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All Journal SINTEK JURNAL: Jurnal Ilmiah Teknik Mesin Science and Technology Indonesia Communications in Science and Technology MOTIVECTION : Journal of Mechanical, Electrical and Industrial Engineering Automotive Experiences JURNAL PERMADI: PERANCANGAN, MANUFAKTUR, MATERIAL DAN ENERGI Bulletin of Chemical Reaction Engineering & Catalysis
Ferry Budhi Susetyo
Jurusan Teknik Mesin, Fakultas Teknik, Universitas Muhammadiyah Jakarta
Aerospace Engineering Automotive Engineering Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Civil Engineering, Building, Construction & Architecture Computer Science & IT Control & Systems Engineering Electrical & Electronics Engineering Energy Engineering Environmental Science Industrial & Manufacturing Engineering Materials Science & Nanotechnology Mechanical Engineering Physics

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Journal : Bulletin of Chemical Reaction Engineering

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Preparation, Characterization, and Photocatalytic Activity of Ni-Cd/Al2O3 Composite Catalyst Yusmaniar, Yusmaniar; Premono, Agung; Susetyo, Ferry Budhi; Yudanto, Sigit Dwi
Bulletin of Chemical Reaction Engineering & Catalysis 2023: BCREC Volume 18 Issue 4 Year 2023 (December 2023)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.20045

Abstract

This study was conducted to determine the effect of the radiation source and radiation time on the methylene blue (MB) solution by adding Ni-Cd/Al2O3 to the percent degradation of MB. To investigate similar purposes, the pH of the MB solution varied as well. The preparation, characterization, and photocatalytic activity of Ni-Cd/Al2O3 are three steps in this research. The Ni-Cd was prepared by mixing Ni(NO3)2.6H2O and Cd(NO3)2.4H2O. Various concentrations of Ni-Cd were mixed with Al2O3, then heated, stirred, dried, and calcined to form Ni-Cd/Al2O3 powder. The dried powder catalysts were characterized using Field emission scanning electron microscopy (FESEM), Energy-dispersive X-ray spectroscopy (EDS), Brunauer-emmett-teller (BET), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and Diffused reflectance spectrometer spectra (DR-UV-Vis). Higher degradation was observed at pH 11, when MB was degraded by 68% and 76% using the 5Ni-2Cd/Al2O3 and 6Ni-1Cd/Al2O3 catalysts, respectively. The 6Ni-1Cd/Al2O3 sample has higher absorption, less surface area, and less band gap; therefore, it has higher performance against degraded MB in the solution. In summary, 6Ni-1Cd/Al2O3 is capable of degrading MB and can be utilized in MB dye waste. Copyright © 2023 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). 
Co-Authors Agus Jamaludin Agus Jamaludin Alhamidi, A. Ali Alias, Juliawati Anggrainy, Rani Ansori, Fuad Anugrah, Hanif Setia Bambang Soegijono Basori Basori Basori Budhy Kurniawan Cahaya Rosyidan Daniel Edbert, Daniel Dwi Nanto, Dwi Etty Mutiara Evi Ulina Margaretha Situmorang Fadwah Maghfurah Hasbi, Muhammad Yunan Heri Hardiyanti Imam Basori Indriasti, Zulfah Jan Setiawan Krisyono, Danar Hari Kurniawan, Ova Lubi, Ahmad Maman Kartaman Ajiriyanto Maman Kartaman Ajiriyanto Mansor, Muhd Ridzuan Maulani, Mustamina Muhammad Fauzan Perdana Putra Muhammad Yunan Hasbi Munzir Qadri Muqafillah, Mochammad Fajr Dzakwan Nababan, Frederik Gresia Notonegoro, Hamdan Akbar Prasetya, Dendy Wardhana Premono, Agung Putra, Valentinus Galih Vidia Raksa, Teguh Yoga Ramlan Rohman, Fakhrony Sholahudin Rosika Kriswarini Ruliyanta Ruliyanta Samura, Lisa Setia Budi Setiawidi, Yoganantya Sigit Dwi Yudanto Simbolon, Silviana Sopiyan Sopiyan, Sopiyan Sudibyo Sudibyo Sugeng Priyanto, Sugeng Sukarno, Ragil Sulis Yulianto Syamsuir Syamsuir, Syamsuir Syaripuddin Syaripuddin Syaripuddin Taufiq Al Farizi Tihera, Dinda Tri Yulianto Triandi, Adrian Ova Yudanto, Sigit Dwi Yunasfi Yunita Sari Yusmaniar Yusmaniar