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HIGH VALUED LIMONENE IN ESSENTIAL OIL EXTRACT FROM LIME PEEL WASTE FOR PARFUM INDUSTRY Rosdanelli Hasibuan; Rita Sundari; Elisabeth Gultom; Rini Anggraini; Juliza Hidayati
AGROINTEK Vol 15, No 4 (2021)
Publisher : Agroindustrial Technology, University of Trunojoyo Madura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21107/agrointek.v15i4.10098

Limonene in essential oils is highly valuable attracts great interest of consumers due to its specific fragrance. It is not surprising that many big perfume industries are looking for high purified limonene found in essential oils of certain fruits and flowers. This study investigates the extraction process of essential oil from lime peel waste. This study has used two extraction methods, i.e. maceration method and Soxhlet technique. Two types of organic solvent applied, i.e. hexane and ethanol. This work studies the effect of extraction time, type of organic solvent, and extraction method on yield of extraction. Characterization studies as FTIR (Fourier Transform Infra Red) Spectroscopy related to type of chemical bonding of limonene in essential oil and GC-MS (Gas Chromatography – Mass Spectrometry) related to limonene fragmentation have also investigated.

FIBERGLASS CIRCULAR TURBULATOR IN COUNTER FLOW DOUBLE PIPE HEAT EXCHANGER: A STUDY OF HEAT TRANSFER RATE AND PRESSURE DROP Sudiono Sudiono; Rita Sundari; Rini Anggraini
SINERGI Vol 25, No 1 (2021)
Publisher : Universitas Mercu Buana

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22441/sinergi.2021.1.007

This preliminary investigation studied the effect of circular turbulator vortex generator on heat transfer rate and pressure drop in a circular channel countercurrent double pipe heat exchanger with water working fluid. Increasing the number of circular turbulator yielded increasing heat transfer rate and pressure drop. The problem generated when increased pressure drop occurred in relation to more energy consumption of the water pumping system. Therefore, optimization in circular turbulator number is necessary to minimize the pressure drop about distance length between circular turbulator, tube diameter and thickness, type of material and crystal lattice, as well as the geometrical shape of fluid passage (circular or square). This study applied PVC outer tube and copper alloy inner tube, as well as fiberglass circular turbulator. The optimum results showed that seven parts of circular turbulator increasing heat transfer rate by 30% and pressure drop by 80% compared to that passage in the absence of circular turbulator at cool water debit of 7 L/min.

CHLORIDE SENSOR FABRICATION BASED ON SPE Ag/AgCl THROUGH CYCLIC VOLTAMMETRIC TECHNIQUE: SCAN RATE EFFECT Mas'ud Asadullah; Sagir Alva; Ali Rinaldi; Rita Sundari
SINERGI Vol 25, No 3 (2021)
Publisher : Universitas Mercu Buana

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22441/sinergi.2021.3.012

The Cyclic Voltammetric (CV) technique is one of the Ag/AgCl fabrication processes. In electrochemical processes using this CV technique, the microstructure of the surface of a substrate or electrode can affect the scan rate. Thus, this study aims to identify the scan rate effect of the Cl-ion sensor fabrication process using the CV technique on the performance of the Cl-ion sensor. First, the CV process was carried out in one cycle to grow the AgCl layer on the Ag surface. Then, this process was carried out at varied scan rates of 20, 40, 60, 80, and 100 mV/s. After completing the Ag/AgCl fabrication process, it was followed by the characterization process, selectivity coefficient test, lifetime test, and validation test to compare the test results of the Cl SPE Ag/AgCl ion sensor with Ag/AgCl commercial. The results showed that the optimum Cl-ion sensor response was obtained at the scan rate of 60 mV/s. Then, based on the validation test, the Cl-ion in the two samples did not show significant differences. Therefore, it indicates that the SPE Ag/AgCl ion sensor has the same performance as the Ag/AgCl commercial.

Induced roll magnetic separator applied for high grade ilmenite separation from mining tailing Wiwik Dahani; Rita Sundari; Subandrio Somali; Irfan Marwanza; Andriyani Andriyani; Djoko Hartanto; Khuzaimah Arifin; Ratna Ediati
SINERGI Vol 27, No 2 (2023)
Publisher : Universitas Mercu Buana

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22441/sinergi.2023.2.015

This article aimed to separate ilmenite (FeTiO3) mineral from tin tailing applying a single splitter IRMS (Induced Roll Magnetic Separator). Ilmenite mineral is the substantial main source for TiO2. This work used air table middling for feeding. The mineral components of middling feeding from air table using grain counting analysis were found as follows: cassiterite (48.61%), ilmenite (21.36%), monazite (18.56%), pyrite (4.60%), zircon (5.85%), quartz (0.71%), anatase (0.27%), and tourmaline (0.02%), It was found that electrical current and opening of single splitter affected the degree of separation addressing to ilmenite recovery and ilmenite grade. The finding showed that current of 15 Ampere and single splitter with opening 4.25 cm yielded ilmenite recovery more than 74%. The high grade ilmenite (90.46 %) and recovery of 29.38% was obtained using 5 Ampere with single splitter opening of 1.0 cm. Up to date, the study on ilmenite separation from tailing only focused on the effect of current, however, the effect of single splitter magnetic separator to enhance ilmenite recovery from other paramagnetic minerals such as monazite, siderite, xenotime and tourmaline has not yet been reported.

Multiple linear regression analysis and lagrange polynomial on pyrolysis process of coconut shell waste producing solid biochar Rosdanelli Hasibuan; Rita Sundari; Hans Martua Pardede; Vikram Alexander; Juliza Hidayati
AGROINTEK Vol 17, No 3 (2023)
Publisher : Agroindustrial Technology, University of Trunojoyo Madura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21107/agrointek.v17i3.17092

Coconut shell waste has generated environmental problems in Indonesia. Due to fossil fuel shortage, coconut shell waste has been advantaged as an energy source to replace the fossil energy. A pyrolysis technique has been used to crack coconut shell waste into charcoal or solid biochar. An MLR (Multiple Linear Regression) analysis and Lagrange polynomial interpolation has been applied to the pyrolysis process related to pyrolysis temperature and time-affected charcoal characteristics. This type of analysis often used for process optimization. The charcoal characteristics are investigated in terms of their yield, water content, ash content, volatile matter, and calorific value. The experimental result shows that the highest calorific value (≈ 7750 cal/g) was obtained at 450oC and 3h with charcoal characteristics: 2.75% water content, 2.70% ash content, and 9.50% volatile matter that meets the SNI requirements. The MLR analysis has justified that the effect of pyrolysis temperature is more dominant than pyrolysis time on almost all charcoal characteristics. The Lagrange polynomial interpolation shows the highest calorific value (≈ 7784 cal/g) obtained at 500oC and 3h. The finding applying MLR analysis and Lagrange polynomial interpolation based on experimental results is a new breakthrough in this investigation.

Pemanfaatan Limbah Kantin Sekolah Menjadi Pupuk Organik Sebagai Teknik Pengolahan Sampah di Sekolah Nur Indah; Darwin Sebayang; Rita Sundari; Subekti Subekti; R. Ariosuko; Fajar Anggara; Gian Villany Golwa
JPPM (Jurnal Pengabdian dan Pemberdayaan Masyarakat) VOL. 8 NOMOR 2 JULI 2024 JPPM (Jurnal Pengabdian dan Pemberdayaan Masyarakat)
Publisher : Universitas Muhammadiyah Purwokerto

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30595/jppm.v8i2.21272

Tujuan kegiatan ini adalah untuk keterampilan dan kemampuan dalam pembuatan pupuk organik cair pada siswa SMKN 35, dalam rangka mengurangi pencemaran lingkungan akibat limbah kantin disekolah. Pelatihan ini terdiri dari dua bagian, yaitu indoor dan outdoor. Dalam indoor diberikan materi mengenai proses dan prosedur pembuatan sampah menjadi pupuk cair. Sedangkan outdoor melakukan praktek cara pembuatan tabung composer dan cara pembuatan pupuk organik cair dari limbah yang berasal dari kantin dan buah-buahan yang busuk. Sehingga siswa-siswi SMKN 35 dapat memperoleh pengetahuan dan keterampilan cara membuat pupuk cair organik dari limbah kantin dan buah-buahan busuk. Hasil kegiatan juga berupa antusiasme dan semangat siswa-siswi yang mengikuti pelatihan sebanyak 30 orang menunjukkan ketertarikan dalam praktek pembuatan pupuk cair organik dari limbah.

PYROMETALLURGICAL PROCESS FOR ZINC ANALYSIS IN SPHALERITE APPLYING XRD AND XRF Dahani, Wiwik; Kurniawati, Riskaviana; Sundari, Rita; Marwanza, Irfan; Rachman, Faisal
Jurnal Rekayasa Mesin Vol. 15 No. 1 (2024)
Publisher : Jurusan Teknik Mesin, Fakultas Teknik, Universitas Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/jrm.v15i1.1525

This paper has analyzed dominant zinc element in sphalerite naturally found together with galena in mineral ore. Since pyrometallurgical route related to roasting process is very common to mineral dressing, therefore, this investigation has studied the effect of varied roasting time (30 min, 60 min, and 90 min) and temperature (500oC, 600oC, and 700oC) on zinc mineral examination using XRD (X-Ray Diffraction) and zinc element using XRF (X-Ray Fluorescence) analyses. Previous studies usually applied cheaper AAS (Atomic Absorption Spectrometer) for zinc analysis in aqueous solution, however, sphalerite is a solid matrix and therefore, this study has applied XRF to analyze zinc. Pyrometallurgical process of zinc mineral in sphalerite is related to mineral transformation in the form of ZnSO4, ZnS, and ZnO that cannot be detected by XRF. Therefore, this study has used XRD that can observe mineral transformation. The XRD pattern shows four intense peaks at 2θ (28o, 47o, 56o, and 76o) justified sphalerite (ZnS) sample with little amount of pyrite (FeS2) and galena (PbS) as impurities. The XRF analysis shows from 30 min to 90 min, the Zn content has increased remarkably at 700oC and Zn content looked stagnant at 500oC, while Zn content increased dramatically from 60 min to 90 min at 600oC. During roasting process at high temperature, ZnS mineral converted to ZnO and expelled SO2 gas due to oxidation reaction causing weight reduction. The study is valuable for mineral processing in searching for optimization.

PYROMETALLURGICAL PROCESS FOR ZINC ANALYSIS IN SPHALERITE APPLYING XRD AND XRF Dahani, Wiwik; Kurniawati, Riskaviana; Sundari, Rita; Marwanza, Irfan; Rachman, Faisal
Jurnal Rekayasa Mesin Vol. 15 No. 1 (2024)
Publisher : Jurusan Teknik Mesin, Fakultas Teknik, Universitas Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/jrm.v15i1.1525

This paper has analyzed dominant zinc element in sphalerite naturally found together with galena in mineral ore. Since pyrometallurgical route related to roasting process is very common to mineral dressing, therefore, this investigation has studied the effect of varied roasting time (30 min, 60 min, and 90 min) and temperature (500oC, 600oC, and 700oC) on zinc mineral examination using XRD (X-Ray Diffraction) and zinc element using XRF (X-Ray Fluorescence) analyses. Previous studies usually applied cheaper AAS (Atomic Absorption Spectrometer) for zinc analysis in aqueous solution, however, sphalerite is a solid matrix and therefore, this study has applied XRF to analyze zinc. Pyrometallurgical process of zinc mineral in sphalerite is related to mineral transformation in the form of ZnSO4, ZnS, and ZnO that cannot be detected by XRF. Therefore, this study has used XRD that can observe mineral transformation. The XRD pattern shows four intense peaks at 2θ (28o, 47o, 56o, and 76o) justified sphalerite (ZnS) sample with little amount of pyrite (FeS2) and galena (PbS) as impurities. The XRF analysis shows from 30 min to 90 min, the Zn content has increased remarkably at 700oC and Zn content looked stagnant at 500oC, while Zn content increased dramatically from 60 min to 90 min at 600oC. During roasting process at high temperature, ZnS mineral converted to ZnO and expelled SO2 gas due to oxidation reaction causing weight reduction. The study is valuable for mineral processing in searching for optimization.

EFFECT OF ACID CONCENTRATION AND ROTATION RATE ON PB LEACHING FROM GALENA ORES Sundari, Rita; Dahani, Wiwik; Marwanza , Irfan; Subandrio, Subandrio; Herdiyanto, Rizky B.
Jurnal Rekayasa Mesin Vol. 16 No. 1 (2025)
Publisher : Jurusan Teknik Mesin, Fakultas Teknik, Universitas Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/jrm.v16i1.1583

This research is related to lead (Pb) leaching from galena ores using acid leaching method. The galena ores have been treated through pyrometallurgy method by roasting at 600oC 1h to yield galena concentrate. The Pb concentration has been determined by AAS (Atomic Absorption Spectrophotometry) using acid leaching method. This study has observed the effect of leaching acid concentration (acetic and sulfuric acids) and rotation rate on Pb leaching at 50oC 45 min. This study shows that varied acetic acid concentrations gave more effect on Pb extraction. Optimum condition achieved for 2.0 M acetic acid for all given rotation speeds (200 rpm, 300 rpm, and 400 rpm). For sulfuric acid leaching, optimum condition achieved at 1.0 M H2SO4 at 400 rpm. From the results, it is apparent that varied rotation speed (200 rpm, 300 rpm, 400 rpm) gave lesser effect on Pb leaching rather than varied acid concentration effect (0.5 M, 0.75 M, 1.0 M, 2.0 M, and 3.0 M). In addition, the XRF (X-Ray Fluorescence) analysis on galena ores shows the existence of lanthanum, ytterbium, and europium (rare earth elements) in significant amount since rare earth elements displays important role in modern industry for nuclear battery, dental apparatus, microchips, hybrid vehicles, catalyst for cracking, audio device, and ceramic agent. Statistical and numerical analysis are briefly included in this study to determine the dominant factor and process optimization.

EFFECT OF SiO2 AND ZnO NANOPARTICLES TO INCREASE REFRIGERATION MACHINE PERFORMANCE Dandi Irwansyah; Rita Sundari; Rini Anggraini; Khuzaimah Arifin
International Journal of Innovation in Mechanical Engineering and Advanced Materials Vol. 5 No. 2 (2023)
Publisher : Universitas Mercu Buana

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22441/ijimeam.v5i2.21859

In this investigation, the impact of silicon dioxide (SiO2) and zinc oxide (ZnO) nanoparticles on the performance of a refrigeration machine system was systematically examined. The focus was on evaluating the coefficient of performance (COP) concerning the utilization of a polyolester (POE) lubricant, R600a refrigerant, and distinct nanoparticles (SiO2 and ZnO) within the refrigeration system. The nanoparticles were individually introduced into the R600a refrigerant in masses of 0.5 g, 1.0 g, and 1.5 g. The experimental outcomes demonstrated a noteworthy enhancement in COP with the addition of nanoparticles. Specifically, the introduction of 1.5 g of SiO2 resulted in a substantial increase of 25.88% in COP, marking it as the most influential dosage. Similarly, the addition of 1.0 g of ZnO led to a significant COP increase of 13.6%, representing the optimal quantity for ZnO. Furthermore, the inclusion of 1.5 g of SiO2 brought about a remarkable reduction in energy consumption, with a decrease of 25.58%, while 1.5 g of ZnO resulted in a notable 16.28% decrease in energy consumption. The experimental configuration involved the use of 20 g of refrigerant and 500 ml of POE lubricant. Comparative analysis demonstrated that the refrigeration system incorporating nanoparticles outperformed the conventional R600a refrigeration system devoid of nanoparticles. This study contributes valuable insights into the potential enhancements in refrigeration system efficiency through the strategic incorporation of SiO2 and ZnO nanoparticles, offering a promising avenue for optimizing the performance of refrigeration technology.

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