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All Journal Eksergi: Chemical Engineering Journal KOVALEN: Jurnal Riset Kimia JC-T (Journal Cis-Trans): Jurnal Kimia dan Terapannya JKPK (Jurnal Kimia dan Pendidikan Kimia) Jurnal Sains dan Teknologi Reaksi International Journal of Applied Technology Research Jurnal Difusi Industrial Research Workshop and National Seminar Journal Serambi Engineering (JSE) Sainteknol : Jurnal Sains dan Teknologi Journal of Green Science and Technology
Paramitha, Tifa
Politeknik Negeri Bandung
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Pengaruh Variasi Daya Microwave Terhadap Rendemen Ekstrak Kulit Pisang Dengan Metode Vacuum Microwave Assisted Extraction Putri, Angelina; Luviana, Angely; Ramadhan, Muhammad Zikri; Nidaulhusna, Anisa; Salsabilla, Iva Najwa; Sihombing, Rony Pasonang; Paramitha, Tifa
Prosiding Industrial Research Workshop and National Seminar Vol. 14 No. 1 (2023): Vol 14 (2023): Prosiding 14th Industrial Research Workshop and National Semina
Publisher : Politeknik Negeri Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35313/irwns.v14i1.5391

Abstract

Pisang merupakan salah satu buah yang proses pertumbuhannya cukup besar di Indonesia. Berdasarkan data Badan Pusat Statistik, produksi pisang Indonesia pada 2021 sebesar 8,84 juta ton. Besarnya produksi pisang dapat menjadi potensi yang sangat besar dalam menghasilkan limbah kulit pisang yang sejauh ini hanya dibuang begitu saja meskipun ada sebagian orang yang memanfaatkannya sebagai olahan makanan. Penelitian mengenai ekstraksi ini diharapkan mampu mendorong peluang pemanfaatan kulit pisang untuk keperluan lain seperti inhibitor korosi. Penelitian ini bertujuan untuk mengetahui pengaruh variasi daya microwave terhadap rendemen ekstrak kulit pisang. Proses ekstraksi dilakukan dengan menggunakan berbagai tingkat daya microwave pada waktu ekstraksi yang konstan. Metode ekstraksi yang digunakan adalah VMAE (Vacuum Microwave Assisted Extraction). Metode ini merupakan teknik ekstraksi yang menggabungkan penggunaan microwave dengan tekanan vakum untuk meningkatkan efisiensi ekstrak kulit pisang. Pelarut yang digunakan adalah etanol 96%, variasi daya sebesar 150, 300, dan 450 watt, serta waktu ekstraksi selama 10 menit. Analisis yang dilakukan adalah analisis gravimetri, perhitungan rendemen, serta uji fitokimia menggunakan reagen. Melalui analisis gravimetri diketahui kadar air kulit pisang awal sebesar 63.71% menurun menjadi 6.98%. Dari proses ekstraksi diperoleh rendemen optimum sebesar 68.23% pada daya 300 watt. Berdasarkan uji fitokimia diketahuui bahwa ekstrak kulit pisang mengandung senyawa alkaloid.
The Effect of Pineapple Crude Enzymes and Fermentation Time on The Decaffeination Process of Robusta Coffee Hariyadi, Tri; Paramitha, Tifa; Irmawati, Dwi; Salsabila, Salwa Ainaya
Jurnal Internasional Penelitian Teknologi Terapan Vol 5 No 1 (2024): February 2024
Publisher : Bandung State Polytechnic (Politeknik Negeri Bandung)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35313/ijatr.v5i1.128

Abstract

The decaffeination of robusta coffee can be done through fermentation with a crude enzyme containing bromelain enzyme from pineapple. The study aims to determine the activity of the bromelain enzyme by the Kunitz method, the effect of fermentation time and crude enzyme concentration on the decaffeination process, and the characteristics of coffee before and after fermentation using FTIR. The fermentation time was varied from 6 to 36 hours and the crude enzyme concentration was varied from 10 to 80%. The activity of the bromelain enzyme was 36 U/ml. Fermentation time affects the decaffeination process, wherein the longer the fermentation time from 6 hours to 36 hours obtained caffeine content from 2.39% to 0.07%. Besides that, the crude enzyme concentration affects the decaffeination process, which obtained the lowest caffeine content or percent decaffeination at the crude extract concentration of 80% (v/v). FTIR results showed that the decaffeination process affected the reduction of caffeine in coffee samples. It can be shown from the increase in the %T value of the C-N functional group from 40.731 to 54.85.
Characterization of Banana Peel Corrosion Inhibitor by Vacuum Microwave Assisted Extraction (VMAE) Method in 2% HCl Environment binti Jamaluddin, Jamarosliza; Paramitha, Tifa; Salsabila, Iva Najwa; Luviana, Angely; Ramadhan, Muhammad Zikri; Putri, Angelina; Nurbaits, Alisya; Sihombing, Rony Pasonang
Jurnal Internasional Penelitian Teknologi Terapan Vol 5 No 1 (2024): February 2024
Publisher : Bandung State Polytechnic (Politeknik Negeri Bandung)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35313/ijatr.v5i1.144

Abstract

Banana peel is a waste that is very abundant in Indonesia. The utilization of banana peel can be used for corrosion inhibitors. The type of environment applied in this study is an acidic environment, which is carried out in 2% HCl solution media. The purpose of this study is utilize banana waste extract obtained from the VMAE method. The extract was obtained by VMAE method at 150 watts, 300 watts and 450 watts for 10 minutes using ethanol solvent. The ratio of feed and solvent used was 1:10 (b/v). The results of the extract were subjected to phytochemical tests using Dragendroff, Wagner and Mayer reagents. After that, the extract was applied to the media for corrosion rate test and GC-MS. The results of the study showed that the lowest corrosion rate was obtained at a concentration of 1500 ppm non-aerated which was 0.7347 mmpy. While based on the GC-MS test results, terpenoid compounds and vitamin E can be detected from banana peel extract, where these two compounds are antioxidant substances that can be utilized as corrosion inhibitors.
Tofu Liquid Waste Treatment Using Effective Volume of Anaerobic Sequencing Batch Reactor (ASBR) Budiastuti, Herawati; Rachmawati, Anissa Nurul; Agustin, Delliana; Paramitha, Tifa; Rusdianasari
KOVALEN: Jurnal Riset Kimia Vol. 10 No. 1 (2024): April Edition
Publisher : Chemistry Department, Mathematics and Natural Science Faculty, Tadulako University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/kovalen.2024.v10.i1.16478

Abstract

The tofu industry produces liquid waste containing high organic compounds. Organic compounds in liquid waste can threaten aquatic ecosystems if discharged directly into water bodies. One of the most effective wastewater treatment systems is the treatment using Anaerobic Sequencing Batch Reactor (ASBR). Besides being able to reduce the content of organic compounds, ASBR can produce biogas, and its decomposing microorganisms do not flow into the effluent stream. The purpose of this study was to evaluate the performance of ASBR at an effective reactor volume according to the design. This is because the use of ASBR in previous studies had not reached the operational stage and did not use an effective volume reactor. The stages of waste treatment using ASBR include the seeding, acclimatization, and operation stages. Waste treatment took place at room temperature in the reactor with an effective volume of 6 L. The operating parameters tested were MLVSS, COD, BOD, pH, and cumulative biogas volume. The results obtained show that the seeding process took 56 days, acclimatization took 10 days, and the operation lasted for 17 days. The efficiency of reducing COD concentration was 60%, the efficiency of reducing BOD concentration was 35.65%, and the cumulative volume of biogas produced was 24,120 mL at the operating stage. The use of the ASBR system at an effective volume of 6 L resulted in the successful processing of tofu liquid waste.
Evaluasi dan Modifikasi Alat Penukar Ion dengan Penambahan Kolom Adsorpsi Karbon Aktif untuk Menurunkan Kesadahan : Evaluation dan Modification of Ion Exchange Equipment with the Addition of Activated Carbon Adsorption Column to Reduce Hardness Endang Kusumawati; Retno Dwi Jayanti; Lestari Herlianti Putri; Nurul Annisa; Paramitha, Tifa
KOVALEN: Jurnal Riset Kimia Vol. 10 No. 1 (2024): April Edition
Publisher : Chemistry Department, Mathematics and Natural Science Faculty, Tadulako University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/kovalen.2024.v10.i1.16556

Abstract

Ion exchange is one of the water treatment methods used to reduce hardness. To improve the performance of the ion exchange columns, modification can be done by adding an activated carbon column placed after the ion exchange column to adsorb ions that were not exchanged by the resin so that the treated water met boiler feed water quality standards. The purposes of this study were to determine the best flow rate to reduce hardness in the configuration of the ion exchange and activated carbon columns, determine the saturation time of each column, and determine their exchange/adsorption capacities. The steps of this study included modifications and repair of equipment, leak tests, and configuration system performance tests. Performance tests were conducted by varying the feed flow rates by 0.2; 0.4; 0.6; 0.8; 1 GPM and analyzed the efficiency of hardness reduction. The results of this study showed that the best flow rate to reduce the initial hardness of 499 mg/ L CaCO3 was a flow rate of 0.6 GPM or 2.2 LPM. The efficiency of hardness reduction in the configuration system was 100%. The conductivity of the effluent of anion column and activated carbon column decreased compared to the conductivity of the effluent of cation column with an average decrease of 33.17% in the anion column and 18.35% in the activated carbon column. The saturation time of the configuration system was 168 minutes in cation resin, 46.4 minutes in anion resin, and 159 minutes in activated carbon. Furthermore, the adsorption capacity of cation resin, anion resin, and activated carbon were 35.28 mg/g, 43.98 mg/g, and 9.61 mg/g, respectively. The addition of activated carbon in the configuration system lowers the conductivity of the effluent and decreases hardness.
PELATIHAN DAN PEMBUATAN MATERI UJI KOMPETENSI (MUK) SKEMA PENANGGUNG JAWAB PENGOPERASIAN PENGOLAHAN AIR LIMBAH (POPAL) Hidayatulloh, Irwan; Budiastuti, Herawati; Soeswanto, Bambang; Kusumawati, Endang; Trirahayu, Dhyna Analyes; Paramitha, Tifa; Ramadhani, Laily lsna; Elizabeth, Lidya
Jurnal Difusi Vol. 7 No. 2 (2024): Jurnal Difusi
Publisher : Pusat Penelitian dan Pengabdian Masyarakat (P3M) Politeknik Negeri Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35313/difusi.v7i2.5561

Abstract

Ada 5 (lima) unit kompetensi dari draft skema okupasi Penanggung Jawab Pengoperasian Pengolahan Air Limbah (POPAL) yang sedang dibuat dan sekaligus akan diberikan dalam pelatihan bagi guru-guru SMK Negeri 7 Bandung oleh dosen-dosen Teknik Kimia, Politeknik Negeri Bandung. Unit kompetensi yang dimaksud yakni Mengoperasikan Instalasi Pengolahan Air Limbah (IPAL), Menilai Tingkat Pencemaran Air Limbah, Melakukan Perawatan IPAL, Mengidentifikasi Bahaya Pengolahan Air Limbah, dan Melakukan Tindakan Keselamatan Kerja terhadap Bahaya dalam IPAL. Dengan demikian para asesor di kedua institusi pendidikan ini dapat memiliki kompetensi dalam membuat MUK dimana MUK menjadi persyaratan wajib dalam pengusulkan draft skema yang akan diajukan untuk dilisensi oleh Badan Nasional Sertifikasi Profesi (BNSP) Indonesia. Hingga saat ini, terdapat beberapa kegiatan yang telah dilaksanakan. Pertama, koordinasi dan pertemuan telah dilakukan dengan pihak mitra untuk sinkronisasi pelaksanaan kegiatan. Kedua, koordinasi internal tim PkM untuk membahas pembagian tugas, rencana pembuatan MUK, dan rencana pelaksanaan pelatihan bagi para peserta pelatihan. Ketiga, merupakan pelaksanaan pelatihan mengenai pembuatan MUK unit kompetensi 1 dan 2. Keempat, merupakan lanjutan pelakasanaan kegiatan pelatihan mengenai pembuatan MUK untuk unit kompetensi 3, 4 dan 5.
Studi Awal Sintesis ZnO/SiO2 dengan Silika dari Limbah Padat Geothermal dan Uji Performansinya dalam Penghilangan Metilen Biru : Preliminary Study of ZnO/SiO2 Synthesis with Silica from Geothermal Solid Waste and Its Performance Test in Methylene Blue Removal Paramitha, Tifa; Joko Suryadi; Rahma Ardelia Raissa; Teguh Aditya Nugraha; Nirmala Utami
KOVALEN: Jurnal Riset Kimia Vol. 9 No. 3 (2023): December Edition
Publisher : Chemistry Department, Mathematics and Natural Science Faculty, Tadulako University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/kovalen.2023.v9.i3.16557

Abstract

Industrial development impacts environmental problems, such as the emergence of wastewater containing methylene blue. In this research, SiO2 was composited with ZnO to remove methylene blue. The steps of this study include SiO2 extraction from geothermal solid waste, ZnO/SiO2 synthesis, and methylene blue removal test. The process of extracting SiO2 from geothermal solid waste used the sol-gel method. The FTIR analysis showed that SiO2 contains siloxane group (Si-OH) and silanol group (Si-O-Si). ZnO/SiO2 synthesis was done by making SiO2 suspension and continued with adding the addition of several Zn(NO3)2.6H2O. The FTIR analysis of ZnO/SiO2 showed no absorption at the wavenumber 960 cm-1 and there is a shoulder around the number 950 cm-1 which indicates the vibration of Si-O-Zn. Meanwhile, methylene blue removal tests were carried out on artificial wastewater. Based on the research results, the highest percent removal (99%) was obtained under operating conditions, including a dose of 500 mg/L, pH 10, and contact time of 30 minutes. Based on box-benkhen analysis, it is known that dose and pH singularly affect the percent removal, while contact time does not affect the percent removal. The optimization results obtained optimum conditions for methylene blue removal at a dose of 581.952 mg/L, pH of 10, and contact time of 30 minutes. Percent removal in conditions without irradiation and with irradiation of UV light were 98.758% and 99.178%. It shows that the adsorption process is the main process in removing methylene blue, while the photocatalytic process has little effect because it is possible that only a small amount of ZnO can attach to the surface of SiO2.
The Effect of Solvent-to-Coffee Ratio on Caffeine Content in Ethyl Acetate Extracts of Arabica Gayo Coffee Beans Soeswanto, Bambang; Sihombing, Rony Pasonang; Suryadi, Joko; Hariyadi, Tri; Paramitha, Tifa; Yusuf, Yusmardhany; -, Alfiana Adhitasari
KOVALEN: Jurnal Riset Kimia Vol. 9 No. 3 (2023): December Edition
Publisher : Chemistry Department, Mathematics and Natural Science Faculty, Tadulako University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/kovalen.2023.v9.i3.16573

Abstract

This paper studies the optimal ratio that gives the highest caffeine amount and improves the efficiency and quality of extraction from Arabica Gayo coffee beans. No previous studies have explored the best ratio of Gayo Arabica coffee beans to ethyl acetate solvent for extracting caffeine. The paper explains the method used, which has four main steps: preparing materials, extracting and measuring caffeine, and analyzing the results. The paper presents the experimental findings and discusses how different ratios affect caffeine content in Arabica Gayo coffee beans. It uses statistics to show significant differences between the ratios and compares them using Tukey tests. The paper concludes that the best solvent-to-coffee ratio for maximizing caffeine in ethyl acetate extracts is 1:5, resulting in a concentration of 1411.1 ppm. This ratio gives the best balance between caffeine yield and solvent usage.
The Effect of Variations in Sulfuric Acid - Oxalic Acid Electrolyte Concentration and Additional Aeration on 1100 Series Aluminum Anodization Results Leoanggraini, Unung; Irianto, Indra; Aji, Restu; Paramitha, Tifa; Sihombing, Rony
Journal of Green Science and Technology Vol 8 No 2 (2024): Journal of Green Science and Technology Vol.8 No.2 September 2024
Publisher : Faculty of Engineering, Universitas Swadaya Gunung Jati

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33603/jgst.v8i2.9425

Abstract

Aluminum is one of the materials used in making various types of goods because it has good properties such as being light, ductile and has good corrosion resistance. One of the disadvantages of aluminum is its low level of hardness. This can be overcome by treating aluminum, one of which is the anodization process. In this research, variations in the type of electrolyte used were sulfuric acid-oxalic acid, the electrolyte concentration was 16% with an interval of 0.5, the temperature used was room temperature with a current density of 3/dm2 and a coating time of 30 minutes. The aim of this research is to determine the acid concentration and the effect of the aeration system on mechanical properties. From the data obtained, it was found that the difference in weight of the best metal with the addition of aeration at a concentration of 13.5+2.5 was 0.0411 gr. This shows that as the concentration of oxalic acid increases it can accelerate the process of aluminum oxide formation, then for electrolyte concentrations of 16+0, 15.5+0.5, 15+1, 14.5+1.5 and 14+2 the difference in mass weight metals increased respectively by 0.0337 gr, 0.0335 gr, 0.0366 gr, 0.0390 and 0.0411 gr. In the anodization process without   additional aeration, the best metal weight difference is found at an electrolyte concentration of 13.5+2.5 of 0.0401 gr. This shows that increasing the concentration of oxalic acid can accelerate the process of aluminum oxide formation. Then at electrolyte concentrations of 16+0, 15.5+0.5, 15+1, 14.5+1.5 and 14+2 the difference in metal mass weight gradually increases by 0.0182 gr, 0.0293 gr, 0.0318 gr, 0.0322 and 0.0362 gr. Keywords: Aluminum, Anodization, Oxide Coating, Electrolyte Solution, Sulfuric Acid, Oxalic acid
Utilization of Coconut Shell and Coffee Grounds as Briquettes Using the Carbonization Method Adhitasari, Alfiana; Manfaati, Rintis; Paramitha, Tifa; Zahwa, Keisya Adellia; Setiawan, Kiranna Shalmadevy; Yusuf, Yusmardhany
Eksergi Vol 22 No 3 (2025)
Publisher : Prodi Teknik Kimia UPN "Veteran" Yogyakarta

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31315/eksergi.v22i3.15128

Abstract

Biomass-based briquettes offer a renewable energy alternative that can help reduce CO₂ emissions. Coconut shells and coffee grounds are promising waste materials due to their high calorific value. This study aimed to optimize the composition and carbonization time in producing briquettes from these two materials. The briquettes were prepared following SNI 01-6235-2000 and export briquette standards. The process included drying, carbonization at 300 °C for 60, 90, 120, 150, and 180 minutes, sieving, mixing, molding, and drying. Coconut shells and coffee grounds were mixed at weight ratios of 9:1, 8:2, 7:3, 6:4, and 5:5 with a total of 46.5 grams and 8.5 grams of adhesive. Briquette quality was evaluated based on moisture content, ash content, volatile matter, density, calorific value, and fixed carbon. The 9:1 composition yielded the highest calorific value of 6,472 cal/g, while a carbonization time of 90 minutes produced the best calorific value of 6,504 cal/g. The results show that a high proportion of coconut shells with limited coffee grounds and optimal carbonization time can produce briquettes with high energy potential, suitable for use as an alternative fuel.
Co-Authors -, Alfiana Adhitasari Agustin, Delliana Aji, Restu Alatif, Ikhsan Akmal Alfiana Adhitasari Alfiana Adhitasari Alya Zettira Sayyida Sulaeman Amelia Nur Aliah Andrijanto, Eko Angelina Putri Angely Luviana Arijan Vevayose Tarigan Azzahra, Rafila Chika Bambang Soeswanto Bambang Soeswanto binti Jamaluddin, Jamarosliza Dea Tri Febrian Deika Irham Faza Al-Ghaniy Dicky Harianto Dwi Irmawati, Dwi Elizabeth, Lidya Endang Kusumawati Endang Kusumawati Gamaliel Tanaka Ghaniari Putri Hariyadi, Tri Herawati Budiastuti Hidayatulloh, Irwan Irianto, Indra Jayanti, Retno Dwi Khoirunnisa Utami Khumaira Maulani Wijaya Lestari Herlianti Putri Luthfiana Kharisma Luviana, Angely Malik, Dava Maulana Manfaati, Rintis Mangku Joyo Diningrat Muhammad Misbahussalam Muhammad Salman Alfarisi Mukhtar Ghozali Mutiara Nur Annisa Najmi Fauziah Nasya Azzahra Ngatin, Agustinus Nidaulhusna, Anisa Nirmala Utami Nisa Rahmah Mujahidah Nurbaits, Alisya Nurcahyo Nurcahyo Nurhasanah, Santy Nurul Annisa Nurulgina, Rahma Permatasari, Rahma Puspa Putri, Angelina Rachmawati, Anissa Nurul Radianti Novita Sari Rafila Chika Azzahra Rahma Ardelia Raissa Rahma Ardelia Raissa Rahmawati, Sri Puji Ramadhan, Muhammad Zikri Ramadhani, Laily lsna Randi Reynaldi Retno Indarti Reynaldi, Randi Rian Muhamad Rizky Rivaldo Rofie Fauzi Budiman Rizky Fauzan Rizky Setianto Robby Sudarman Rony Pasonang Sihombing rony sihombing Rusdianasari Rusdianasari Sabinna Azahra Sulaeman Salsabila, Iva Najwa Salsabila, Salwa Ainaya Salsabila, Shafira Salsabilla, Iva Najwa Setiawan, Kiranna Shalmadevy Shafira Yulianthina Shoerya Shoelarta Sihombing, Rony Sihombing, Rony Pasonang Suminar, Dian Ratna Suryadi, Joko Synbi Pasya Octaviarine Adihartanto Teguh Aditya Nugraha Teguh Aditya Nugraha Tika Paramitha Tika Paramitha Tika Paramitha Tira Nur Khoirunisa Tri Reksa Saputra Trirahayu, Dhyna Analyes Unung Leoanggraini Yuki Martha Anggraini Yusuf, Yusmardhany Zahwa, Keisya Adellia