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All Journal ASEAN Journal of Systems Engineering Jurnal Rekayasa Proses Jurnal Bahan Alam Terbarukan Seminar Nasional Teknik Kimia Kejuangan Journal of Degraded and Mining Lands Management Jurnal Sains & Teknologi Lingkungan Konversi Journal of the Civil Engineering Forum Communications in Science and Technology Jurnal Chemurgy Jurnal Rekayasa Proses Media Ilmiah Teknik Lingkungan INSIST (International Series on Interdisciplinary Research) Jurnal Inovasi Teknik Kimia Prosiding Conference on Research and Community Services Prosiding Simposium Nasional Rekayasa Aplikasi Perancangan dan Industri Hexagon
Ahmad Tawfiequrrahman Yuliansyah
Departemen Teknik Kimia, Fakultas Teknik, Universitas Gadjah Mada
Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Civil Engineering, Building, Construction & Architecture Computer Science & IT Control & Systems Engineering Economics, Econometrics & Finance Education Electrical & Electronics Engineering Energy Engineering Environmental Science Industrial & Manufacturing Engineering Materials Science & Nanotechnology Mathematics Mechanical Engineering Social Sciences Other

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Analysis of the Carrying Capacity and the Total Maximum Daily Loads of the Karang Mumus Sub-watershed in Samarinda City Using the WASP Method Achmad Diansyukma; Sri Puji Saraswati; Ahmad Tawfiequrrahman Yuliansyah
Journal of the Civil Engineering Forum Vol. 7 No. 2 (May 2021)
Publisher : Department of Civil and Environmental Engineering, Faculty of Engineering, UGM

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/jcef.62826

Abstract

Watershed is a multi-aspect ecological system, which functions as a source of water resources, in order to meet daily needs. It also motivates both economical and life matters, as well as serve as a sanitary channel for the surrounding community. Watershed also generates pollutants, which are known to potentially cause a decrease in river water quality. The degradation of river habitats that are caused by high pollutants penetration into the water body, decreases the capacity to carry out self-purification of toxic loads. The water pollutant load-carrying capacity is then calculated through various methods, one of which is the use of a computerized numerical modeling simulation called WASP (Water Quality Analysis Simulation Program). This method was developed by the ES-EPA, in order to process TMDLs (Total Maximum Daily Loads) data on river bodies, as well as examine each part of the water quality, based on spatial and temporal inputs. This study was conducted at the Karang Mumus Sub-watershed flowing through the centre of Samarinda City, with aims to determine the pollutants' carrying capacity, existing load, and toxic waste allocation, via the use of the BOD (Biological Oxygen Demand) technique as a parameter of water quality. The calculation was carried out by segmenting the river into five parts, based on the number of districts it passes through, during pollutant loads inventory. The WASP modeling simulation showed that the total pollutant load-carrying capacity of the whole segments was 5,670 kg/day. It also showed the existing loads of about 3,605 kg/day, with the margin having the ability to receive pollutants at 2,065 kg/day. Moreover, the allocation of pollutant loads varies for each segment, with 2, 3, and 4 observed to reduce the pollutant by 390, 220, and 10 kg/day, respectively. However, segments 1 and 5 were still allowed to receive pollutant loads up to 1,740 and 945 kg/day, respectively.
Manganese Recovery from Hydrocracking Spent Catalyst Using Citric Acid and Its Kinetics Himawan Tri Bayu Murti Petrus; Dewi Purnama Sari; Ahmad Tawfiequrrahman Yuliansyah; Fika Rofieq Mufakhir; Widi Astuti; Yusuf Iskandar; Danu Bratakusuma; Shinta Virdhian
INSIST Vol 4, No 2 (2019)
Publisher : Universitas Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar

Abstract

Aiming for recovery and kinetics of manganese from hydrocracking spent catalyst using citric acid, this study has been conducted. In order to justify the performance of citric acid, a comparative study has been conducted using both inorganic and organic acids in the same pH condition of about 1,5 - 2. pH was used as the controlled variable due to the different dissociation degree of the acids. In comparison to that of inorganic acid, the manganese recovery is four times higher when citric acid was applied. Acetic acid performed 33% lower in manganese recovery compared to the citric acid. Moreover, kinetics study was conducted with three varying temperature of 30C, 60C, and 90C. From the resulted data, it can be concluded that the kinetics of mengan leaching from spent catalyst using citric acid is in accordance to the shrinking core model. The controlling step is product diffusion with activation energy (Ea) of about 23.27 kJ/mol calculated using Arrhenius expression. With higher selectivity and leaching reagent which is harmless to the environment, the application of citric acid in manganese leaching from spent catalyst will indeed support the enactment of sustainable development aspect in recycle processing
Karakterisasi Larutan Polimer KYPAM HPAM untuk Bahan Injeksi dalam Enhanced Oil Recovery (EOR) Harimurti Wicaksono; Sutijan; Ahmad Tawfiequrrahman Yuliansyah
Jurnal Rekayasa Proses Vol 9, No 1 (2015)
Publisher : Departemen Teknik Kimia Fakultas Teknik Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/jrekpros.24524

Abstract

Polymer injection is one method of Enhanced Oil Recovery (EOR), where the polymer is dissolved in water, usually the formation water. Hydrolyzed polyacrylamide (HPAM) polymer types are most commonly used. This study aims to investigate the effect of KYPAM HPAM polymer concentration and operating conditions upon the water injection in order to determine the optimal injection system. Viscosity of polyacrylamide solution was measured with a Brookfield viscometer. Variation in salinity is carried out by mixing formation water with distilled water, whereas for high salinity of formation water using evaporation method. Shear rate was varied in the range of 145 s-1, while solution temperature was varied in the range of 70  87°C , and the effect of H2S gas in the solution was conducted by saturating the solution using natural gas which has concentration of H2S as 100 ppm. The results show that the effect of salinity solution has the greatest influence on the decrease in viscosity of the solution when compared to the other factors. Decrease in viscosity was due to agglomeration process resulting precipitate of polyacrylamide in the form of vaterite and aragonite morphology. The result also show that an increase in shear rate resulting lower viscosity. The increase in temperature causes the viscosity of the solution decreases. Meanwhile, the presence of H2S in the solution reduces the viscosity of the solution due to chemical degradation. Keywords: EOR, formation water, polymer injection, hydrolyzed polyacrylamide, salinity, polymer concentration. Injeksi polimer merupakan salah satu metode dalam Enhanced Oil Recovery (EOR). Dalam hal ini, polimer terlebih dulu dilarutkan dalam air, biasanya air formasi. Poliakrilamida terhidrolisis (HPAM) merupakan salah satu jenis polimer yang paling sering digunakan. Penelitian ini bertujuan untuk mengetahui pengaruh konsentrasi polimer KYPAM HPAM dan kondisi operasi pada injeksi air untuk menentukan sistem injeksi yang optimal. Larutan poliakrilamida diukur viskositasnya dengan viskometer Brookfield. Variasi salinitas dilakukan dengan mencampur air formasi dan aquades, sedangkan untuk salinitas tinggi dari air formasi dengan menggunakan metode penguapan.Variasi shear rate dilakukan pada kisaran 145 s-1, sedangkan suhu larutan divariasikan di kisaran 7087°C. Pengaruh gas H2S dalam larutan dilakukan dengan menjenuhkan larutan menggunakan gas alam yang memiliki konsentrasi H2S 100 ppm. Hasil penelitian menunjukkan bahwa salinitas memiliki pengaruh terbesar pada penurunan viskositas larutan bila dibandingkan dengan faktor-faktor lain. Penurunan viskositas disebabkan aglomerasi menghasilkan endapan poliakrilamida dalam bentuk vaterite dan morfologi aragonit. Hasil percobaan juga menunjukkan bahwa peningkatan shear rate, mengakibatkan viskositas larutan terukur rendah. Peningkatan suhu menyebabkan viskositas larutan turun, sedangkan kehadiran H2S dalam larutan mengurangi viskositas larutan karena terjadi degradasi kimia pada polimer. Kata kunci: EOR, air formasi, injeksi polimer, hydrolyzed polyacrylamide, salinitas, konsentrasi polimer
Pemanfaatan Cangkang Biji Pala sebagai Briket dengan Proses Pirolisis Rukmana; Suryo Purwono; Ahmad Tawfiequrrahman Yuliansyah
Jurnal Rekayasa Proses Vol 9, No 2 (2015)
Publisher : Departemen Teknik Kimia Fakultas Teknik Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/jrekpros.31033

Abstract

The abundance of nutmeg seed shells in Tidore is the reason to study the possibility to produce charcoal briquettes. The use of charcoal briquettes was expected to reduce waste of nutmeg seed shell and can be an alternative energy source with a high economic value. This study aims to investigate the effect of pyrolysis temperature and composition of tapioca adhesive to resulting quality of briquettes. The first step of the research was the preparation of nutmeg seed shells consisted of drying and size reduction into less than 20 mesh size. Afterward, the powder was put into furnace and heated to 350°C, 400°C, and 450°C for 90 minutes. During the process, volume of gas and liquids were measured every 15 minutes, while gas was sampled at 60-minute reaction. When pyrolysis was finished, about 20 g of charcoal was mixed with tapioca adhesive. The compositions of adhesive were 10%, 15%, 20%, 25%, and 30%. Finally, composite was formed in a cylindrical shape and compressed with hydraulic press at f 3 tons weight for a minute. The briquettes were then dried and analyzed with proximate analysis test. The results show that the highest calorific value was 6717.74 cal/g for material pyrolyzed at 450oC and 20% adhesive. The effect of adhesive on shatter index test showed that increasing composition of adhesive makes a better briquette quality as shown by a lower shatter index. In this study, the minimum weight loss was obtained by the addition of 30% adhesive. Keywords: briquettes, nutmeg seed shells, pyrolysis Ketersediaan cangkang biji pala yang melimpah di kota Tidore menjadi dasar dilakukannya penelitian mengenai pemanfaatan cangkang biji pala menjadi briket arang. Penggunaan briket arang diharapkan dapat mengurangi limbah cangkang biji pala dan sebagai sumber energi alternatif ramah lingkungan yang memiliki nilai ekonomi tinggi. Penelitian ini bertujuan untuk mempelajari pengaruh suhu pirolisis dan komposisi campuran perekat dengan arang cangkang biji pala terhadap kualitas briket. Tahap pertama dalam penelitian ini adalah penyiapan bahan baku berupa pengeringan dan penyesuaian ukuran cangkang biji pala sebesar 20 mesh. Tahap kedua yaitu proses pirolisis dengan cara memasukkan bubuk cangkang biji pala ke dalam tungku pirolisis (pirolisis selama 90 menit dengan variasi suhu 350oC, 400oC dan 450oC). Selama proses pirolisis berlangsung, volume gas dan cairan diukur setiap 15 menit, sedangkan pengambilan sampel gas dilakukan setelah pirolisis mencapai waktu 60 menit. Setelah dipirolisis, arang cangkang biji pala ditimbang seberat 20 gram kemudian bahan ini dicampurkan dengan perekat tapioka dengan variasi komposisi sebesar 10%, 15%, 20%, 25%, dan 30%. Setelah itu, arang cangkang biji pala dicetak dalam bentuk silinder dan dikempa dengan alat kempa hidrolik dengan berat 3 ton selama 1 menit. Briket kemudian dikeringkan dan dianalisis uji proksimat. Hasil uji proksimat menunjukkan bahwa nilai kalor yang tertinggi sebesar 6717,74 kal/g dimiliki oleh bahan hasil pirolisis suhu 450oC dengan campuran perekat 20%. Pengaruh perekat terhadap uji shatter index menunjukkan bahwa semakin tinggi kandungan perekat dalam briket maka semakin baik shatter index dari briket. Pada penelitian ini diketahui bahwa briket dengan penambahan perekat sebesar 30% mengalami kehilangan berat yang paling sedikit. Kata kunci: briket, cangkang biji pala, pirolisis
Produksi Organic Preservative dan Solid Biofuel dari Hydrothermal Treatment Tongkol Jagung dengan Variasi Temperatur Haidar Ali; Ahmad Tawfiequrrahman Yuliansyah
Jurnal Rekayasa Proses Vol 10, No 2 (2016)
Publisher : Departemen Teknik Kimia Fakultas Teknik Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/jrekpros.33338

Abstract

Corn is one of staple food and influential commodity driving Indonesia’s economy. Indonesia currently produces as high as 19 million tons of corn which contains 50% of biomass in the form of cob. Waste from harvesting and consumption of corn, namely, corn cob (CC) is left as waste. This CC is actually a sustainable, easily accessible, and renewable biomass energy source as an alternative to Indonesia’s depleting fossil fuel reserves. Hydrothermal treatment is a conversion method that has some consequential advantages compared to other methods; e.g. the ability to treat high-moisture biomass like CC and the possibility to use lower temperature. This research aims to produce and characterize liquid and solid fuel subsequent to hydrothermal treatment of CC obtained from Sleman, Yogyakarta. After size reduction, fine particles were mixed with water to form slurry. Slurry was heated in an autoclave for hydrothermal treatment at initial pressure of 2.0 MPa and was held for 200 °C, 240 °C, and 270 °C in 30 minutes. The solid and liquid products were then separated. Liquid was analyzed using GC-MS and solid by using AAS. The result showed that, in comparison to raw material, solid product had higher carbon content which resulted in the increase of calorific value of the solid biofuel. The calorific value of solid product ranged from 19,59 -22,02 MJ/kg or 20,93-35,87% higher than raw materials and 4-17% higher than average coal used in Indonesia. Major component in liquid product are N, N-dimethyl formamide, furfural, and phenolic compound, with benzoic acid present as minor component. The potential of liquid products as organic preservatives are examined by testing the tenacity of wood against termite according to ASTM D3345-74 standard method. Result showed that liquid product were effective in exhibiting termiticidal activity and temperature 200 °C showed the optimum condition.  ABSTRAKJagung merupakan salah satu makanan pokok dan komoditas yang berpengaruh terhadap ekonomi Indonesia. Produksi jagung Indonesia saat ini mencapai 19 juta ton dan sebanyak 50% berupa tongkol. Limbah dari pemanenan dan konsumsi jagung adalah tongkol jagung (CC) yang cepat busuk dan banyak kelemahannya yang harus ditangani. Sebetulnya, CC merupakan solusi yang berkelanjutan, mudah diperoleh, serta sumber energi terbarukan berupa biomassa yang dapat menjadi alternatif solusi untuk berkurangnya cadangan bahan bakar fosil di Indonesia. Hydrothermal treatment adalah metode konversi yang memiliki beberapa keunggulan jika dibandingkan dengan metode lain seperti kemampuan untuk menangani kandungan air yang tinggi pada CC dan kemungkinan penggunaan temperatur yang rendah. Penelitian ini bertujuan untuk mengkarakterisasi cairan dan padatan yang dihasilkan dari proses hydrothermal terhadap tongkol jagung yang diperoleh dari Sleman, Yogyakarta. Setelah proses reduksi ukuran, partikel halus tersebut dicampur dengan air sehingga terbentuk slurry. Slurry dipanaskan dalam autoclave untuk dijalankan proses hydrothermal dengan tekanan awal sebesar 2.0 MPa dan dijalankan pada suhu 200 °C, 240 °C, dan 270 °C dengan holding time selama 30 menit. Padatan dan cairan yang dihasilkan dipisahkan. Cairan dianalisis dengan GC-MS sedangkan padatan dengan AAS. Hasil menunjukkan bahwa dengan perbandingan bahan baku, padatan memiliki kandungan karbon yang lebih tinggi sehingga terjadi kenaikan nilai kalor. Nilai kalor padatan berkisar antara 19,59-22,02 MJ/kg atau 20,93-35,87% lebih tinggi dari bahan baku dan 4-17% dari batubara yang ada saat ini. Cairan yang dihasilkan didominasi oleh N,N-dimethyl formamide, furfural, phenolic compound serta sedikit asam berupa benzoic acid. Pengujian produk cairan sebagai pengawet organik dilakukan dengan pengujian ketahanan kayu terhadap rayap sesuai dengan standar ASTM D3345-74. Hasil menunjukkan bahwa cairan yang dihasilkan cukup efektif sebagai pembunuh rayap dan variasi temperatur 200 °C memberikan kondisi yang optimum.
Pengaruh Jenis Limbah dan Rasio Umpan pada Biokonversi Limbah Domestik Menggunakan Larva Black Soldier Fly (Hermetia illucens) Mahfudl Sidiq Muhayyat; Ahmad Tawfiequrrahman Yuliansyah; Agus Prasetya
Jurnal Rekayasa Proses Vol 10, No 1 (2016)
Publisher : Departemen Teknik Kimia Fakultas Teknik Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/jrekpros.34424

Abstract

The high content of protein is the main reason for domestic waste to be potentially processed by bioconversion using Hermetia illucens larvae. Hermetia illucens larva can accumulate protein content as high as 45-50% and fat which reaches 24-30%, so that it becomes a good source of highly nutritious feed. This research studied the production of Hermetia illucens larvae through bioconversion process on rice waste, cassava leaf, and mixed rice-cassava leaf (with the weight ratio of 1: 1), by varying the feed rate of 60, 80, and 100 mg/larva/day. The experiment was conducted for 21 days. Samples were taken periodically to be analyzed for their weight, substrate consumption, and waste reduction index. Proximate analysis was conducted on raw material and larvae media. The results of this study indicated that the optimum waste for larvae was the mixed rice-cassava leaf waste with feed rate of 60 mg/larva/day or total weight of 10.00 grams per feeding. At this condition, the optimal waste reduction in the bioconversion process was observed as substrate consumption of 65.82% and the waste reduction index of 18.02%. ABSTRAKTingginya kandungan protein membuat limbah domestik berpotensi untuk diproses secara biokonversi dengan menggunakan larva Hermetia illucens. Larva Hermetia illucens memiliki kandungan nutrisi protein yang mencapai 45-50% dan lemak yang mencapai 24-30%, sehingga dapat dijadikan sumber pakan bernutrisi tinggi. Penelitian ini mempelajari produksi larva Hermetia illucens melalui proses biokonversi pada limbah nasi, daun singkong dan campuran nasi-daun singkong (1:1), dengan memvariasikan feed rate sebesar 60, 80, 100 mg/larva/hari. Penelitian dilakukan selama 21 hari, dengan menganalisis berat larva, substrate consumption, dan waste reduction index. Analisis proksimat dilakukan pada media pakan dan larva. Hasil penelitian ini menunjukan bahwa limbah yang paling optimal memproduksi larva dalam proses ini adalah limbah campuran nasi-daun singkong dengan feed rate 60 mg/larva/hari atau dengan berat total 10,00 gram per feeding. Reduksi limbah paling optimal pada proses biokonversi teramati sebagai nilai konsumsi substrat sebesar 65,82% dan waste reduction index sebesar 18,02%.
Pengaruh Variasi Suhu Hidrotermal dan Aktivator Kalium Hidroksida (KOH) terhadap Kemampuan Hydrochar sebagai Adsorben pada Proses Adsorpsi Limbah Cair Metilen Biru Aziz Askaputra; Ahmad Tawfiequrahman Yuliansyah
Jurnal Rekayasa Proses Vol 14, No 2 (2020)
Publisher : Departemen Teknik Kimia Fakultas Teknik Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/jrekpros.57394

Abstract

Oil palm shell is one of biomass-wastes which is abundantly found in palm oil industries. Its economical value can be enhanced by converting it into hydrochar using a hydrothermal carbonization process (HTC). In this study, preparation of oil palm shell hydrochar was performed and the material was used as adsorbent to remove methylene blue from waste water. Effects of HTC temperature, KOH activator concentration, and adsorption time were studied. Functional groups of hydrochar were evaluated by Fourier transform infrared (FTIR) spectroscopy. Meanwhile, the uptake capacity of hydrochar to adsorp methylene blue was measured by using UV-Vis spectrophotometer. The results showed that dehydration and decarboxylation reactions took place more progressively at the higher temperature of HTC. It was also found that activation process resulted higher removal efficiency of methylene blue. The highest adsorption capacity (16.58 mg/g, with removal efficiency 99.51%) was obtained by hydrochar prepared by HTC 270°C, KOH 1.5 N, and carried out for 80 minutes.Keywords: activator; adsorption; hydrothermal carbonization; methylene blue; oil palm shellA B S T R A KTempurung kelapa sawit merupakan salah satu limbah biomassa yang jumlahnya cukup melimpah di industri minyak kelapa sawit. Nilai ekonomi tempurung kelapa sawit dapat ditingkatkan, salah satunya melalui hydrothermal carbonization process (HTC). Dalam penelitian ini, hydrochar dari tempurung kelapa sawit dibuat dan digunakan sebagai adsorben untuk menjerap metilen biru dari limbah cair. Dalam hal ini, akan dipelajari pengaruh suhu HTC, konsentrasi aktivator KOH, dan durasi adsorpsi. Gugus fungsional hydrochar dianalisis dengan FT-IR spectroscopy, sementara itu kapasitas adsorpsi terhadap metilen biru diukur dengan spektrofotometer UV-Vis. Hasil percobaan menunjukkan bahwa reaksi dehidrasi dan dekarboksilasi pada kondisi hidrotermal terjadi lebih cepat pada suhu HTC yang lebih tinggi. Selain itu, proses aktivasi dengan KOH terbukti dapat meningkatkan efisiensi penyisihan metilen biru. Kapasitas adsorpsi maksimum sebesar 16,58 mg/g (dengan efisiensi penyisihan 99,51%) dihasilkan dari adsorpsi dengan menggunakan hydrochar yang diperoleh dari HTC suhu 270 °C, diaktivasi dengan KOH 1,5 N dan durasi adsorpsi selama 80 menit.Kata kunci: adsorpsi; aktivator; karbonisasi hidrotermal; metilen biru; tempurung kelapa sawit 
Optimasi Biaya dalam Proses Pemurnian Metanol untuk Mengurangi Resin sebagai Limbah Bahan Berbahaya dan Beracun di PT Kaltim Methanol Industri Reno Imam Arthapersada; Muhammad Kurniawan Adiputra; Indra P Hakim; Imam Karfendi Putro; Asep P Zainuddin; Lisendra Marbelia; Ahmad Tawfiequrahman Yuliansyah
Jurnal Rekayasa Proses Vol 14, No 2 (2020)
Publisher : Departemen Teknik Kimia Fakultas Teknik Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/jrekpros.59553

Abstract

Purification process of raw methanol from its impurities to produce pure methanol at PT. Kaltim Methanol Industri (PT KMI) is carried out by several steps, including degassing, distillation, and adsorption. One of the impurities, tri methyl amine (TMA), could be removed by adding NaOH. Another method to remove TMA is conducted by adsorption process on ion exchange resin on the vessel called TMA catchpot. The TMA catchpot performance is very crucial in methanol purification process. Thus, monitoring and optimization are required to be performed regularly. Once the TMA catchpot resin has exhausted, the performance will be drop and methanol purification could not be done efficiently. Furthermore, the ion exchange resin should be replaced with new resin. This study evaluates the performance of the TMA catchpot during the charge of 2010, 2012, and 2016, calculates the NaOH consumption during operational time, and optimizes the cost. Resin regeneration option was introduced and compared with the conventional method (i.e. resin replacement). Economic evaluation shows that the lowest annual cost could be obtained by fresh resin replacement every 4 years and resin regeneration every 2 years. Resin regeneration option gives not only annual cost reduction, but also positive impact to the environment, by decreasing the amount of hazardous waste (i.e. spent resin) significantly.Keywords: ion exchange resin; methanol purification; regeneration; tri methyl amineA B S T R A KProses pemurnian metanol mentah (raw) dari pengotornya untuk menghasilkan metanol murni di PT. Kaltim Methanol Industri (PT KMI) dilakukan melalui beberapa tahapan antara lain degassing, distilasi dan adsorpsi. Salah satu zat pengotor adalah tri methyl amine (TMA) yang dapat dihilangkan dengan penambahan NaOH. Metode lain untuk menghilangkan TMA adalah dengan proses adsorpsi menggunakan resin penukar ion di dalam tangki yang disebut TMA catchpot. Performa TMA catchpot sangat penting dalam proses pemurnian metanol. Oleh karena itu, pemantauan dan optimalisasi perlu dilakukan secara berkala. Setelah resin pada TMA catchpot jenuh, performanya akan menurun dan pemurnian metanol tidak dapat dilakukan secara efisien. Selanjutnya, resin penukar ion harus diganti dengan resin baru. Artikel ini mengevaluasi kinerja catchpot TMA pada penggantian resin (charge) 2010, 2012 dan 2016, menghitung konsumsi NaOH sebagai fungsi waktu operasi, dan mengoptimasi biaya pemurnian. Selain itu, disimulasikan opsi regenerasi resin, sebagai pembanding metode konvensional (penggantian resin). Evaluasi ekonomi menunjukkan bahwa biaya tahunan paling rendah didapatkan dengan penggantian resin baru setiap 4 tahun, dan regenerasi resin setiap 2 tahun. Selain biaya tahunan yang rendah, regenerasi ini berdampak positif terhadap lingkungan dengan mengurangi timbulan limbah B3 (resin bekas) secara signifikan.Kata kunci: pemurnian metanol; regenerasi; resin penukar ion; tri metil amin 
Evaluasi Aspek Teknis dan Lingkungan Instalasi Pengolahan Air Limbah (IPAL) Komunal di Kabupaten Sleman Yogyakarta Dwi Saputri; Fajar Marendra; Ahmad Tawfiequrrahman Yuliansyah; Ir. Agus Agus Prasetya Prasetya
Jurnal Rekayasa Proses Vol 15, No 1 (2021)
Publisher : Departemen Teknik Kimia Fakultas Teknik Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/jrekpros.65833

Abstract

As the producer of waste (both in solid form and wastewater), the increase of population creates a dominant effect on environmental problems. Escalation of the amount of domestic wastewater has led to greater sanitation problems. Indonesian government has carried out several programs for improving sanitation access and facilities. Community-based wastewater treatment plant (Communal WWTP) is one of the priority programs. Sleman Regency in Special Province of Yogyakarta owns 131 communal WWTP, where the oldest one had been built in 2006 while the newest one was installed in 2018. In this study, the techno-environmental assessment of communal WWTP in the District of Sleman, Yogyakarta was carried out. Sampling selection of communal WWTPs was undertaken using Stratified Random Sampling techniques. Data collection was executed by a combination of field surveys and in depth-interview of several relevant personnel. The study was done for 30 communal WTTP in various Districts in Sleman regency. Assessment was carried out based on the Likert scale of 4. The results showed that the average score for environment aspect was 2.94 (good), while that for technical aspect was 3.52 (very good). Overall, the techno-environmental score of communal WWTP in Sleman Regency, Yogyakarta was 3.23 out of 4, which was categorized as good.Keywords: communal WWTP; domestic wastewater; Likert scale sanitation; Sleman regency; stratified random samplingA B S T R A KSebagai produsen limbah (baik limbah padat maupun air limbah), peningkatan jumlah penduduk berpengaruh dominan terhadap masalah lingkungan. Eskalasi jumlah air limbah domestik berujung pada masalah sanitasi yang semakin besar. Pemerintah Indonesia sudah menjalankan beberapa program untuk meningkatkan fasilitas dan akses sanitasi. Instalasi pengolahan air limbah komunal (IPAL) menjadi salah satu program prioritas. Kabupaten Sleman memiliki 131 IPAL komunal, yang tertua dibangun tahun 2006 dan yang terbaru pada tahun 2018. Dalam penelitian ini, asesmen teknologi lingkungan (techno-environment) dilakukan terhadap IPAL komunal di Kabupaten Sleman, Yogyakarta. Pengumpulan data dikerjakan menggunakan kombinasi metode survei lapangan dan wawancara mendalam dengan pelaku IPAL komunal yang relevan. Pemilihan sampel IPAL komunal dipilih menggunakan teknik Sampling Acak Terstratifikasi (Stratified Random Sampling). Penelitian dilakukan terhadap 30 IPAL Komunal di berbagai Kecamatan di Kabupaten Sleman.  Asesmen dilakukan berdasarkan skala Likert (4). Hasil penelitian menunjukkan bahwa aspek lingkungan memperoleh skor rata-rata 2,94 (baik) dan aspek teknis-teknologis 3,52 (sangat baik). Secara keseluruhan kategori teknologi-lingkungan (techno-environment) dari IPAL Komunal di Kabupaten Sleman Yogyakarta mempunyai skor rata-rata 3,23 dari nilai maksimal 4, dan dikategorikan sebagai baik.Kata kunci: air limbah domestic; IPAL komunal; Kabupaten Sleman; sanitasi; Sampling Acak Terstratifikasi; skala Likert
DESULFURISASI BATUBARA MENGGUNAKAN ASAM NITRAT (HNO3) Muhamad Johar Ardany; Ahmad Tawfiequrrahman Y.; Suryo Purwono
Prosiding Conference on Research and Community Services Vol 1, No 1 (2019): Prosiding Conference on Research and Community Services)
Publisher : STKIP PGRI Jombang

Show Abstract | Download Original | Original Source | Check in Google Scholar

Abstract

Desulfurisasi batubara merupakan proses penurunan kadar sulfur dalam batubara, dimana pembakaran batubara yang mengandung sulfur  dapat menyebabkan kerusakan pada alat dan pencemaran lingkungan salah satunya adalah terjadinya hujan asam. Tujuan penelitian ini adalah untuk menentukan kondisi optimal leaching sulfur dalam batubara menggunakan asam nitrat. Metode yang digunakan adalah desulfurisasi untuk memisahkan komponen sulfur yang terikat dalam batubara. Proses desulfurisasi dilakukan selama 2 jam pada temperatur ruang. Optimasi leaching menggunakan asam nitrat dilakukan dengan variasi konsentrasi 10%-30% dan rasio S/L (15gram/150mL). Dari hasil analisis didapatkan bahwa konsentrasi optimum asam nitrat adalah 15% yang mampu mereduksi sulfur sebesar 57%. Konsentrasi asam nitrat sangat mempengaruhi seberapa besar sulfur yang dapat di reduksi dalam batubara. Semakin tinggi konsentrasi asam nitrat, semakin tinggi % sulfur yang terambil pada batubara. Pentingnya hasil dari penelitian ini yaitu industri yang menggunakan batubara sebagai bahan bakar pabrik mampu menerapkan proses desulfurisasi ini sehingga polusi yang dihasilkan dari hasil pembakaran semakin kecil. Selain itu, proses ini sangat membantu pengusaha batubara yang mengekspor batubara.
Co-Authors Achmad Diansyukma Agus Prasetya Ahmad Hanafi Arief Budiman Asep P Zainuddin Aziz Askaputra Bagus Putro Budi Utomo Bratakusuma, Danu Britania Dewi Clarasinta Budi Kamulyan C. Chika Oktalia Putri Cahyono, Rochim Bakti Claudino de Almeida Cabral D Bratakusuma Danu Bratakusuma Dedi Eko Yunanto Dewi Purnama Sari Dewi Purnama Sari Dwi Saputri Dwi Saputri Edia Rahayuningsih Erlina Kurnianingtyas Fajar Marendra Fajar Marendra Fami Amalia Putri Fika Rofiek Mufakir Fika Rofieq Mufakhir Fitriani Fitriani Haidar Ali Handayani, Destias Selly Harimurti Wicaksono Hary Sulistyo Hasanah, Nur Hayati Himawan Tri Bayu Murti Petrus Imam Karfendi Putro Indra P Hakim Kidung Wulan Utami Lestari, Dwi Indah Lisendra Marbelia Mahfudl Sidiq Muhayyat Marendra, Fajar Mufakhir, Fika Rofieq Muhamad Johar Ardany Muhammad A. A. Ramadhan, Muhammad Muhammad Irsan B Muhammad Kurniawan Adiputra mulhidin, mulhidin Pasca Giffari Jusuf Rahmah, Puspa Reno Imam Arthapersada Riski Amalia, Riski Rizka Lestari Rizki Laksono, Rizki RR. Ella Evrita Hestiandari Rukmana Saputri, Dwi Sarto Sarto Septina AVIA Avia Shinta Virdhian shinta virdhian, shinta Sri Puji Saraswati Suprianto Suprianto Suryo Purwono Sutijan Wahyu Wilopo Widi Astuti Widi Astuti Widi Astuti Y Iskandar Yuni Rosita Yusuf Iskandar Zakiah Awalia J S Dahlan