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Antioxidant Capacity, Phytochemical Profile, and Clustering of Pomegranate (Punica granatum L.) Peel Extracts Using Different Solvent Extraction Rafi, Mohamad; Wulansari, Laela; Septaningsih, Dewi Anggraini; Purnomo, Tsania Firqin; Auliatifani, Reza; Khaydanur, Khaydanur; Ilmiawati, Auliya; Yulianti, Wina; Nengsih, Nunuk Kurniati; Suparto, Irma Herawati; Kusuma, Wisnu Ananta
Journal of Tropical Life Science Vol 11, No 3 (2021)
Publisher : Journal of Tropical Life Science

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Abstract

Pomegranate has valuable nutritional content and contains various bioactive compounds, one found in the fruit's peel. The utilization of these bioactive compounds could be used as herbal medicines and supplements, such as antioxidants. This study aimed to determine the antioxidant capacity, phytochemical profile, and pomegranate peel extract grouping using different extracting solvents. The three extracting solvents used were water, 70% ethanol, and ethanol p.a. Antioxidant capacity of the three extracts was measured using the DPPH and CUPRAC methods. We also determined the total phenolic and flavonoid levels and the TLC fingerprint analysis and FTIR spectrum of the pomegranate peel extracts. The 70% ethanol extract owned the largest antioxidant capacity than the other two extracts with a value of 358.67 and 2981.59 µmol trolox/g dried sample using the DPPH and CUPRAC methods, respectively. The three pomegranate peel extracts' total phenolic and flavonoid levels ranged from 287.26–1068.81 mg GAE/g dried sample and 0.24-0.75 mg QE/g dried sample. TLC fingerprint analysis of pomegranate peel extract yielded 2, 6, and 6 bands for water extract, 70% ethanol, and p.a ethanol, respectively. The three extracts can be grouped based on FTIR spectrum data using principal component analysis using three principal components with a total variance of 93%. The results obtained show that using different extracting solvents provides different antioxidant capacities and phytochemical profiles.
KINETIKA ADSORPSI AMMONIUM DARI KOPOLIMER SELULOSA JERAMI PADI DENGAN ASAM AKRILAT DAN AKRILAMIDA Wina Yulianti
Jurnal Biofisika Vol. 8 No. 2 (2012): Jurnal Biofisika
Publisher : Jurnal Biofisika

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Abstract

Copolymerization  of  cellulose  from  rice  straw  with  acrylic  acid  and  acrylamide produce  biodegradable  superabsorbent  Copolymerization  was  carried out  at  65  C under nitrogen athmosphere.  Initiator and cross linking agent  used were potassium peroxodisulfate  and  N'N-methylene  bis  acrylamide.  Superabsorbent  produced  is anionic,  that  can  bind  ammonium  cation.  The  kinetics  of  swelling  adsorption  was following pseudo second-order equation.
Pelatihan Pengenalan Kopi dari Bean ke Cup di Sekolah Islam Terpadu Insantama Leuwiliang, Bogor Hidayati Fatchur Rochmah; Ade Astri Muliasari; Wina Yulianti
Agrokreatif: Jurnal Ilmiah Pengabdian kepada Masyarakat Vol. 8 No. 1 (2022): Agrokreatif Jurnal Ilmiah Pengabdian Kepada Masyarakat
Publisher : Institut Pertanian Bogor

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29244/agrokreatif.8.1.32-39

Abstract

Educational activities introducing coffee plants from bean to cup in community service activities had been carried out at the Integrated Islamic School (SIT) Insantama Leuwiliang, Bogor. The method of implementing activities were carried out in two ways, offline for teacher and online for student participants. Material delivery using presentation methods and simulations coffee cup testing. Evaluation of community service activities were carried out by distributing questionnaires. Evaluation of the results of community service activities at SIT Insantama Leuwiliang showed that community service activities were useful and received good responses from teachers and junior high school students. Submission of materials in introduction to coffee plants is important and has been conveyed clearly. The results of the selection materials, needed for further community service activities are materials related to junior high school students in the form of experiments, making tofu and tempe, effective online learning methods, fruit cultivation, plant cultivation in narrow yard (housing), making hand soap, the introduction of Covid 19 and making of meatballs.
SINTESIS DAN KARAKTERISASI SUPERABSORBEN DARI SELULOSA JERAMI PADI (Superabsorbent Synthesis and Characterization of Rice Straw Cellulose) Wina Yulianti; Farida Laila
Jurnal Sains Terapan : Wahana Informasi dan Alih Teknologi Pertanian Vol. 4 No. 1 (2014): Jurnal Sains Terapan, Volume 4, Nomor 1, Tahun 2014
Publisher : IPB University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (587.451 KB) | DOI: 10.29244/jstsv.4.1.46-52

Abstract

Copolymerization of cellulose from rice straw with acrylic acid and acrylamide produce biopolymer superabsorbent. Cellulose was purified from fat content by extraction with toluene:ethanol (2:1). Hemicelluloses and lignin were removal by using potassium hydroxide 5% and hydrogen peroxide 2% at alkaline pH. Cellulose yield obtained was 21.56%. FTIR spectra of lignin showed a loss of absorption at 1728 cm-1. Copolymerization was carried out at 65 C under nitrogen athmosphere. Initiator and cross linking agent used were potassium peroxodisulfate and N'N-methylene bis acrylamide. Superbasorben resulted from this experiment showed the water swelling capacity after 24 hour for the water, solution of 100 ppm of ammonium chloride, and urea respectively 387,11 g/g ; 193,47 g/g and 400,17 g/g.Keywords : superabsorbent, rice straw, swelling capacity
POTENSI EKSTRAK DAUN KERSEN SEBAGAI BAHAN SANITASI KERABANG TELUR PADA PROSES PENETASAN TELUR ITIK ALABIO: The Potential Of Cherry Leaf Extract (Mutinga calabura L) As A Sanitary Agent For Eggshell In The Alabio Ducks Hatching Process Gilang Ayuningtyas; Rina Martini; Wina Yulianti
Jurnal Sains Terapan : Wahana Informasi dan Alih Teknologi Pertanian Vol. 10 No. 2 (2020): Jurnal Sains Terapan, Volume 10 Nomor 2, Tahun 2020
Publisher : IPB University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (220.9 KB) | DOI: 10.29244/jstsv.10.2.50-61

Abstract

The objective of this research was to study the potential of cherry leaf extract as natural sanitizer agent for Alabio eggshell in hatching process. A number of 533 of Alabio hatching eggs were used in this study. Hatching eggs produced from College of Vacational Studies IPB University, were collected three times a day. Three hundred thirty-three hatching eggs were divided into five treatment groups. The first group was considered as control, the second was dipping into commercial disinfection, and the third and the fifth gruop were dipping into cherry leaf extract 250 ppm, 500 ppm, and 750 ppm respectively. The results showed cherry leaf extract has secondary metabolite compounds : alkaloids, flavonoids and tannins. All of these secondary metabolite compounds have a role as antibacterial agent. cherry leaf extract 750 ppm shows the same potential as commercial disinfectants in reducing the microbial population in eggshells. The dipping treatment of 750 ppm cherry leaf extract in alabio duck hatching eggs resulted in the lowest embryo mortality rate compared to other treatments (9.3%). Key words: Alabio duck, cherry leaf extract, hatchery, total plate count of eggshell
PENGARUH METODE EKSTRAKSI DAN POLARITAS PELARUT TERHADAP KADAR FENOLIK TOTAL DAUN KERSEN (Muntingia calabura L): Effect of Extraction Method and Solvent Polarity on Total Phenolic Content of Cherry Leaves (Muntingia calabura L) Wina Yulianti; Gilang Ayuningtyas; Rina Martini; Ika Resmeiliana
Jurnal Sains Terapan : Wahana Informasi dan Alih Teknologi Pertanian Vol. 10 No. 2 (2020): Jurnal Sains Terapan, Volume 10 Nomor 2, Tahun 2020
Publisher : IPB University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (201.223 KB) | DOI: 10.29244/jstsv.10.2.41-49

Abstract

ABSTRACTThe method of extraction and the type of solvent used during extraction will influence effectiveness of the extraction and compound extracted. The aim of this research was determined the effect of extraction methode and solvent polarity on total phenolic content of cherry leaves (Muntingia calabura L). Extraction of cherry leaves used maceration and soxhelation methods with ethanol and chloroform as solvents. The total phenolic contain was determined by visible spechtrophotometer at 765 nm. It has been showed that the soxhletation method was a higher yield value than the maceration methods with the highest yield value showed by ethanol extract, it was 13,29% w/w. Otherwise maceration method showed a higher total phenolic contain with the highest total phenolic contain showed by ethanol extract, it was 10,70% GAE.
Determination of Nitrite and Nitrate Level in Wastewater Discharge from Smoked Fish Industry Wina Yulianti; Ima Kusumanti; Nurul Jannah
JURNAL SAINS NATURAL Vol. 12 No. 1 (2022): Sains Natural
Publisher : Universitas Nusa Bangsa

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (485.586 KB) | DOI: 10.31938/jsn.v12i1.323

Abstract

This research aimed to determine nitrite and nitrate contamination in wastewater discharge from the smoked fish industry around the fishpond area in Penatarsewu village, Sidoarjo East Java. Samples were taken from ten locations along The Alo River from September to November 2020. Nitrate and nitrite levels were determined by the Standard Method for Examination of Water and Wastewater 4500-NO2-B dan 4500-NO3-B. Nitrite formed a reddishpurple azo dye produced by coupling diazotized sulfanilamide with N-(1-naphthyl)-ethylene-diamine dihydrochloride after a visible spectrophotometer measured the complexes nitrite at wavelength 543 nm. Meanwhile, the Nitrate level was determined by ultraviolet spectrophotometer at a wavelength of 220 nm. The standard nitrite calibration curve was shown by the line equation y= 3,30361x-0,0028 and a determination coefficient of 0.9999. Whereas the standard nitrate was showed by the line equation y=0,2507x + 0,0067 and a determination coefficient 0,9996. The level of nitrate and nitrite in the sample ranged from 0.05-0.93mg / L 1,2-1,6 mg / L. According to a quality standard threshold value for nitrite and nitrate-based on the Government Regulation of the Republic of Indonesia (PPRI) No.82 2001 is 0,06mg/L and 10 mg/L, therefore it can be concluded that some samples are above the threshold value for nitrite level.Keywords: Alo River,  nitate,  nitrite,  smoked fish,  spectrophotometerPenentuan Kadar Nitrit dan Nitrat Pembuangan Limbah Cair Industri Ikan AsapABSTRAKPenelitian bertujuan untuk menentukan tingkat kontaminasi nitrat dan nitrit pada limbah industri ikan asap di sekitar kawasan tambak ikan asap di Desa Penatarsewu, Sidoardjo, Jawa Timur. Sampel diambil dari 10 titik  di areal sekitar tambak sepanjang badan Sungai Alo pada bulan September sampai November 2020. Penentuan kadar nitrat dan nitrit mengacu pada Standard Methods for the Examination Water and Wastewater 4500-NO2-B dan 4500-NO3-B. Nitrit membentuk kompleks ungu kemerahan yang dihasilkan dari kopling sulfanilamida dengan N-(1-naptil)-etilena-diamina dihidroklorida kemudian kadarnya ditentukan dengan spektrofotometer sinar tampak pada panjang gelombang 543 nm. Kadar nitrat ditentukan menggunakan spektrofotometer ultraviolet pada panjang gelombang 220 nm. Hasil pengukuran standar nitrit menghasilkan persamaan garis y=3,30361x-0,0028 dengan koefesien determinasi 0,999 dan standar nitrat menghasilkan persamaan garis y=0,2507x+0,0067 dengan koefesien determinasi 0,9996. Kadar nitrit dan nitrat secara berturut-turut berkisar antara 0,05-0,93 mg/L dan 1,2-1,6 mg/L. Berdasarkan nilai ambang batas baku mutu nitrit dan nitrat berdasarkan Peraturan Pemerintah Republik Indonesia (PPRI) No.82 tahun 2001 adalah 0,06 mg/L dan 10 mg/L, maka dapat disimpulkan bahwa beberapa sampel mengandung kadar nitrit  di atas ambang batas.Kata kunci : ikan asap, nitrat, nitrit, Sungai Alo, spektrofotometer
Antioxidant Capacity, Phytochemical Profile, and Clustering of Pomegranate (Punica granatum L.) Peel Extracts Using Different Solvent Extraction Mohamad Rafi; Laela Wulansari; Dewi Anggraini Septaningsih; Tsania Firqin Purnomo; Reza Auliatifani; Khaydanur Khaydanur; Auliya Ilmiawati; Wina Yulianti; Nunuk Kurniati Nengsih; Irma Herawati Suparto; Wisnu Ananta Kusuma
Journal of Tropical Life Science Vol. 11 No. 3 (2021)
Publisher : Journal of Tropical Life Science

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.11594/jtls.11.03.14

Abstract

Pomegranate has valuable nutritional content and contains various bioactive compounds, one found in the fruit's peel. The utilization of these bioactive compounds could be used as herbal medicines and supplements, such as antioxidants. This study aimed to determine the antioxidant capacity, phytochemical profile, and pomegranate peel extract grouping using different extracting solvents. The three extracting solvents used were water, 70% ethanol, and ethanol p.a. Antioxidant capacity of the three extracts was measured using the DPPH and CUPRAC methods. We also determined the total phenolic and flavonoid levels and the TLC fingerprint analysis and FTIR spectrum of the pomegranate peel extracts. The 70% ethanol extract owned the largest antioxidant capacity than the other two extracts with a value of 358.67 and 2981.59 µmol trolox/g dried sample using the DPPH and CUPRAC methods, respectively. The three pomegranate peel extracts' total phenolic and flavonoid levels ranged from 287.26–1068.81 mg GAE/g dried sample and 0.24-0.75 mg QE/g dried sample. TLC fingerprint analysis of pomegranate peel extract yielded 2, 6, and 6 bands for water extract, 70% ethanol, and p.a ethanol, respectively. The three extracts can be grouped based on FTIR spectrum data using principal component analysis using three principal components with a total variance of 93%. The results obtained show that using different extracting solvents provides different antioxidant capacities and phytochemical profiles.
Evaluasi Kadar Senyawa Fenolat, Flavonoid Total, serta Aktivitas Antioksidan Secara in vitro dalam Ekstrak Metanol Bawang Dayak (Eleutherine palmifolia (L.) Merr : Evaluation of Phenolic Compounds, Total Flavonoid Content and in vitro Antioxidant Activity of Methanol Extract of Dayak Onion Bulbs (Eleutherine palmifolia (L.) Merr Farida Laila; Ika Resmeliana; Wina Yulianti; Atep Dian Supardan
KOVALEN: Jurnal Riset Kimia Vol. 8 No. 3 (2022): December Edition
Publisher : Chemistry Department, Mathematics and Natural Science Faculty, Tadulako University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/kovalen.2022.v8.i3.16175

Abstract

Dayak onion bulbs are a plant originating from Kalimantan which has been used for generations to treat various diseases. This plant is quite easy to grow and develop in many places in Indonesia. The aims of the present study were to evaluate the antioxidant potential of the methanol extract of Dayak onion bulbs based on the total of the phenolic and flavonoids contents and also the antioxidant activity using 2,2-diphenyl-1-picrylhydrazyl (DPPH) free radical scavenging ability, ferric reducing power and total antioxidant capacity. The results showed the total phenolic and flavonoid methanol extract of Dayak onion bulbs were 14.49 ± 1.42 mg GAE/g dry weight and 5.41 ± 1.01 mg QE/g dry weight, respectively. Antioxidant activity as measured by the DPPH, total antioxidant capacity, and ferric reduction assay with IC50 values of 16.95 ± 1.58 μg/mL, 24.22 ± 2.51 µg/mL, and 85.40 ± 16.88 µg/mL, respectively. These results suggest that the methanol extract of Dayak onion bulbs has potential bioactive compounds with good antioxidant activity and can be developed as an effective and safe source of natural compounds for functional food or herbal medicine.
KONSERVASI SUMBER DAYA ALAM DALAM PERSPEKTIF ISLAM Syariful Anam, Muhammad; Yulianti, Wina; Nur Safitri, Sari; Nur Qolifah, Siti; Rosia, Rina
Al-Madaris Jurnal Pendidikan dan Studi Keislaman Vol. 2 No. 1 (2021): Islamic Studies
Publisher : Lembaga Penelitian dan Pengabdian Masyarakat (LP2M) Sekolah Tinggi Agama Islam Jamiatut Tarbiyah Lhoksukon

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.47887/amd.v2i1.19

Abstract

This study examines how Islam views natural resource conservation. This is a qualitative research with a descriptive approach. Based on the results of the studies that have been carried out, it can be concluded that Islam teaches humans to be responsible for all of Allah's creation, including being responsible for protecting and maintaining natural resource ecosystems. The principle of conservation in Islam is based on mutual care between humans and nature, because basically humans take advantage of the available natural resources. In addition, in the utilization of natural resources, humans must pay attention to balance, not be exploitative and remain proportional so that natural resources are preserved.