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All Journal PHARMACON Biology, Medicine, & Natural Product Chemistry SELAPARANG: Jurnal Pengabdian Masyarakat Berkemajuan Pharmasipha Majalah Farmasetika Jurnal Kefarmasian AKFARINDO Pharma Xplore : Jurnal Sains dan Ilmu Farmasi JPK: Jurnal Proteksi Kesehatan Jurnal Ilmiah Ibnu Sina (JIIS): Ilmu Farmasi dan Kesehatan Jurnal Farmasi Etam Jurnal Pengabdian Masyarakat Tjut Nyak Dhien Media Farmasi Jurnal Sains dan Kesehatan Jurnal Ilmiah Manuntung: Sains Farmasi dan Kesehatan
Nurillahi Febria Leswana
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Religion Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemistry Computer Science & IT Control & Systems Engineering Economics, Econometrics & Finance Education Engineering Environmental Science Health Professions Immunology & microbiology Languange, Linguistic, Communication & Media Law, Crime, Criminology & Criminal Justice Medicine & Pharmacology Neuroscience Nursing Public Health Social Sciences Other

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Synthesis Polyelectrolyte Complex Membrane Polystyrene Sufonate-Chitosan from Styrofoam Waste as The Adsorbent for Cu(II) and Ni(II) Metal Nurillahi Febria Leswana; Dwi Siswanta; Adhitasari Suratman
Jurnal Farmasi Etam (JFE) Vol 1 No 1 (2021): Juni
Publisher : Unit Penelitian dan Pengabdian Kepada Masyarakat (UPPM) STIKES Dirgahayu Samarinda

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (563.262 KB) | DOI: 10.52841/jfe.v1i1.173

Abstract

ABSTRAK Telah dilakukan sintesis membran polistirena sulfonat (PSS)-kitosan dari modifikasi limbah styrofoam, kemudian dipelajari kemampuannya dalam mengadsorpsi logam Ni(II) dan Cu(II). Telah ditentukan pula komposisi optimum PSS-kitosan, uji stabilitas asam basa, dan kemampuan swellingnya. Parameter kajian adsorpsi yang dipelajari dalam penelitian ini meliputi pH optimum, kinetika adsorpsi, isoterm adsorpsi, pengaruh kation lain secara selektifitas, dan penentuan mekanisme adsorpsi. Analisis logam Cu(II) dan Ni(II) sebelum dan sesudah proses adsorpsi dilakukan dengan menggunakan metode Spektrofotometri Serapan Atom (SSA) Hasil penelitian menunjukkan bahwa polistirena sulfonat (PSS) berhasil diperoleh dari reaksi sulfonasi limbah styrofoam yang ditunjukan dengan spektra FTIR. Komposisi optimum membran PSS:kitosan untuk mengadsorpsi logam Cu(II) dan Ni(II) adalah perbandingan 60:40 dengan kestabilan, sifat fisik, dan kemampuan adsorpsi yang paling baik. Keadaan pH optimum adsorpsi logam Cu(II) dan Ni(II) berada pada pH 5, waktu optimum berturut-turut 45 menit dan 60 menit, serta konsentrasi optimum berturut-turut 60 ppm dan 40 ppm. Model kinetika dan isoterm adsorpsi logam Cu(II) dan Ni(II) pada membran PSS-kitosan adalah orde kedua semu (McKay dan Ho) dan model isoterm Freundlich. Tetapan laju reaksi logam Cu(II) dan Ni(II) pada pH 5 berturut-turut 0,480 mmol/g-1menit-1 dan 0,423 mmol/g-1menit-1. Adanya logam Ni(II) dalam adsorpsi Cu(II) tidak memberikan pengaruh yang signifikan sampai pada perbandingan Ni(II)/Cu(II)= 2:1, namun sebaliknya dengan kehadiran logam Cu(II) pada adsorpsi logam Ni(II) sudah memberikan pengaruh pada perbandingan Ni(II)/Cu(II)=1:1. Afinitas membran PSS-kitosan terhadap logam adalah Cu(II) > Ni(II). Pada studi desorpsi diketahui jenis interaksi antara adsorbat dan situs aktif adsorben merupakan mekanisme pembentukan kompleks, pemerangkapan dan pembentukan ikatan hidrogen. ABSTRACT Synthesis of polystyrene sulphonate (PSS) – chitosan membrane of styrofoam waste modification and its ability to adsorb Ni (II) and Cu (II) metals has been studied. The optimum composition of PSS-chitosan, acidity stability test, and swelling ability have been determined. The parameters of the adsorption study studied in this study include optimum pH, adsorption kinetics, adsorption isotherms, selective cationic effects, and determination of adsorption mechanisms. Analysis of Cu (II) and Ni (II) metals before and after the adsorption process was performed using Atomic Absorption Spectrophotometric (AAS) The results showed that polystyrene sulphonate (PSS) was obtained from the sulfonation of styrofoam waste using the FTIR spectra. The optimum composition of rasio PSS: chitosan membrane for adsorbing Cu (II) and Ni (II) is 60:40 with the best stability, physical properties, and adsorption capability. The optimum pH adsorption of Cu (II) and Ni (II) metals was at pH 5, the optimum time was 45 min and 60 min, and the optimum concentrations were 60 ppm and 40 ppm. The kinetic and adsorption models of Cu (II) and Ni (II) metals on PSS-chitosan membranes are second-order (McKay and Ho) and Freundlich isotherm model. The reaction rates of Cu (II) and Ni (II) reactions at pH 5 were 0.480 mmol / g-1menit-1 and 0.423 mmol / g-1menit-1. The presence of Ni (II) metal in Cu (II) adsorption did not give a significant effect to the ratio of Ni (II) / Cu (II) = 2: 1, but with the presence of Cu (II) metal on metal adsorption Ni (II) have an effect on the ratio of Ni (II) / Cu (II) = 1: 1. The affinity of PSS-chitosan membrane to metal is Cu (II)> Ni (II). Sequential desorption studies showed that the adsorption of Cu (II) and Ni (II) metals on the PSS-chitosan membrane were estimated to follow a complex formation, hydrogen bond formation, and physical entrapment mechanisms.
ANALISIS KADAR RHODAMIN B PADA LIPTINT YANG BEREDAR DI PASAR SEGIRI KOTA SAMARINDA DENGAN METODE SPEKTROFOTOMETRI UV-VISIBLE Hiasinta Meliana Hangin; Susana Linden; Nurillahi Febria Leswana
Pharma Xplore : Jurnal Sains dan Ilmu Farmasi Vol 7 No 2 (2022): Pharma Xplore : Jurnal Sains dan Ilmu Farmasi
Publisher : Fakultas Farmasi Universitas Buana Perjuangan Karawang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.36805/jpx.v7i2.2903

Abstract

Liptint is one type of cosmetic lip color that is often used by women. The use of rhodamine B as a cosmetic coloring agent is prohibited by BPOM because Rhodamine B can be carcinogenic and spur the growth of cancer cells if used continuously. The purpose of this study was to determine the presence or absence of harmful substances Rhodamine B in Liptint circulating in the market Segiri Samarinda. Liptint samples were studied as many as 10 samples. Qualitative test of rhodamine B by thin layer chromatography observed under UV lamp light 254 nm. Based on the qualitative test results, samples that tested positive for Rhodamine B were samples A, B, C, E, G, H, I, and J. sample A, B have Rf value (0,907), sample G, I and J (0,802), sample C (0,789), sample H (0,828) and sample E (0,921) and raw Rf Rhodamin B (0,921) with pink spots when viewed vusual and orange spots stain when placed under UV light 254 nm. Quantitative test results from 10 samples, 9 samples tested positive for rhodamine B, namely samples A , B, C, E, F, G, H, I and J with an average content of 0,02%-0,5% w/w.
Identifikasi Kandungan Hidrokuinon dalam Krim Pemutih yang Beredar di Pasar Segiri Kota Samarinda dengan Metode Spektrofotometri UV-Visible Monika Julan; Nurillahi Febria Leswana; Susana Linden
PHARMACON Vol. 12 No. 2 (2023): PHARMACON
Publisher : UNIVERSITAS SAM RATULANGI

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35799/pha.12.2023.47660

Abstract

Hidrokuinon sering kali digunakan sebagai pemutih dalam krim. Hidrokuinon merupakan senyawa aktif yang mampu mengendalikan produksi pigmen, yakni berfungsi untuk mengurangi atau menghambat pembentukan melanin kulit. Penggunaan bahan hidrokuinon pada kulit sangat berbahaya. Hidrokuinon merupakan senyawa yang berpotensi sebagai karsinogenik. Efek samping yang paling sering timbul yaitu rasa terbakar pada kulit, perasaan gatal, iritasi, pigmentasi. Tujuan penelitian ini untuk mengetahui kandungan hidrokuinon pada pemutih wajah yang dijual di Pasar Segiri Kota Samarinda menggunakan uji kualitatif dan kuantitatif. Penelitian ini adalah penelitian eksperimental dengan pemilihan sampel Purposive sampling. Sampel yang diteliti sebanyak 10 sampel krim pemutih yang beredar di Pasar Segiri Kota Samarinda. Uji kualitatif hidrokuinon dengan reagen FeCl3 terhadap sampel krim pemutih memperoleh hasil sampel B, D, E, G, H, dan J mengandung Hidrokuinon dengan menunjukan perubahan warna menjadi kehitaman. Sedangkan uji kromatografi lapis tipis menggunakan fase gerak n-heksana-aseton (6:4) menunjukan terdapat sampel krim pemutih yang positif mengandung Hidrokuinon yaitu pada sampel B, D, E, F, H, I dan J dengan nilai Rf yang mendekati nilai Rf baku hidrokuinon. Uji kuantitatif juga dilakukan untuk menetapkan kadar Hidrokuinon dalam sampel menggunakan Spektrofotometri UV-Visible diperoleh hasil kadar Hidrokuinon dengan rentang 0,36% b/b – 6,08% b/b.v
Pengukuran aktivitas antioksidan ekstrak etanol buah matoa (Pometia pinnata) dengan metode DPPH (2,2-difenil-1,1-pikrilhidrazil) Sulistiani, Sulistiani; Leswana, Nurillahi Febria; Linden, Susana
Pharmasipha : Pharmaceutical Journal of Islamic Pharmacy Vol. 8 No. 2 (2024): September
Publisher : University Of Darussalam Gontor

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21111/pharmasipha.v8i2.10634

Abstract

Tanaman matoa dimanfaatkan oleh Bangsa Asia (Indonesia dan Malaysia) sebagai salah satu obat tradisional yang diketahui mengandung senyawa kimia berupa flavonoid, tanin, dan saponin. Berdasarkan latar belakang tersebut, rumusan masalah dalam penelitian ini yaitu bagaimana aktivitas antioksidan dari ekstrak etanol buah matoa (Pometia pinnata). Tujuan dari penelitian ini yaitu untuk mengetahui aktivitas antioksidan ekstrak etanol buah matoa (Pometia pinnata) dengan metode DPPH. Penelitian ini dilakukan pada bulan Juni-Juli 2023. Aktivitas antioksidan ekstrak buah matoa dianalisis menggunakan alat spektrofotometri UV-Vis pada panjang gelombang 517 nm. Hasil penelitian yang diperoleh menunjukkan nilai IC50 ekstrak buah matoa sebesar 181,551 ppm sedangkan larutan pembanding vitamin C sebesar 5,807 ppm. Nilai IC50 tersebut dapat ditentukan bahwa ekstrak etanol buah matoa merupakan antioksidan yang bersifat lemah.   Kata Kunci: Buah matoa, DPPH, antioksidan, Pometia pinnata
Antioxidant Activity of Tahongai Leaves (Klenhovia hospital L.) Infusa Using DPPH Method Leswana, Nurillahi Febria; Sianturi, Sister
JURNAL PROTEKSI KESEHATAN Vol 13 No 1 (2024): JPK: Jurnal Proteksi Kesehatan
Publisher : Poltekkes Kemenkes Riau

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.36929/jpk.v13i1.791

Abstract

Tahongai plant (Kleinhovia hospita Linn.) is a plant that grows naturally on the edge of Indonesian rivers, especially in East Kalimantan. Tahongai plants are used as medicine by the Dayak people in Kalimantan, namely that empirically the use of tahongai plants is effective as a medicine that can treat various diseases such as jaundice, hypertension, diabetes, and cholesterol by drinking the boiled water. The active substances contained in tahongai leaves are saponins, flavonoids, and alkaloids are expected to have antioxidant activity. The purpose of this study was to measure the antioxidant activity of tahongai leaf infusa. The extraction method used in this study was infusa while the radical specimen used was DPPH with Vitamin C as the comparison. Phytochemical screening was also carried out ontahongai leaf infusa extract positively containing flavonoids, tannins, saponins and phenols. Based on the results of the DPPH radical scavenging analysis of Tahongai leaf infusion, the IC50 value was 139.51 mg/L with the medium antioxidant activity.
Perbandingan Efektivitas Bioadsorben Serbuk Kulit Singkong Dan Serbuk Kulit Pinang Terhadap Logam Pb (II) Limbah Cair Laboratorium Farmasi Morijan, Risky asrina; Leswana, Nurillahi Febria; Butar-Butar, Maria Elvina Tresia
Media Farmasi Vol 20 No 1 (2024): Media Farmasi Edisi April 2024
Publisher : Jurusan Farmasi Poltekkes kemenkes Makassar

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.32382/mf.v20i1.146

Abstract

Comparison of bio-adsorbent effectiveness of cassava shell powder and betel nut powder against Pb (II) metal of pharmaceutical laboratory liquid waste Pharmaceutical laboratory liquid waste is a source of heavy metal pollutants that can be harmful to living things if not treated properly. One of these heavy metals is lead (Pb), which if discharged directly into the environment can damage the environment and cause health problems. To adsorb these heavy metals, bio-adsorbents can be used, including cassava peel and areca nut peel because they contain cellulose and pectin. In this study, measurements of Pb levels in the waste before and after adsorption were carried out using the UV-visible spectrophotometry method, and the reagent used was alizarin sulfonate from variations in pH. optimum, optimum contact time and optimum mass of the validation method carried out is precision and accuracy. The aim of this study was to determine the comparison of the adsorption effectiveness of cassava peel powder and areca nutshell powder bioadsorbents against Pb metal in pharmaceutical laboratory wastewater. The results obtained were the optimum areca nut skin at pH 5, contact time 45 minutes, and mass 175 mg. Whereas cassava peel at pH 5, contact time 75 minutes, and mass 75 mg. The adsorption effectiveness of areca nut peels is better than that of cassava peels with an adsorption percentage of areca nut peels of 83.38%, while cassava peels are 54.46%. The results of the method validation are declared valid by showing an accuracy value in the range of 80-110% and a precision value of not more than 2%. Limbah cair laboratorium farmasi merupakan sumber pencemar logam berat yang dapat berbahaya bagi makhluk hidup jika tidak diolah dengan baik. Salah satu logam berat tersebut adalah timbal (Pb) yang jika dibuang langsung ke lingkungan dapat merusak lingkungan dan gangguan kesehatan. Untuk mengadsorpsi logam berat tersebut dapat digunakan bioadsorben salah satunya adalah kulit singkong dan kulit pinang karena mengandung selulosa dan pektin, pada penelitian ini dilakukan pengukuran kadar Pb dalam limbah sebelum dan sesudah adsorbsi menggunakan metode spektrofotometri UV-Visible dan reagen yang digunakan alizarin sulfonat dari variasi pH optimum, waktu kontak optimum, dan massa optimum metode validasi yang dilakukan adalah presisi dan akurasi tujuan penelitian ini dilakukan adalah untuk menentukan perbandingan efektivitas adsorbsi bioadsorben serbuk kulit singkong dan serbuk kulit pinang terhadap logam Pb limbah cair laboratorium farmasi. Hasil yang diperoleh adalah kulit buah pinang optimum pada pH 5, waktu kontak 45 menit, dan massa 175 mg. Sedangkan pada kulit singkong pada pH 5, waktu kontak 75 menit, dan massa 75 mg. Efektivitas adsorbsi kulit pinang lebih baik dibandingkan dengan kulit singkong dengan persentase adsorbsi kulit pinang sebesar 83,38%, sementara kulit singkong 54,46%. Hasil validasi metode dinyatakan valid dengan menunjukkan nilai akurasi pada rentang 80-110% dan nilai presisi tidak lebih dari 2%.
Analysis of Sodium Benzoate Content in Sauces Circulating in Segiri Market Samarinda City by UV-Vis Spectrophotometric Method Jenly Adinata; Nurillahi Febria Leswana; Maria Elvina Tresia Butar-Butar
Jurnal Sains dan Kesehatan Vol. 5 No. 5 (2023): J. Sains Kes.
Publisher : Fakultas Farmasi, Universitas Mulawarman, Samarinda, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25026/jsk.v5i5.2008

Abstract

Sodium benzoate is one of the permitted preservatives, if the amount is still below the maximum limit. This study was conducted to identify sodium benzoate levels in sauces circulating in Segiri Market, Samarinda. According to BPOM RI regulation No.36 of 2013, the maximum amount of sodium benzoate used in sauce is 1000 mg/kg. In this study, a qualitative analysis of sodium benzoate was carried out using the FeCl3 reagent, where 10 sauce samples taken from the Segiri market in Samarinda City were positive of containing sodium benzoate, forming a salmon-colored or brownish-red precipitate. Quantitative analysis was performed using a UV-Vis spectrophotometer where sodium benzoate was measured at a maximum wavelength of 226 nm. The verification parameters tested in this study are accuracy test and precision test. Based on the verification parameters, the average % recovery was 94.505% which is still in the range of 80-110%, and %RSD of 0.0642% which is less than 2%. Based on quantitative analysis, sample A content was 2,084.8 mg/kg, sample B was 1,895.1 mg/kg, sample C was 2,547.4 mg/kg, sample D was 1,700.7 mg/kg, sample E was 1,466 mg/kg, sample F was 7. 100.1 mg/kg, sample G by 1,388.1 mg/kg, sample H by 1,587.6 mg/kg, sample I by 1,647.1 mg/kg, sample J by 3,172.9 mg/kg, the sodium benzoate content in the sauce samples above the maximum amount as determined by the  BPOM regulation No. 36 of 2013. Keywords:          Sodium benzoate, Preservative, Sauce, UV-Vis Spectrophotometry
Formulation of Keruing (Dipterocarpus grandiflorus) Oleoresin Aromatherapy Candles Maria Elvina Tresia Butar-Butar; Adhe Septa Ryant Agus; Nurillahi Febria Leswana; Andrian Fernandes
Jurnal Sains dan Kesehatan Vol. 6 No. 4 (2024): J. Sains Kes.
Publisher : Fakultas Farmasi, Universitas Mulawarman, Samarinda, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25026/jsk.v6i4.2331

Abstract

Aromatherapy is an alternative treatment method that utilizes essential oils and volatile components, such as terpenes and aromatic compounds. The active compounds of keruing oleoresin are phthalic acid, namely phthalic acid di(3-methoxybenzyl) ester and phthalic acid, 5-ethyl-1,3-dioxan-5-yl octyl ester causing keruing oleoresin to have a distinctive fragrance. The purpose of this study was to formulate keruing oleoresin in aromatherapy candle preparations. This research method includes base optimization, formulation of keruing oleoresin aromatherapy candles with concentrations of 0%; 2.5%; 5%; 7.5%; and 10%, and evaluation of aromatherapy candles including organoleptic testing, melting point, and burning time. The results of organoleptic testing of aromatherapy candles in shape, aroma, and color showed that F4 with 10% oleoresin concentration had a more dominant aroma and color. Melting point and burning time tests showed F1 with a concentration of 2.5% had a higher melting point of 54.6°C and a longer burning time of 144 minutes. Keywords:          Dipterocarpus grandiflorus, oleoresin, aromatherapy candle
PENETAPAN KADAR FLAVONOID PADA EKSTRAK ETANOL DAUN PANDAN WANGI (Pandanus amaryllifolius Roxb.) DENGAN METODE SPKETROFOTOMETRI UV-VIS Bua, Tin Sanda Liling; Linden, Susana; Leswana, Nurillahi Febria
Jurnal Kefarmasian Akfarindo Vol 10 No 1 (2025)
Publisher : Akademi Farmasi Indonesia Yogyakarta

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.37089/jofar.v10i1.253

Abstract

Daun pandan wangi (Pandanus amaryllifolius Roxb.) merupakan tumbuhan yang sejak dahulu digunakan sebagai obat tradisional. Daun pandan wangi memiliki senyawa metabolit sekunder yaitu alkaloid, flavonoid, tanin, polifenol, dan zat warna. Tujuan dari penelitian ini, yaitu untuk mengetahui kadar flavonoid ekstrak etanol daun pandan wangi dengan metode spektrofotometri UV-Vis. Tahapan penelitian diawali dengan pengumpulan sampel dan determinasi tumbuhan, pembuatan simplisia, pembuatan ekstrak etanol simplisia dengan metode maserasi menggunakan pelarut etanol 70%, skrining fitokimia dan penetapan kadar flavonoid dengan metode spektrofotometri UV-Vis dengan baku pembanding kuersetin. Data dianalisis secara deskriptif. Diperoleh hasil rendemen ekstrak etanol daun pandan wangi 16,29%, penetapan kadar air pada ekstrak kental 12%, dan kadar flavonoid pada panjang gelombang 432 nm 2,3979% ± 0,227.
FORMULASI DAN UJI MUTU FISIK KRIM MASKER WAJAH ANTI-AGING FRAKSI DAUN MIANA (Coleus scutellarioides (L) Benth) Silaban Erllin Tirza Stevany; Muh. Taufiqurrahman; Nurillahi Febria Leswana
Jurnal Ilmiah Ibnu Sina (JIIS): Ilmu Farmasi dan Kesehatan Vol 10 No 1 (2025): Jurnal Ilmiah Ibnu Sina
Publisher : Sekolah Tinggi Ilmu Kesehatan ISFI Banjarmasin

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.36387/jiis.v10i1.2204

Abstract

One of the natural ingredients that can be used as a cosmetic ingredient is miana leaf (Coleus scutelleroides (L) Benth) which contains flavonoid compounds with antioxidant activity that can be used for skin care. These compounds can prevent free radicals that can cause premature aging. The extraction method was used in this study with 96% ethanol solvent and continued with the fractionation process. The determination of antioxidant activity was determined by calculating the IC50 value where the IC50 value of the ethyl acetate fraction of miana leaves obtained was 27.90 ppm. In the study, a formulation of face mask cream preparations with a variety of active ingredients (0,6; 1,2; 2,4). Evaluation of the preparation was carried out on the physical quality of face mask cream using the cycling test method. Based on the results of stability tests on the four preparations, formula 2 with 1.2 g of active ingredients shows the best formula. Antioxidant testing from F1, F2 and F3 obtained IC50 values of 96.33 ppm, 82.73 ppm, 72.71 ppm. The statistical test of antioxidant activity showed a p<0.05 result which indicates that there is a significant difference between the three formulas. Cycling test showed that the facial mask cream preparation was physically and chemically stable. There was no significant change in color, odor, texture, phase separation, or pH change. Viscosity also remained stable, indicating good shelf life during normal storage.
Co-Authors Abdul Rahim Adhitasari Suratman Agnes Elisa Agus, Adhe Septa Ryant Andrian Fernandes Ayugistia, Falen Sindi Bua, Tin Sanda Liling Clara Ritawany Sinaga Dwi Siswanta Hiasinta Meliana Hangin Hutagalung, Remita Ully Iju, Sesilia Karolina Jenly Adinata Linden, Susana Maria Elvina Tresia Butar-Butar Monika Julan Morijan, Risky asrina Nainggolan, Angel Natalia Pangestika, Ruth Gratia Dwi Pijaryani, Indria Ping, Maria Floriana Silaban Erllin Tirza Stevany Sister Sianturi Sulistiani Sulistiani, Sulistiani susana linden Susana Linden Taufiqurrahman, Muh