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Degradation of Phenol Using Sonolysis and Photolysis by TiO2/RHAC Catalyst and Analysis with Spectrophotometer UV-VIS and HPLC Safni - Safni; Eno Okta Patricia; Trisna Ollinovela; Yulizar Yusuf
al Kimiya: Jurnal Ilmu Kimia dan Terapan Vol 10, No 1 (2023): al Kimiya: Jurnal Ilmu Kimia dan Terapan
Publisher : Department of Chemistry, Faculty of Science and Technology, UIN Sunan Gunung Djati Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.15575/ak.v10i1.24775

This study focuses on the degradation of phenol in aqueous solutions using photolysis and sonolysis methods. It investigates the impact of catalyst mass, types of light (UV-A, UV-C, and visible light), types of catalyst (RHAC, TiO2, and TiO2/RHAC), and processing time on phenol degradation. The phenol solutions are analyzed before and after degradation using Spectrophotometer UV-Vis and HPLC. The research aims to understand the factors influencing phenol degradation and provide a basis for further studies to enhance the efficiency of phenol removal. Results show significant improvements in degradation percentages of phenol by using TiO2/RHAC as the catalyst. Sonolysis achieves a degradation of 20.82% with a catalyst, which increases to 50.57% with the catalyst. Photolysis achieves a degradation of 29.06%, which rises to 91.99% with the catalyst. The highest degradation percentage is achieved using UV-A light for 5 hours with a catalyst mass of 30 mg of TiO2/RHAC catalyst. HPLC analysis confirms a decreased phenol concentration and the presence of intermediate compounds. The TiO2/RHAC catalyst demonstrates the promising potential for efficient phenol degradation in aqueous solutions.

Advancement in Green Synthesis of Titanium Dioxide : Photocatalytic and Larvicidal Activities – A review Deliza, Deliza; Safni, Safni; Zein, Rahmiana; Putri, Reza Audina
Hydrogen: Jurnal Kependidikan Kimia Vol 12, No 1 (2024): February 2024
Publisher : Universitas Pendidikan Mandalika

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33394/hjkk.v12i1.10655

Nanotechnology is a fast expanding field with several applications in science, engineering, healthcare, pharmaceutical, and other areas. Nanoparticles (NP) are frequently produced through a variety of physical and chemical methods. Recently, green synthesis technologies that are more simple, sustainable, and cost-effective have been developed. The environmentally friendly/sustainable synthesis of titanium dioxide nanoparticles (TiO2 NPs) has been in great demand in the previous quarter. Bioactive components found in organisms, such as plants, facilitate the processes of bio-reduction and restriction. This review described green synthesis of TiO2 NPs, the photocatalytical uses, and managing the larvicidal activity of disease-spreading mosquitoes. Various natural reducing agents including proteins, enzymes, phytochemicals, and others, are involved in the synthesis of TiO2 NPs. Current research findings and future concerns in a viable platform based on biologically meditated TiO2 nanostructures for industrial applications.

Training on Postharvest Guava Fruit Processing in KWT Jambu Biji, VII Koto Sungai Sariak, Pariaman Yefrida Yefrida; Refilda Refilda; Imelda Imelda; Refinel Refinel; Rahmiana Zein; Safni Safni; Admi Admi; Dheasy Gustira; Jihanul Khaira; Harza Dipajana Umardi
Warta Pengabdian Andalas Vol 31 No 3 (2024)
Publisher : Lembaga Penelitian dan Pengabdian kepada Masyarakat (LPPM) Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jwa.31.3.510-517.2024

Red guava fruit is one type of fruit that quickly changes colour, texture and spoilage. This is of course a problem for farmers. At harvest time, not all of the fruit is marketable. So sometimes farmers just leave the fruit on the tree, because if harvested it will only increase operational costs. The KWT Jambu Biji Bengke Sakato, VII Koto Sungai Sariak, Pariaman is a group of red guava farmers. They tried to find a solution to this problem by discussing with TIM PPM KIMIA UNAND of the Department of Chemistry, FMIPA, Universitas Andalas. Finally it was agreed that the solution was to make products from red guava. The products made in this program are dodol and red guava ice cream. The KWT members and the Tim PPM KIMIA UNAND together made these two types of products. The results obtained, dodol and ice cream made are quite delicious and have an attractive appearance. This product can be an alternative to red guava processing that has economic value.

Optimasi Pemanfaatan Katalis TiO2/Karbon Aktif (Sekam Padi) Untuk Degradasi Methyl Violet Secara Sonolisis dan Fotolisis Safni, Safni; Aldini, Tasya; Yefrida, Yefrida; Zilfa, Zilfa; Deliza, Deliza
REACTOR: Journal of Research on Chemistry and Engineering Vol 5, No 2: December 2024
Publisher : Politeknik ATI Padang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.52759/reactor.v5i2.156

The textile industry is a major contributor to pollution, with 10-15% of dyes lost in wastewater during processing, including Methyl Violet. The degradation products of these dyes are often carcinogenic. Conventional biological treatment methods are ineffective due to the complex nature of synthetic dyes. A study aimed to develop a new photocatalytic activity using a UV A lamp and sonolysis using a sonicator. The study modified TiO2/Activated Carbon from Rice Husk as a catalyst to degrade Methyl Violet and textile industry effluent effectively, which was dual benefits as an adsorbent-photocatalyst. Results showed that the degradation by sonolysis and photolysis was 12.99% and 79.16%, respectively. The degradation by photolysis was 14.95% and 94.12%. The light and catalyst with the highest percentage of degradation were TiO2/activated carbon with UV A light of 94.12%. This study aims to develop effective treatment techniques for the textile industry's dyes.

Pembuatan Teh Daun Kelor untuk Peningkatan Ekonomi Masyarakat di Kecamatan Ulakan Tapakis, Padang Pariaman Matlal Fajri Alif; Yulizar Yusuf; Emriadi Emriadi; Deswati Deswati; Mai Efdi; Novesar Jamarun; Syukri Arief; Adlis Santoni; Bustanul Arifin; Suryati Suryati; Yetria Rilda; Safni Safni; Zilfa Zilfa; Olly Norita Tetra
Warta Pengabdian Andalas Vol 31 No 4 (2024)
Publisher : Lembaga Penelitian dan Pengabdian kepada Masyarakat (LPPM) Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jwa.31.4.682-688.2024

The Moringa plant, a tropical species, exhibits prolific growth and is abundantly present in Indonesia and other tropical regions worldwide. An extended lifespan, continuous flowering, and a high tolerance for elevated temperatures characterize it. Utilizing its components, including leaves, bark, seeds, and roots, this multifaceted plant is renowned for its therapeutic properties. The plant's antioxidants and various nutrients, including vitamins and minerals (iron, magnesium, vitamin B6, vitamin B2, vitamin C, and vitamin A), have led to studies on the plant's potential health benefits. In order to develop the local economy in Ulakan village, Padang Pariaman Regency, Moringa plants were processed by using the plant leaves to manufacture herbal tea, which can then be sold. This community service program was significant given the widespread presence and ease of cultivation of Moringa plants within the local region. The program involved the planning and selection of the activity site, the implementation of training sessions, and the assessment of the program's outcomes. The result of this community engagement initiative was the demonstrated interest of many participants in producing Moringa leaf tea.

Training on Postharvest Guava Fruit Processing in KWT Jambu Biji, VII Koto Sungai Sariak, Pariaman Yefrida Yefrida; Refilda Refilda; Imelda Imelda; Refinel Refinel; Rahmiana Zein; Safni Safni; Admi Admi; Dheasy Gustira; Jihanul Khaira; Harza Dipajana Umardi
Warta Pengabdian Andalas Vol 31 No 3 (2024)
Publisher : Lembaga Penelitian dan Pengabdian kepada Masyarakat (LPPM) Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jwa.31.3.510-517.2024

Red guava fruit is one type of fruit that quickly changes colour, texture and spoilage. This is of course a problem for farmers. At harvest time, not all of the fruit is marketable. So sometimes farmers just leave the fruit on the tree, because if harvested it will only increase operational costs. The KWT Jambu Biji Bengke Sakato, VII Koto Sungai Sariak, Pariaman is a group of red guava farmers. They tried to find a solution to this problem by discussing with TIM PPM KIMIA UNAND of the Department of Chemistry, FMIPA, Universitas Andalas. Finally it was agreed that the solution was to make products from red guava. The products made in this program are dodol and red guava ice cream. The KWT members and the Tim PPM KIMIA UNAND together made these two types of products. The results obtained, dodol and ice cream made are quite delicious and have an attractive appearance. This product can be an alternative to red guava processing that has economic value.

Pembuatan Teh Daun Kelor untuk Peningkatan Ekonomi Masyarakat di Kecamatan Ulakan Tapakis, Padang Pariaman Matlal Fajri Alif; Yulizar Yusuf; Emriadi Emriadi; Deswati Deswati; Mai Efdi; Novesar Jamarun; Syukri Arief; Adlis Santoni; Bustanul Arifin; Suryati Suryati; Yetria Rilda; Safni Safni; Zilfa Zilfa; Olly Norita Tetra
Warta Pengabdian Andalas Vol 31 No 4 (2024)
Publisher : Lembaga Penelitian dan Pengabdian kepada Masyarakat (LPPM) Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jwa.31.4.682-688.2024

The Moringa plant, a tropical species, exhibits prolific growth and is abundantly present in Indonesia and other tropical regions worldwide. An extended lifespan, continuous flowering, and a high tolerance for elevated temperatures characterize it. Utilizing its components, including leaves, bark, seeds, and roots, this multifaceted plant is renowned for its therapeutic properties. The plant's antioxidants and various nutrients, including vitamins and minerals (iron, magnesium, vitamin B6, vitamin B2, vitamin C, and vitamin A), have led to studies on the plant's potential health benefits. In order to develop the local economy in Ulakan village, Padang Pariaman Regency, Moringa plants were processed by using the plant leaves to manufacture herbal tea, which can then be sold. This community service program was significant given the widespread presence and ease of cultivation of Moringa plants within the local region. The program involved the planning and selection of the activity site, the implementation of training sessions, and the assessment of the program's outcomes. The result of this community engagement initiative was the demonstrated interest of many participants in producing Moringa leaf tea.

Analysis of Water-Soluble Vitamin Change in Tomato (S.lycopersicum) Due to Ozonolysis of Imidacloprid Degradation Treatment by Using Spectrometry and HPLC Method Donanita, Tysa; Safni, Safni; Suryati , Suryati
Jurnal Akademika Kimia Vol. 12 No. 2 (2023)
Publisher : Universitas Tadulako

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/j24775185.2023.v12.i2.pp92-99

In this study, the effect of imidacloprid degradation on the reduction of water-soluble vitamins in tomatoes was observed, such as ascorbic acid, pyridoxine, niacin, and thiamine. Analysis was carried out using a spectrophotometer and high-performance liquid chromatography. The degradation method with ozone water for 15 minutes showed a better result than the ozonolysis method because the decrease in levels of water-soluble vitamins is smaller. The percentage decrease of each water-soluble vitamin in the ozone water method is ascorbic acid by 17.103 %, pyridoxine by 6.723 %, niacin by 2.781 %, and thiamine by 0.333 %. Ozone water methods also produce a high percentage of degradation which is 90.56 %.

Advancement in Green Synthesis of Titanium Dioxide : Photocatalytic and Larvicidal Activities â€“ A review Deliza, Deliza; Safni, Safni; Zein, Rahmiana; Putri, Reza Audina
Hydrogen: Jurnal Kependidikan Kimia Vol. 12 No. 1 (2024): February 2024
Publisher : Universitas Pendidikan Mandalika

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33394/hjkk.v12i1.10655

Nanotechnology is a fast expanding field with several applications in science, engineering, healthcare, pharmaceutical, and other areas. Nanoparticles (NP) are frequently produced through a variety of physical and chemical methods. Recently, green synthesis technologies that are more simple, sustainable, and cost-effective have been developed. The environmentally friendly/sustainable synthesis of titanium dioxide nanoparticles (TiO2 NPs) has been in great demand in the previous quarter. Bioactive components found in organisms, such as plants, facilitate the processes of bio-reduction and restriction. This review described green synthesis of TiO2 NPs, the photocatalytical uses, and managing the larvicidal activity of disease-spreading mosquitoes. Various natural reducing agents including proteins, enzymes, phytochemicals, and others, are involved in the synthesis of TiO2 NPs. Current research findings and future concerns in a viable platform based on biologically meditated TiO2 nanostructures for industrial applications.

Optimasi Pemanfaatan Katalis TiO2/Karbon Aktif (Sekam Padi) Untuk Degradasi Methyl Violet Secara Sonolisis dan Fotolisis Safni, Safni; Aldini, Tasya; Zilfa, Zilfa; Deliza , Deliza
REACTOR: Journal of Research on Chemistry and Engineering Vol. 5 No. 2 (2024)
Publisher : Politeknik ATI Padang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.52759/reactor.v5i2.156

The textile industry is a major contributor to pollution, with 10-15% of dyes lost in wastewater during processing, including Methyl Violet. The degradation products of these dyes are often carcinogenic. Conventional biological treatment methods are ineffective due to the complex nature of synthetic dyes. A study aimed to develop a new photocatalytic activity using a UV A lamp and sonolysis using a sonicator. The study modified TiO2/Activated Carbon from Rice Husk as a catalyst to degrade Methyl Violet and textile industry effluent effectively, which was dual benefits as an adsorbent-photocatalyst. Results showed that the degradation by sonolysis and photolysis was 12.99% and 79.16%, respectively. The degradation by photolysis was 14.95% and 94.12%. The light and catalyst with the highest percentage of degradation were TiO2/activated carbon with UV A light of 94.12%. This study aims to develop effective treatment techniques for the textile industry's dyes.

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