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PERBANDINGAN MOTEDE KONVENSIONAL EKSTRAKSI PEKTIN DARI KULIT BUAH PISANG DENGAN METODE ULTRASONIK Adhiksana, Arief
Journal of Research and Technology Vol 3, No 2 (2017)
Publisher : Universitas Nahdlatul Ulama Sidoarjo

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (94.741 KB) | DOI: 10.5281/zenodo.2581831

Abstract

The Banana is the most widely produced fruit in Indonesia with waste of banana peel about 1/3 of the fruit. If the banana peel is not utilized in large quantities it will cause environmental problems and is a waste of resources because the waste can still be utilized. The Banana peel contains a variety of compounds such as pectin 10-21%. Based on its content, banana peels have potential as a source of pectin. Pectin can be utilized in various industries of making jelly, jam, gelling, thickener, stabilizer andemulsifier. The purpose of this study was to find the influence of ultrasonic and mass on pectin yield. This research was conducted by using ultrasonic method extraction using 0.05 N HCl solvent of 400 mL and extraction temperature of 60 oC. variation of mass in this research are 5, 10, 20, 30 and 40 grams. The highest yield obtained in ultrasonic method is 20.0008 gram with yield of 25,59%. The conventional method only can reach 18,3%.
PENGARUH JUMLAH PELARUT PADA PROSES EKSTRAKSI MINYAK KAYU CENGKEH MENGGUNAKAN MICROWAVE Adhiksana, Arief; Kusyanto, .
Journal of Research and Technology Vol 1, No 01 (2015)
Publisher : Universitas Nahdlatul Ulama Sidoarjo

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (2949.226 KB) | DOI: 10.5281/zenodo.2581105

Abstract

Clove oil is usually produced from the leaves and flowers, while the twigs cloves actually have potential to be exploited. One of the latest methods that can be used is the microwave assisted extraction. The advantages of microwaves is its ability to deliver energy directly to all material, so it can save time compared to conventional extraction methods. This research aims to study the effect of solvents on the extraction using microwaves. The solvent is water because the polar so very good at absorbing microwave. The variables studied were the weight (75-150 grams) and volume of solvent (400-500 ml) , while the microwave power of 264 W. The choice of wood clove oil yield was obtained of 3.89 % on the amount of solvent to 500 ml with weight is 150 grams.
Pengaruh Waktu Dan Temperatur Hidrolisis Dalam Proses Sintesis Furfural Dari Sekam Padi Dengan Menggunakan Metode Hidrolisis Dan Dehidrasi Amborowati, Cindi; Adriani, Uni; Aditya, Indah Lukyta; Feviasari, Hanifati; Hastin, Tidar Kumala; Adhiksana, Arief
Journal of Research and Technology Vol 2, No 2 (2016)
Publisher : Universitas Nahdlatul Ulama Sidoarjo

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (109.415 KB) | DOI: 10.5281/zenodo.2582002

Abstract

Rice fields in East Kalimantan is one of productive land. It looks from many piles of rice husk waste in rice milling. The rice husk waste has not been used much, so this research used the rice husk waste as raw material of furfural manufacturing. This research has three stages, there are raw material preparation, hydrolysis, and product analysis. At the preparation stage, rice husk is diminished to 100 mesh, then dried in oven. Hydrolysis process used sulfuric acid 1% as catalyst with the variation times were 10, 40, 70, 100, 130 (minutes) and temperature are 30, 50, 70, 90, 105 (°C). Then hydrolysis result was filtered and the filtrate was quantitatively analyzed by volumetric method. Highest result of time variation obtained was at 130 minutes with furfural concentration as much 8,182 mol/L, while highest result of temperature variation obtained was at 105 °C with furfural concentration as much 10,741 mol/L.
PEMANFAATAN GELOMBANG MIKRO DALAM EKSTRAKSI ANTOSIANIN DARI KULIT BUAH NAGA SEBAGAI PENGGANTI RHODAMIN B UNTUK SEDIAAN PEWARNA BIBIR ALAMI Adhiksana, Arief; Jumardi, Andi; Kusyanto, Kusyanto; Andriani, Rina
Journal of Research and Technology Vol 3, No 1 (2017)
Publisher : Universitas Nahdlatul Ulama Sidoarjo

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (393.414 KB) | DOI: 10.5281/zenodo.2581960

Abstract

Today, microwave can be used in various chemical processes. The advantage of microwaves is able to deliver energy directly to the material. One of microwave application is the extraction process of natural materials. Microwaves can be used to reduce extraction process time of the anthocyanin from the dragon fruit skin. This research aims to determine the solvent extracted effect to the anthocyanin extraction of dragon fruit skin using microwaves. The solvent used was 95% ethanol, 85% ethanol, 75% ethanol, 95% ethanol –citric acid, 85% ethanol -acids and 75% - citric acid ethanol to the anthocyanin extraction results of dragon fruit skin extracted using microwaves. The consumption of microwave power is 400 watt with 50 gram of dragon fruits skin. Then, anthocyanin extracts are mixe with supporting materials to be made as lipstick and proposed for topical and favorite test. The best yield can be obtained by using ethanol-citric acid solvent at 25,031%.
Optimasi Produksi Sumur CBM dengan Radial Jet Drilling (RJD) Afifah, Rohima Sera; Karmila, Karmila; Adhiksana, Arief; Jumardi, Andi
JST (Jurnal Sains Terapan) Vol 6, No 1 (2020): JST (Jurnal Sains Terapan)
Publisher : Pusat Penelitian dan Pengabdian kepada Masyarakat, Politeknik Negeri Balikpapan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32487/jst.v6i1.748

Abstract

To produce gas methane from the coal bed methane (CBM) field requires the right completion system that considers the reservoir properties which are encountered. One of technologies that is recommended to produce gas methane in the CBM field is Radial Jet Drilling System (RJD). Two important aspects which are considered to test the feasibility of RJD in the CBM field are the problems that usually show up while drilling and producing. The other aspects are the principle of RJD that considers several special tools like radial jetting and length of radial and the problems that usually present during RJD’s application in conventional field like water blocking, hole positioning and hole cleaning. To see the effectiveness of RJD, a comparison with other completion systems (vertical well) is done through simulation step by using WS field data, precisely at BP formation. CBM field simulation that is produced with vertical well system is sensed by adding wells. Meanwhile the CBM field that is produced by RJD completion is sensed by the number of radial phases and the length of each phase.The results show that RJD can be applied in the CBM well with certain parameters then the RJD effectiveness can be achieved with the minimum number of three phases, where the distance of each phase is 90 degrees and length of each radial phase is 300 until 500 ft.Key words: Completion, CBM, RJD, radial jetting, water blocking, hole cleaning, hole positioning, simulation, WS fieldABSTRAK Untuk memperoleh produksi gas metan pada lapangan CBM maka dibutuhkan sistem komplesi yang tepat dengan tetap mempertimbangkan karakteristik reservoir CBM yang dihadapi.  Salah satu teknologi yang di rekomendasikan untuk memproduksi gas metan pada lapangan CBM adalah Radial Jet Drilling (RJD).Dua aspek penting yang dipertimbangkan untuk menguji kelaikan RJD pada lapangan CBM ialah masalah yang biasa muncul pada saat pemboran dan pada saat proses produksi. Aspek berikutnya adalah prinsip kerja RJD yang mempertimbangkan beberapa alat khusus seperti radial jetting dan panjang radial, serta masalah yang biasa muncul seiring dengan aplikasi RJD pada lapangan konvensional seperti water blocking, hole position dan hole cleaning.Sementara untuk melihat keefektifan RJD maka dilakukan perbandingan dengan sistem komplesi lain (sumur vertical) melalui tahap simulasi dengan menggunakan data lapangan WS tepatnya pada formasi BP. Simulasi lapangan CBM yang diproduksi dengan sistem sumur vertikal di sensitivitas dengan menambahkan sumur. Sedangkan lapangan CBM yang diproduksi dengan sistem komplesi RJD di sensitivitas terhadap jumlah fase radial dan panjang masing-masing fase.Hasil pengujian menunjukkan bahwa RJD dapat diaplikasikan pada sumur CBM dengan parameter tertentu sedangkan efektifitas RJD dapat dicapai pada jumlah fase minumum 3 (tiga), dengan jarak antara fase 90o dan dengan panjang radial masing-masing fase 300 ft – 500 ft.Kata kunci : Komplesi, CBM, RJD, radial jetting, water blocking, hole cleaning, hole position, simulasi, WS.
Implementation of appropriate technology programs in Tanjung Batu Village, Kutai Kartanegara, to realize an environmentally friendly independent village Surahman, Surahman; Ali, Sudirman; Adhiksana, Arief; Regiyana, Yuan; Hayati, Nuria
Community Empowerment Vol 6 No 9 (2021)
Publisher : Universitas Muhammadiyah Magelang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31603/ce.5964

Abstract

This community service program aims to realize Tanjung Batu village, Tenggarong Seberang District, Kutai Kartanegara Regency as an Independent Village in environmentally friendly livestock cultivation. This community service is carried out through Focus Group Discussions (FGD), implements Appropriate Technology product on SMEs and Maggot cultivation business actors as an alternative feed for high protein and inexpensive fish, and conducts social media management training for Youth Organizations. In addition, this PPTTG activity is also filled with training on the use of organic waste counting equipment and the cultivation of Maggot larvae for breeders and training for creative youth groups to use social media as a means of promoting SMEs products or promoting Tanjung Batu village as an independent village. The outputs produced in this PkM include improving the performance of partners, village officials, SMEs, and creative groups to produce more innovative and planned performance. So that Tanjung Batu village has a competitive advantage in human resources and produces high quality products that are marketed.
OPTIMIZATION OF RICE HUSK HYDROLYSIS TIME INTO FURFURAL ASSISTED BY MICROWAVE Marinda Rahim; Arief Adhiksana; Mina Indriani
Konversi Vol 8, No 2 (2019): Oktober 2019
Publisher : Universitas Lambung Mangkurat

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20527/k.v8i2.7013

Abstract

Rice production in East Kalimantan is quite high. In the process of milling usually rice husk obtained is about 20-30% from grains weight produced. The quite potential amount of rice husk  has not yet widely utilized, even though rice husk contains pentosan which can be processed into furfural by hydrolysis method.  The purpose of this research is to develop one step hydrolysis technique of rice husk into furfural  with  microwaves assistance to obtain the optimum time which can produce maximum furfural. In  this research 50 grams of rice husk was added with 500 mL of H2SO4 1% as the catalyst. The mixture was then hydrolyzed using microwave-assisted method with a time variety of 15, 30, 45, 60, 75, 90, 105 and 120  minutes.  The result of analysis by Gas Chromatography (GC) showed that the highest result of furfural was at 90 minutes with a yield of 2.923%.
HIDROLISIS AMPAS TEBU MENJADI FURFURAL DENGAN KATALISATOR ASAM SULFAT BERBANTUKAN GELOMBANG MIKRO Arief Adhiksana; Cantika Nawang Wulan; Nurul Hidayatul Islamiyah
JURNAL TEKNIK KIMIA VOKASIONAL (JIMSI) Vol 2, No 1 (2022): JURNAL TEKNIK KIMIA VOKASIONAL (JIMSI)
Publisher : Politeknik Negeri Samarinda

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (705.041 KB) | DOI: 10.46964/jimsi.v2i1.1472

Abstract

Tebu yang merupakan bahan proses pembuatan gula memiliki tingkat produksi yang tinggi di Indonesia. Hasil samping dari proses ini berupa ampas tebu yang jumlahnya mencapai 35–40% dari tebu gilingan. Pemanfaatan kembali ampas tebu masih belum optimal, padahal ampas tebu kaya akan pentosan dengan persentase 29,97% yang dapat diolah menjadi furfural dengan metode hidrolisis. Tujuan dari penelitian ini adalah mengetahui pengaruh konsentrasi katalisator asam sulfat dan waktu hidrolisis dalam pembuatan furfural dari ampas tebu berbantukan gelombang mikro. Pada penelitian ini ampas tebu dikeringkan dan diayak dengan ukuran -20 +70 mesh. Proses dijalankan menggunakan 15 gram ampas tebu pada variasi konsentrasi asam sulfat antara 1,5 M sampai dengan 3,5 M sebanyak 450 mL dan variasi waktu hidrolisis antara 20 menit sampai dengan 40 menit. Campuran dihidrolisis dengan bantuan gelombang mikro berdaya 600 W 50 Hz. Hidrolisat disaring dan filtratnya ditambahkan dengan kloroform untuk memisahkan furfural dengan sisa asam dan air. Produk furfural dianalisa kualitatif menggunakan anilin asetat dan analisa kuantitatif dengan Gas Chromatography (GC). Berdasarkan hasil analisa kualitatif, perubahan warna sampel dari kuning menjadi merah menandakan terbentuknya furfural. Akan tetapi, konsentrasi furfural yang didapatkan masih belum diketahui hasilnya secara kuantitatif menggunakan GC. 
PEMANFAATAN GELOMBANG MIKRO DALAM EKSTRAKSI ANTOSIANIN DARI KULIT BUAH NAGA SEBAGAI PENGGANTI RHODAMIN B UNTUK SEDIAAN PEWARNA BIBIR ALAMI Arief Adhiksana; Andi Jumardi; Kusyanto; Rina Andriani
Journal of Research and Technology Vol. 3 No. 1 (2017): JRT Volume 3 No 1 Jun 2017
Publisher : 2477 - 6165

Show Abstract | Download Original | Original Source | Check in Google Scholar

Abstract

Today, microwave can be used in various chemical processes. The advantage of microwaves is able to deliver energy directly to the material. One of microwave application is the extraction process of natural materials. Microwaves can be used to reduce extraction process time of the anthocyanin from the dragon fruit skin. This research aims to determine the solvent extracted effect to the anthocyanin extraction of dragon fruit skin using microwaves. The solvent used was 95% ethanol, 85% ethanol, 75% ethanol, 95% ethanol –citric acid, 85% ethanol -acids and 75% - citric acid ethanol to the anthocyanin extraction results of dragon fruit skin extracted using microwaves. The consumption of microwave power is 400 watt with 50 gram of dragon fruits skin. Then, anthocyanin extracts are mixed with supporting materials to be made as lipstick and proposed for topical and favorite test. The best yield can be obtained by using ethanol-citric acid solvent at 25,031%.
Effect of Catalysts H2SO4 8% and Baggase Ratio on Yield of Furfural with Hydrolysis Method Using Microwaves Arief Adhiksana; Ayu Chandra Kartika Fitri; Vini Kumara Lalita Siniwi; Medya Ayunda Fitri
Jurnal Teknik Kimia dan Lingkungan Vol. 6 No. 1 (2022): April 2022
Publisher : Politeknik Negeri Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (540.281 KB) | DOI: 10.33795/jtkl.v6i1.289

Abstract

Ampas tebu mengandung pentosan sebesar 12,7%. Kandungan pentosan yang cukup tinggi dalam ampas tebu dapat digunakan sebagai bahan baku pembuatan furfural melalui proses hidrolisis. Penelitian ini bertujuan untuk menentukan pengaruh rasio ampas tebu dan katalis H2SO4 terhadap yield furfural yang didapat dari proses hidrolisis menggunakan microwave. Ampas tebu ditambahkan dengan H2SO4 8% sebagai katalisator dengan variasi rasio ampas tebu dan katalisator H2SO4 yaitu 1:20, 1:30, 1:40, 1:50, dan 1:60 pada temperatur microwave 100oC dan waktu reaksi 75 menit. Sampel dianalisa secara kualitatif dengan uji warna menggunakan anilin- asetat sebagai pereaksi. Setelah anilin-asetat ditambahkan ke sampel, warna sampel berubah dari kuning cerah menjadi merah sebagai tanda sampel mengandung furfural. Furfural yang dihasilkan dianalisa untuk mengetahui yield dari furfural dengan menggunakan Gas Chromatography (GC). Hasil penelitian menunjukkan yield furfural terbaik pada rasio ampas tebu dan katalisator H2SO4 1:30 yakni sebesar 0,28%. The sugar cane bagasse contains 12.7% pentosan. The relatively high pentosan content in the sugar cane bagasse can be used as the raw material of furfural production by utilizing the hydrolysis process. This research aims to determine the effects of ratio variations of bagasse and H2SO4 catalyst on the yield of furfural obtained from the hydrolysis process using a microwave. The sugar cane bagasse was added with H2SO4 8% as catalyst with a variations ratio of sugar cane bagasse and H2SO4 catalyst that is 1:20, 1:30, 1:40, 1:50, and 1:60 in a microwave with the reaction temperature of 100oC and reaction time of 75 minutes. The sample was analyzed qualitatively with a color test by using aniline-acetic as the reactant. After the aniline-acetic was added to the sample, the color of the sample changed from bright yellow to red as a sign that the sample contains furfural. The obtained furfural was analyzed to find out the yield of furfural by using Gas Chromatography (GC). The research product showed that the best yield of furfural on the ratio of bagasse and H2SO4 catalyst of 1:30 is 0.28%.