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All Journal Jurnal Teknologi Dan Industri Pangan VALENSI ILMU KELAUTAN: Indonesian Journal of Marine Sciences Jurnal Sains Materi Indonesia Microbiology Indonesia Majalah Ilmiah Ekonomi Komputer Jurnal Penelitian Hasil Hutan Agrointek Majalah Kulit, Karet, dan Plastik Jurnal Industri Hasil Perkebunan Indonesian Journal of Chemical Science INDONESIAN JOURNAL OF ESSENTIAL OIL Jurnal Ilmiah Ibnu Sina (JIIS): Ilmu Farmasi dan Kesehatan Indonesian Journal of Chemistry Biosaintifika: Journal of Biology & Biology Education Jurnal Pascapanen dan Bioteknologi Kelautan dan Perikanan Jurnal Ilmu Kefarmasian Indonesia Jurnal Penelitian Hasil Hutan Jurnal Ilmiah Ibnu Sina (JIIS): Ilmu Farmasi dan Kesehatan Jurnal Pijar MIPA Makara Journal of Science JURNAL REKAYASA KIMIA & LINGKUNGAN
Tun Tedja Irawadi
Chemistry Department, Faculty Of Mathematics And Natural Science, IPB University, Kampus IPB Dramaga, Bogor, 16680, Indonesia
Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Decision Sciences, Operations Research & Management Earth & Planetary Sciences Economics, Econometrics & Finance Energy Engineering Environmental Science Health Professions Immunology & microbiology Industrial & Manufacturing Engineering Materials Science & Nanotechnology Mathematics Medicine & Pharmacology Physics Public Health

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Journal : Indonesian Journal of Chemistry

 1 
Performance of Zinc-Difattyalkyldithyocarbamate as Anti-Friction/Anti-Wear Lubricant Additives Komar Sutriah; Zainal Alim Mas’ud; Tun Tedja Irawadi; Mohammad Khotib
Indonesian Journal of Chemistry Vol 14, No 1 (2014)
Publisher : Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (592.03 KB) | DOI: 10.22146/ijc.21271

Abstract

Dithyocarbamate is an organosulphur compound that has long been known and widely applied in various fields, including in agriculture and industry. Several variants of synthesized vegetable oil-based Zinc-difattyalkyldithyocarbamate were tested its anti-friction/anti-wear performance on four ball machine using the method of ASTM-D2783. Anti-friction/anti-wear test to six of additive variants of Zinc-difattyalkyldithyocarbamate at doses of 1.2% indicated that all variants of the product has welding point value higher than the lube base oil lubricant HVI 60, and from US Steel 136 standard for Hydraulic lubricants, but only two additive variants of Zinc-bis(lauryl palmityl)dithyocarbamate and Zinc-bis(lauryl oleyl)dithyocarbamate which has a larger load wear index value than the standard, and meet the criteria as an additive extreme pressure according to US steel 136 standard. Zinc-bis(lauryl palmityl)dithyocarbamate is an additive variant with the best performance, meet bi-functional lubricant additives criteria, as anti-friction/anti-wear and antioxidant additive.
SYNTHESIS OF ZINC-DIFATTYALKYLDITHIOCARBAMATES AND THEIR ANTIOXIDANT ACTIVITIES Komar Sutriah; Zainal Alim Mas’ud; Tun Tedja Irawadi
Indonesian Journal of Chemistry Vol 12, No 2 (2012)
Publisher : Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (444.768 KB) | DOI: 10.22146/ijc.21362

Abstract

Zinc-difattyalkyldithiocarbamates are organosulfur compounds with many functions, including as an antioxidant in a lubrication system. They were synthesized by reacting secondary fatty amine with ZnCl2 and CS2 giving result zinc-difattyalkyldithiocarbamates of around 77-87%. The synthesized products were characterized using infrared (IR) spectroscopic techniques. The IR spectra of zinc-difattyalkyldithiocarbamates showed sharp bands at 1450-1550 cm-1 for thioureida v (C-N), 950-1050 cm-1 for v (C-S), and in the far-red area 300-400 cm-1 for sulfur-metal bond. Products recovery was evaluated by AAS and the purity was analyzed by HPLC. Seven variants of zinc-difattyalkyldithiocarbamates were obtained. Antioxidant activity was evaluated by rancimat test regarding their induction time. At 125 ppm levels all variants showed higher value in each of their induction time as compared to those of butylated hydroxyanisole and butylated hydroxytoluene, commercial antioxidants No.1, and commercial antioxidants no.2. Three variants, i.e. Zn-bis(dilauryl)dithiocarbamate, Zn-bis(laurylpalmityl)dithiocarbamate, and Zn-bis(laurylstearyl)dithiocarbamate had higher values in their induction time than the other variants. The values are 16.67, 26.54, and 16.11 h, respectively.
Co-Authors . Muntamah A.A. Ketut Agung Cahyawan W Adi Cifriadi Afifi, Muhammad Ridho Ahmad Zakaria Aini, Zahratul Ali, Mohamad Makrus Amatullah, Afra Najiyah Amril Aman Anas Miftah Fauzi Ani Suryani Awan Purnawan Bambang Marwoto BAMBANG MARWOTO Bambang Marwoto Irawadi Cifriadi, Adi Dewi Sondari Djumali Mangunwidjaja Djumali Mangunwidjaja Dwi Setyaningsih ERWAHYUNI ENDANG PRABANDARI ERWAHYUNI ENDANG PRABANDARI Henny Purwaningsih Inda Iliyin Irma Herawati Suprapto Jorion Romengga Jorion Romengga Kapelle, Imanuel B. D. Khaswar Syamsu Komar Sutriah Komar Sutriah Krisnawati Krisnawati Krisnawati, Krisnawati Liesbetini Hartoto Liesbetini Hartoto LIESBETINI HARTOTO M. Syamsul Maarif Mas’ud, Zainal Alim Meika Syahbana Rusli Mira Rivai Mohamad Rafi Mohammad Khotib Muhammad Agus Muljanto Muhammad Hanafi Muhammad Romli dan Suprihatin Andes Ismayana Noviyan Darmawan Pamungkas, Wahyu Widji Puspitasari, Santi Retno Djulaika Rofiq Sunaryanto Rofiq Sunaryanto ROFIQ SUNARYANTO Santi Puspitasari Silvester Tursiloadi Sr Sugiarti Sugara, Taufan H Suharto Honggokusumo Suprapto, Irma Herawati Tanto Pratondo Utomo Taufan H Sugara Tetty Kemala Wahono Sumaryono Widia Citra Anggundari, Widia Citra Yandra Arkeman YOPI YOPI Zainal Alim Mas'ud Zainal Alim Mas'ud Zainal Alim Mas'ud ZAINAL ALIM MAS'UD Zainal Alim Mas’ud Zainal Alim Mas’ud Zainal Alim Mas’ud Zainal Alim Mas’ud