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All Journal Reaktor Jurnal Teknik Kimia Jurnal Fisika Unand Journal of Natural Sciences and Mathematics Research CHEESA: Chemical Engineering Research Articles International Journal of Economics, Business and Accounting Research (IJEBAR) ASEAN Journal of Community Engagement G-Tech : Jurnal Teknologi Terapan Nusantara Science and Technology Proceedings International Journal of Eco-Innovation in Science and Engineering (IJEISE) Jurnal Pengbdian Teknik Mesin Serambi Engineering JURNAL REKAYASA KIMIA & LINGKUNGAN
SRIE MULJANI
Universitas Pembangunan Nasional Veteran Jawa Timur
Agriculture, Biological Sciences & Forestry Humanities Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Civil Engineering, Building, Construction & Architecture Computer Science & IT Control & Systems Engineering Decision Sciences, Operations Research & Management Earth & Planetary Sciences Economics, Econometrics & Finance Education Electrical & Electronics Engineering Energy Engineering Environmental Science Industrial & Manufacturing Engineering Law, Crime, Criminology & Criminal Justice Materials Science & Nanotechnology Mechanical Engineering Medicine & Pharmacology Physics Public Health Social Sciences Other

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Precipitated calcium oxide nanosize from limestone and blood clam shells Caecilia - Pujiastuti; Srie Muljani; Ketut Sumada
Journal of Natural Sciences and Mathematics Research Vol 9, No 1 (2023): June
Publisher : Faculty of Science and Technology, Universitas Islam Negeri Walisongo Semarang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21580/jnsmr.2023.9.1.13209

Abstract

Calcium oxide (CaO) is a product that is needed by various types of industries such as the pharmaceutical, chemical, agricultural and health industries. CaO is generally produced by the calcination method of CaCO3 materials such as calcium carbonate rocks or from various types of shells. The calcination method requires a large amount of energy because the operating temperature is above 1000 C and the resulting calcium oxide product is still micrometer size. This study developed nanosize precipitated CaO from two calcium sources, namely blood clam shells and limestone. For clam shells using hydrochloric acid as a solvent and sodium hydroxide as a precipitating agent, while for limestone using phosphoric acid as a solvent and potassium hydroxide as a precipitating agent. The effect of acidity (pH) and calcination temperature on the characteristics of the precipitated CaO was observed. The blood calm shell produces precipitated CaO 85-92 % with a particle size of 200-250 Nm and the limestone produces precipitated CaO 42-66% with a particle size of 250-300 Nm 
THE IMPACT OF ENVIRONMENT AND BEHAVIOR OF DAILY CATTLE BREEDERS ON CONSIDERATION OF INVESTORS IN INVESTING IN GALENGDOWO VILLAGE, JOMBANG J.E. Sutanto; Farida Pulansari; Srie Muljani; Sukirmayadi Sukirmayadi
International Journal of Economics, Business and Accounting Research (IJEBAR) Vol 6, No 3 (2022): IJEBAR, Vol. 6 Issue 3, September 2022
Publisher : LPPM ITB AAS INDONESIA (d.h STIE AAS Surakarta)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29040/ijebar.v6i3.5837

Abstract

The purpose of the study was to determine and analyze whether cow dung, environmental permits, and farmer behavior affect investors in investing in Galengdowo village. Design/Methodology/approach, the population in this study were all dairy farmers who had more than 5 dairy cows, while the number of samples used was 73 respondents. Data collection in this study was carried out by distributing research instruments using a Likert scale instrument and after the data was collected, data processing was carried out using the SPSS version 25 program. towards investors; (2) the environmental permit variable partially has a significant effect on investors, and (3) the breeder's behavior variable partially has a significant effect on investors. Based on the multiple linear regression equation, it can be explained as follows: First, the cow dung waste variable (X1) has the highest influence. Second, the farmer behavior variable (X3) has the lowest effect compared to the cow dung waste variable (X1) and the environmental permit variable (X2).
A Teknologi Pembuatan Pembersih Lantai Sereh untuk Menambah Kesejahteraan Kelompok Tani Kosagrha Lestari Surabaya Suprihatin; Susilowati, Titi; Muljani, Srie; Edahwati, Luluk; Sutiyono, Sutiyono
abdimesin Vol. 3 No. 2 (2023): Abdi-mesin
Publisher : UPN "Veteran" Jawa Timur

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33005/abdimesin.v3i2.53

Abstract

Pemanfaatan tanaman sereh wangi untuk dijadikan sebagai pembersih lantai organik sereh ramah lingkungan. Pembersih lantai sangat diperlukan dalam rumah tangga yang berfungsi menghilangkan bau tak sedap serta untuk membunuh bakteri yang menempel dilantai. Minyak Atsiri sereh wangi mempunyai bau yang menyegarkan dan juga sebagai antimikroba untuk membunuh bakteri. Pengabdian Masyarakat ini mempunyai tujuan untuk memberikan pengetahuan tentang pembuatan pembersih lantai organik sereh yang hasilnya bisa diterapkan untuk rumah tangga sendiri juga bisa berpeluang untuk berwirausaha sehingga akan menambah pendapatan keluarga
Sintesis dan Karakterisasi Kalsium Fosfat dari Cangkang Bekicot dengan Metode Presipitasi Pangestu, Titan Obby; Damayanti, Savira Farizqy; Santi, Sintha Soraya; Muljani, Srie
CHEESA: Chemical Engineering Research Articles Vol. 4 No. 2 (2021)
Publisher : Universitas PGRI Madiun

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25273/cheesa.v4i2.8931.82-90

Abstract

Cangkang bekicot memiliki potensi sebagai bahan baku sintesis kalsium fosfat karena kandungan kalsium yang sangat tinggi, yaitu sekitar 99 %. Kalsium fosfat dapat diaplikasikan sebagai biomaterial karena sifatnya yang sama dengan jaringan penyusun tulang. Pada saat ini kebutuhan akan biomaterial sangat tinggi dan telah memberi dampak yang cukup besar terutama dalam bidang kedokteran ortopedi. Penelitian ini bertujuan untuk mengkaji karakteristik kalsium fosfat dengan menggunakan bahan baku cangkang bekicot. Penelitian ini dilakukan dengan metode presipitasi dengan variasi pH dan suhu sintering. Cangkang bekicot di kalsinasi pada suhu 900 oC lalu di campurkan dengan larutan asam fosfat sesuai dengan rasio molar Ca/P 1,67. Pengendapan kalsium fosfat dilakukan saat proses presipitasi dengan penambahan NaOH untuk mengatur pH pada rentang 11 dan 12. Selanjutnya dilakukan proses sintering pada suhu 600, 700, 800, dan 900 oC. Karakterisasi kalsium fosfat yang dihasilkan menggunakan XRF, XRD, dan SEM. Hasil penelitian menunjukkan perolehan hidroksiapatit (Hap) mencapai 100% pada pH 12, dan suhu 600 oC dengan struktur kristal amorf.
Sintesis dan Karakterisasi Al-MCM-41 dari Kaolin: Pengaruh Konsentrasi HCl terhadap Struktur dan Kapasitas Adsorpsi Iodin Abdullah, Affan Zein; Putri, Alisyah Ananda; Muljani, Srie; Nugraha, Reva Edra
Jurnal Serambi Engineering Vol. 10 No. 2 (2025): April 2025
Publisher : Faculty of Engineering, Universitas Serambi Mekkah

Show Abstract | Download Original | Original Source | Check in Google Scholar

Abstract

Al-MCM-41 can be synthesized using kaolin from Bangka Belitung without requiring additional sources of silica or aluminum. The process begins with calcination of kaolin to produce metakaolin, followed by HCl treatment for dealumination, which helps remove impurities and excess alumina. This step is crucial to achieve the optimal SiO₂/Al₂O₃ mole ratio, making the material effective as an adsorbent or catalyst. The hydrothermal process enhances silica polymerization and pore formation due to the strong electrostatic interactions between CTAB and silicate anions, increasing the pore size. The mesoporous structure and SiO₂/Al₂O₃ ratio of Al-MCM-41 are influenced by the CTAB concentration and the extent of dealumination through HCl treatment. In this synthesis, CTAB acts as a structure-directing agent, forming the hexagonal mesoporous framework, while HCl concentration regulates the removal of alumina from kaolin. To optimize the process, HCl concentrations of 2M, 4M, and 6M were tested to evaluate the extent of alumina and impurity removal. The 6M HCl treatment produced a SiO₂/Al₂O₃ ratio of 25.359, which aligns with the commercial Al-MCM-41 standard from ACS Material. Additionally, the iodine adsorption test demonstrated significantly higher adsorption capacity (653.14 mg/g) for Al-MCM-41 compared to kaolin (76.2 mg/g).
Peningkatan Kualitas Bio-Oil Hasil Pirolisis Cangkang Kelapa Sawit Berstandar Pelumas Organik Wiraya, Wira Arta; Rifaldi, Kornelius; Muljani, Srie; Siswati, Nana Dyah; Karaman, Novel
Jurnal Fisika Unand Vol 14 No 3 (2025)
Publisher : Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jfu.14.3.249-254.2025

Abstract

Palm kernel shells are biomass waste that has the potential to be processed into bio-oil through pyrolysis, but its quality needs to be improved to meet organic lubricant standards. This study aims to improve the quality of bio-oil through a transesterification process with activated carbon-NaOH catalyst and the addition of guar gum as a thickening agent. Pyrolysis was carried out at a temperature of 300°C for 60 minutes, and transesterification at a temperature of 60°C for 2 hours with a methanol:bio-oil ratio of 6:1. The results showed that increasing the amount of catalyst up to 10% increased the yield of methyl ester, while the addition of guar gum increased the kinematic viscosity to 7.9 cst, approaching commercial lubricant standards such as top 1 Evo 5W-30 and pertamina fastron gold 5W-30. However, the flash point is still lower than industrial lubricants. Thus, the quality of bio-oil from palm kernel shell pyrolysis can be improved to approach organic lubricant standards, making it a more environmentally friendly alternative lubricant and has the potential for industrial applications.
Estimation of Critical Properties of Eucalyptol, Alpha-Terpineol, Limonene, and Caryophyllene in Eucalyptus Oil (Melaleuca leucadendra) Using the Group Contribution Method Prasetyo, Muhammad Dewa; Muljani, Srie; Sari, Amilia Putri Puspita
Jurnal Rekayasa Kimia & Lingkungan Vol 20, No 1 (2025): Jurnal Rekayasa Kimia & Lingkungan (June, 2025)
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v20i1.42409

Abstract

Critical property estimation of compounds in eucalyptus oil has been conducted using the Group Contribution method to improve the accuracy of calculations of critical temperature (Tc), critical volume (Vc), critical pressure (Pc), and normal boiling point (Tb). This study updates the previous research by adding a comparative analysis of estimation errors between methods. Eucalyptus oil was extracted using microwave hydrodistillation followed by vacuum distillation to determine experimental data, then estimated using the Joback, Constantinou-Gani (CG), Wilson-Japerson (WJ), and Marrero-Pardillo (MP) methods. The results show that the Wilson-Japerson method provides the most accurate Pc estimation with %AAE of 12.7819%, the Marrero-Pardillo method is best for Vc with %AAE of 5.3393%, the Marrero-Pardillo method provides the most accurate Tc estimation with %AAE of 2.7143%. The Joback method is most suitable for Tb with a %AAE of 20.0828%. The application of the results of this study in the essential oil industry is crucial in optimizing the extraction and distillation process, increasing the efficiency of separation units, developing refining technology, and formulating essential oil-based products. The method with the best accuracy can be used in the design of distillation equipment and thermodynamic reactors, thereby improving production efficiency and product quality in the pharmaceutical, cosmetic, and natural chemical industries.
Optimization of Biodiesel Synthesis from Avocado Seeds Using Response Surface Methodology (RSM) Nicander, Priscillia stevanies; Muljani, Srie; Darma, Apriandi Putra
Jurnal Rekayasa Kimia & Lingkungan Vol 20, No 1 (2025): Jurnal Rekayasa Kimia & Lingkungan (June, 2025)
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v20i1.42035

Abstract

The synthesis of biodiesel from avocado seed oil has been successfully conducted. This study aimed to determine the optimized parameters for the transesterification reaction using Response Surface Methodology (RSM). The transesterification reaction was carried out with variations in the methanol mole ratio of 1:4, 1:6, and 1:8 at temperatures of 40 C, 50 C, and 60 C, utilizing 1 wt% KOH relative to the oil. The avocado seed oil, obtained from the extraction process, has a free fatty acid content of 1.95%. The RSM results indicated that the optimized parameters for biodiesel production were at a temperature of 60 C with a methanol mole ratio of 1:6. The final yield achieved was 82%, calculated based on the initial weight of the oil. The biodiesel produced had a cetane number of 75, a density of 877.4 kg/m, and a viscosity of 4.768 cSt. These values meet the SNI standards, which require a minimum cetane number of 51, a density of 850890 kg/m, and a viscosity of 2.36 cSt.
Synthesis and Characterization of Calcium Phosphate Using Two Stages of Process Anggoro, Achmad Rahditya Viman; Arianti, Rahma Dea Rerindra; Pujiastuti, Caecilia; Sumada, Ketut; Muljani, Srie
Jurnal Rekayasa Kimia & Lingkungan Vol 19, No 1 (2024): Jurnal Rekayasa Kimia & Lingkungan (June 2024 )
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v19i1.37829

Abstract

Calcium phosphate, a naturally occurring biomaterial found in human and animal bones and teeth, possesses desirable properties such as strength, biocompatibility, and the ability to stimulate tissue growth. This study investigates the synthesis of calcium phosphate through a precipitation method without calcination. The process involves dissolving raw materials in phosphoric acid, followed by precipitation using KOH as the precipitating agent. The resulting precipitate was then calcined for 3 hours. The calcium phosphate product was characterized using XRF, XRD, and SEM-EDX techniques. The results indicate a Ca-P molar ratio ranging from 1.855 to 2.302, with the predominant phase identified as -calcium pyrophosphate. SEM analysis reveals a plate-like morphology with agglomerated particles ranging in size from 888 nm to 7.79 m. The synthesized calcium phosphate holds potential for various biomedical applications due to its unique properties and composition.
Synthesis of Aragonite Polymorphs from Five Types of Sea Shells by Carbonation Method Hadi, Prasetyo; Hidayah, Wahyu; Sani, Sani; Muljani, Srie
G-Tech: Jurnal Teknologi Terapan Vol 9 No 3 (2025): G-Tech, Vol. 9 No. 3 July 2025
Publisher : Universitas Islam Raden Rahmat, Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.70609/gtech.v9i3.6998

Abstract

Shell waste accumulates along the coastal areas of Surabaya and Sidoarjo, with various types of shells including blood shells, green shells, feather shells, kampak shells, and batik shells. Currently, the waste from these shells is not being utilized optimally. Marine shell waste contains more than 95% calcium carbonate (CaCO3), making it suitable for the production of aragonite crystals, which can serve as raw materials for applications such as bone regeneration, paper manufacturing, and as fillers in rubber and plastics. The objective of this research is to synthesize aragonite from five types of marine shells and to investigate the effect of carbonation temperature on the percentage of aragonite formation. The method employed for synthesizing aragonite crystals is carbonation. Initially, the CaCO3 derived from marine shells is calcined at 900°C to produce calcium oxide (CaO). This calcium oxide is then dissolved in hydrochloric acid (HCl) to form calcium chloride (CaCl2). Subsequently, sodium hydroxide (NaOH) is added to CaCl2, and carbon dioxide (CO2) gas is bubbled through the solution to precipitate CaCO3 along with by-products of NaCl and water. The variables examined include comparisons among five types of shells (blood shells, green shells, feather shells, kampak shells, and batik shells) at calcination temperatures of 30°C, 60°C, and 90°C. The best results were obtained from the synthesis using green shells, yielding an aragonite crystal polymorph percentage of 76.4% at a carbonation temperature of 90°C. Conversely, the smallest yield of aragonite crystal polymorph was observed with batik shells at 26.0%.
Co-Authors A. R Yelvia Sunarti Abdullah, Affan Zein Amalia, Ayu Rizka Anggoro, Achmad Rahditya Viman Arianti, Rahma Dea Rerindra Astuti, Dwi Hery Bambang Wahyudi Bambang Wahyudi Wahyudi Caecilia - Pujiastuti Damayanti, Savira Farizqy Darma, Apriandi Putra Erwan Adi Saputro Farida Pulansari Hidayah, Wahyu ISNI UTAMI J.E. Sutanto JE Sutanto Ketut Sumada Caecillia Pujiastuti Kindriari Nurma Wahyusi Kusuma, Kurnia Arifiani L.Urip Widodo, Yohandrik Novel Karaman Luluk Edahwati Maulana, Mochamad Titus Mega Rosilina Mochamad Titus Maulana Nana Dyah Siswati, Anwar Zain and Mohammad Nicander, Priscillia stevanies Nofitasari, Luluk Nove Kartika Nugraha, Reva Edra Nur Hapsari Pangestu, Titan Obby Pradana, Alfian Rizki Prasetyo Hadi Prasetyo, Muhammad Dewa Pujiastuti, Caecilia Pujiastuti, Caecilia - Putri, Alisyah Ananda Rifaldi, Kornelius Rosilina, Mega S Suprihatin Sani Sani SANI SANI Santi, Sintha Soraya Sari, Amilia Putri Puspita Sintha Soraya Santi Sukirmayadi Sukirmayadi Sunarti, A.R Yelvia Suprihatin sutiyono sutiyono Titi Susilowati Wiraya, Wira Arta