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R.Y. Perry Burhan, R.Y. Perry
Department Of Chemistry Institut Teknologi Sepuluh Nopember
Aerospace Engineering Agriculture, Biological Sciences & Forestry Arts Humanities Automotive Engineering Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Control & Systems Engineering Decision Sciences, Operations Research & Management Earth & Planetary Sciences Education Electrical & Electronics Engineering Energy Engineering Environmental Science Industrial & Manufacturing Engineering Languange, Linguistic, Communication & Media Materials Science & Nanotechnology Mathematics Mechanical Engineering Physics Public Health Social Sciences Other

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Journal : Journal of Environmental Engineering and Sustainable Technology

 1 
METHOD OF ANALYSIS FOR DETERMINATION OF THE CHROMIUM (Cr) SPECIES IN WATER SAMPLES BY SPECTROPHOTOMETRY WITH DIPHENYLCARBAZIDE Adam Wiryawan; Rurini Retnowati; Perry Burhan; Syekhfani Syekhfani
Journal of Environmental Engineering and Sustainable Technology Vol 5, No 1 (2018)
Publisher : Lembaga Penelitian dan Pengabdian kepada Masyarakat Universitas Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (447.166 KB) | DOI: 10.21776/ub.jeest.2018.005.01.6

Abstract

Speciation of Chromium (Cr) is very important because of the toxicity of these metals depending on the oxidation number and its concentration is very low in the water system. Chromium occurs in the environment primarily in two valence states, trivalent Cr(III) and hexavalent Cr(VI). Chromium (III) is an essential micro-nutrients for the human body, while the Cr(VI) is highly toxic and carcino-gennic. Chromium(VI) in the water can be analyzed by spectrophotometry with diphenylcarbazide as reagent on pH=1 at maximum wavelength of 540 nm. The experimental result show that Cr(VI) can be analyzed using diphenylcarbazide in the concentration of 0.0015% and H3PO4 solution as acidic in 0.03 mol/L. The absorbance was measured at minutes 5 after preparation. There is interference from ion Fe(III) at least 6.0 ppm and this interference can be overcome by using 0.3 % NaF solution. The limit of detection of this method is -samples, mix of Cr(III) and Cr(VI), can be analyzed by using this method without oxidation by KMnO4 solution. While Cr(III)  in the artificial samples, mix of Cr(III) and Cr(VI), can be analyzed by using this method via oxidation by KMnO4 solution in the acidic media (H2SO4), the result of this analysis is the total concentration of Chromium. The concen-tration of Cr(III) can be calculate via subtract the total of Cr concentration by concentration of Cr(VI).Keywords: speciation, Cr(III), Cr(VI), spectropho-tometry, diphenylcarbazide, Fe(III), interference.
Co-Authors Abduh Muharram Chairacita Adam Wiryawan Agus Wahyudi Agus Wahyudi Agus Wahyudi Agus Wahyudi Amirotul Ula Anis Febriati Arga Dias Pratama Arizal Firmansyah Arizal Firmansyah Aufa Fadhliah Aulia, Wulan Awalia Wardatil Firdaus Batari, Nirmala Puteri Christoffel S I Maweikere Didik Prasetyoko Dyah Nirmala Edi, Eduardus Endah Mutiara Endah Mutiara Marhaeni Putri Endah Mutiara Marhaeni Putri Fahimah Martak Fina Riandra Firdausa, Yunita Alfiyati Firdhausya, Talitha Fitra Gunawan, Triyanda Hamzah Fansuri Hariyanto, Rhiby Ainur Basit Hidayati, Ririn Eva Imam B. Sosrowidjojo Iqbal, Rendy Muhamad Jein Jelsi Lamia Kusuma, Hendra Siswanto Lukman Atmaja Lukman Sugiharto Wijaya M. Nadjib M M. Nadjib Mujahid M. Rachimoellah M. Rachimoellah Maulida Fitriyyah Meliana Wahyuningtyas Miranti Widi Puspita Ayu Mujahid, M. Nadjib Mujahid, Muhammad Nadjib Nadjib, Muhammad Nia Nurfitria Novesar Jamarun Nugraheni, Zjahra Vianita Nurul Jadid Pusparatu Pusparatu Putri, Endah Mutiara Marhaeni Putri, Rizka Berliana R. Arizal Firmansyah Ramadhan, Zein Firdaus Rhiby Ainur Basit Hariyanto Riandra, Fina Riandra, Fina Ridho Bayuaji Rizka, Rizka Berliana Rurini Retnowati Sholihah, Sovia Masfuri Walidatus Silvana Dwi Nurherdiana Sosrowidjojo, Imam B. Sosrowidjojo, Imam B. Sovia Masfuri Walidatus Sholihah Spanton, Perdana Ixbal Subaer - Supiana Dian Nurtjahyan Supriadi, Warih Syekhfani Syekhfani Titik Andriani Wahyu Prasetyo Utomo Wijaya, Lukman Sugiharto Zein Firdaus Ramadhan Zetra, Yulfi Zetra, Yulfi Zjahra Vianita Zjahra Vianita Nugraheni