memuaskan.

FABRICATION OF CHITOSAN BIOPOLYMER FROM PEARL OYSTER SHELLS (Pinctada maxima) FOR MEDICAL APPLICATIONS Nurmaulida, Siti Ema; Alawiyah, Geby; rahayu, Susi; Taufik S, Ahmad; Hidayatullah, Kholik; Kurniawidi, Dian W.; Ali, Muhamad
Indonesian Physical Review Vol. 6 No. 2 (2023)
Publisher : Universitas Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/ipr.v6i2.227

Chitosan is one of the biopolymers that has recently been developed in the medical field. Chitosan is biocompatible, biodegradable, and non-toxic, so it is safe for the human body. This study aimed to identify the characteristics of chitosan isolated from pearl oyster shells. Chitosan is obtained through three stages: deproteination, demineralization, and deacetylation. Characterization of chitosan is done physically and chemically including organoleptic test, yield calculation in each step of isolation, FTIR, and XRD. Isolated chitosan identified deacetylation degree and functional group with FTIR. While the crystal structure was determined using XRD. The results showed that chitosan powder has a beige color with a final yield of 7,06%. The characterization of FTIR shows that synthesized pearl oyster shells have successfully formed chitosan compounds with a deacetylation degree of 81,50%. Another characteristic is the crystal structure obtained; chitosan has orthorhombic unit cells with a degree of chitosan crystallinity of 36,94%. Based on the result, chitosan has met several standards in medical applications as a biomaterial.

PEMANFAATAN DAUN JATI DAN DAUN MANGGA SEBAGAI SUMBER PEWARNA ALAMI UNTUK KAIN PADA PENGRAJIN TENUN LOMBOK BERBASIS GREEN TEKNOLOGI Kurniawidi, Dian W.; Ardianto, Teguh; Alaa', Siti; Alhadi, Kasnawi; Dewi, Diah L.; S., RR. Delima; Rahayu, Susi
Jurnal Abdi Insani Vol 11 No 1 (2024): Jurnal Abdi Insani
Publisher : Universitas Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/abdiinsani.v11i1.1372

The Mandalika Central Lombok Special Economic Zone (SEZ) is one of the world-class national priority tourist destinations. However, until now there has been no branding of the village's superior woven products that can contribute significantly to the Mandalika SEZ. So it is important to carry out this service activity, to give birth to entrepreneurial pioneer weaving craftsmen towards "LOMBOK WEANING, LOCAL GOING GLOBAL". To achieve this goal, the craftsmen group experienced several problems (1) limited insight into the importance of developing weaving for the tourism sector towards international tourism and (2) the dyeing process was still using conventional methods which took a long time and was impractical. This problem arose due to a lack of human resources owned by the village, even though the natural resource potential it has really supports the songket weaving industrial center. Therefore, the role of academics is really needed to innovate to provide solutions to problems based on green technology. The solutions to the problems that will be offered are (1) activities to open people's insight into the importance of the tourism sector (2) dissemination of green synthesis technology using a modified steam extraction method to produce natural dye powder accompanied by students of the material characterization method course (3 credits). So that both solutions can be delivered appropriately, a systematic flow of activities needs to be carried out consisting of (a) socialization, training, (c) mentoring, and (d) monitoring and evaluation. A series of activities have been carried out, it is hoped that the craftsmen's skills will increase so that they are able to independently produce coloring powder from various existing local natural resources and be able to compete internationally. In addition, different types of leaves will produce different color pigments. Differences in dyeing processes and techniques will produce cotton threads with different qualities. In general, natural dyes always produce soft colors.

Characteristics of Dyeing Cotton Thread Using Fine Particle Powder from Tectona Grandis Leaf Kurniawidi, Dian W.; Dewi, Diah L.; Rahayu, Susi; Budianto, Arif; Alaa, Siti
Jurnal Penelitian Pendidikan IPA Vol 9 No 10 (2023): October
Publisher : Postgraduate, University of Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/jppipa.v9i10.3753

In Lombok, the traditional process of dyeing woven fabrics primarily involves the use of synthetic dyes, which can contribute to environmental pollution. This study aimed to identify the characteristics of woven yarn and assess the effect of dye solution pH on yarn properties when using teak leaves (Tectona grandis) to produce dye powder through a mechanical thermal method. The thread coloring process comprised mordanting, coloring, and fixation stages, with the assistance of Android applications for color analysis and a Universal Tensile Machine Type RTG-1310 to assess mechanical properties. The results revealed that dyeing yarn with anthocyanin powder from teak leaves yielded a range of colors, including shades of gray, brown, and red. The highest tensile strength observed was 2,664 cN/dtex, and the solution's pH significantly influenced the dominant color, with red being prominent. Notably, optimal tensile strength (1,649 cN/dtex) was achieved at pH six. These findings highlight the potential for producing high-quality cotton threads using different dyeing processes and techniques. The study's insights contribute to both environmental protection and thread quality enhancement in the textile industry

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