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Multistage Sonication Effect on the Composition and Properties of Degraded Chitosan Product Arifin, Nurul Laili; Savitri, Emma; Indah, Anjar; Putra, Fesa; Sumarno, Sumarno
Makara Journal of Technology Vol. 23, No. 1
Publisher : UI Scholars Hub

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Abstract

The sonication method randomly breaks polymer chains to produce a varied distribution of products. A scheme with multi-stage sonication steps is proposed to identify oligomers and low molecular weight chitosan based on changes to the degrad-ed product. For each sonication level, 1% (w/v) chitosan in 1% (v/v) aqueous acetic acid was sonicated for 120 min at 60 °C. The products of the sonication treatment were deprotonized by adding an alkali solution, freeze dried and insoluble product re-sonicated until a low molecular weight was produced. Low molecular weight chitosan/insoluble products were character-ized with Fourier-transform infrared spectra (FT-IR) and X-ray diffraction (XRD) to determine the effect of multistage soni-cation on degree of deacetylation (DD) and degree of crystallinity. The viscosity of the average molecular weight of insolu-ble chitosan was estimated by a viscometric method, while the degree of polymerization (DP) of the chitosan oligomers (COS) were determined by end group analysis. The results showed that the molecular weight of insoluble chitosan decreased and reached a limiting value, (Mlim). The percent yield of oligoglucosamine of the soluble products increased with the num-ber of the sonication stages. The degree of crystallinity of insoluble chitosan increased from 19% to 34.14% while the DD decreased from 82% to 78.1%.
Rancang Bangun Kerangka Tanaman Hidroponik Politeknik Negeri Batam Pamungkas, Nurman; Widiastuti, Hanifah; Restu, Fedia; Leksonowati, Nur Fitria Pujo; Arifin, Nurul Laili; Muvariz, Mufti Fathonah; Ulfah, Nurul; Widodo, Widodo; Baharudin, Budi; Fajrin, Aulia; Fyona, Annisa; Kamsyah, Domi; Gemala, Mega; Rosbandrio, Wowo; Aryswan, Adhe; Siregar, James; Saputra, Hendra; Irawan, Benny Haddli; Saputra, Ihsan; Ariyanto, Nugroho Pratomo; Mutiarani, Mutiarani
Jurnal Pengabdian kepada Masyarakat Politeknik Negeri Batam Vol 5 No 1 (2023): Jurnal Pengabdian kepada Masyarakat Politeknik Negeri Batam
Publisher : Politeknik Negeri Batam

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30871/abdimaspolibatam.v5i1.4866

Abstract

The hydroponic pilot project in the Batam State Polytechnic area was motivated by problems with economic conditions and declining health conditions during the Covid-19 pandemic. This project is expected to support the “growing your own food movement” in an effort to reduce unemployment, increase food security and a healthy lifestyle. The hydroponic method was chosen because it is very easy to do and does not require a large area of ​​land. In this community service activity, a hydroponic plant building framework will be made as a prototype of an efficient and efficient hydroponic building so that it can be used by the wider community. This activity is also useful for applying design knowledge as one of the PbL activities carried out by CAD, CNC, CAM, and Fabrication Engineering courses in the Mechanical Engineering Department, so that it can become an arena for higher education participation to support people's lives. The method of implementing this community service activity is to make observations to find a suitable area to build a hydroponic plant house, then the results of the observations are poured in the form of a design by utilizing software so that the materials needed and the shape of the framework that is built can be known. The last activity is making a hydroponic plant place. This activity is planned to be carried out from April to November 2021. Based on the results of the evaluation of the service program questionnaire for product distribution, it is known that the majority of respondents are satisfied with the products produced.
Perbandingan Ketangguhan Material S355G7+M Pada Pengelasan SAW (Original) dan SMAW (Repair) Dengan Metode Impact Charpy V-Notch Puspita, Roza; Rahman, Muhammad Noval; Arifin, Nurul Laili; Butar Butar, Hendra
Jurnal Teknologi dan Riset Terapan (JATRA) Vol. 6 No. 1 (2024): Jurnal Teknologi dan Riset Terapan (JATRA) - June 2024
Publisher : Politeknik Negeri Batam

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30871/jatra.v6i1.7624

Abstract

Proses pengelasan SAW menggunakan fluks yang berbentuk seperti pasir yang berfungsi melindungi logam pengisi yang mencair saat proses pengelasan agar tidak terjadinya kontaminasi dengan udara luar sehingga didapatkan hasil pengelasan yang cukup baik. Sedangkan elektroda SMAW (Shielded Metal Arc Welding) diselaputi atau dilindungi oleh fluks dengan proses pengerjaan secara manual. Penelitian ini bertujuan untuk menganalisa perbandingan hasil pengelasan dengan menggunakan metode standar WPS PS-03 (Original) dan WPS PS-03R (Repair), dengan menggunakan pengujian impact untuk mengetahui ketangguhan pada spesimen S355G7+M. Pengujian ini bertujuan untuk mengetahui ketangguhan impact pada bagian hasil pengelasan pada WPS PS-03 (Original) dan WPS PS-03R (Repair). Spesimen WPS PS-03R memiliki nilai lebih besar di bandingkan dengan spesimen WPS PS-03. Apabila nilai kekuatan spesimen semakin besar, maka semakin kuat dan tangguh pula pada spesimen tersebut. Temperatur pada spesimen sangat berpengaruh terhadap keuletan atau kegetasan suatu logam. Semakin tinggi temperaturnya maka semakin ulet logam tersebut begitupun sebaliknya.
OPTIMALISASI SUMBER DAYA DAN TEKNOLOGI DALAM PROGRAM PEMBERDAYAAN MASYARAKAT DESA PULAU JEMARE Leksonowati, Nur Fitria Pujo; Pamungkas, Nurman; Butar, Hendra Butar; Aryswan, Adhe; Juangsa Putra, Lalu Giat; Fyona, Annisa; Nugroho, Cahyo Budi; Wibowo, Ari; Gemala, Mega; Ariyanto, Nugroho Pratomo; Arifin, Nurul Laili; Puspita, Roza; Sriyanto, Sriyanto; Dzulfiqar, Mohamad Alif; Stefani, Windy; Batubara, Ninda Hardina; Fajrin, Aulia; Purba, Adi Syahputra; Manurung, Meilani Mandhalena; Budiman, Budiman
Jurnal Pengabdian kepada Masyarakat Politeknik Negeri Batam Vol. 7 No. 1 (2025): Jurnal Pengabdian kepada Masyarakat Politeknik Negeri Batam
Publisher : Politeknik Negeri Batam

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30871/abdimaspolibatam.v7i1.7105

Abstract

This paper discusses in depth the implementation of the Village Community Empowerment Program (P2MD) carried out on Jemare Island. The main focus of this program is the application of appropriate technology, which includes public street lighting and a water pump system, both powered by solar panels. The main objective of this initiative is to improve the quality of lighting and the provision of clean water on the island, two important aspects that are greatly needed by the local residents. Through a series of intensive observations and discussions with the local residents, the community service team was able to identify and solve various problems faced by the residents. As a result of these efforts, four street lights have been successfully installed and operated, and the water pump system has been successfully connected to the water pump machine and water storage tank. It is hoped that this initiative can have a significant positive impact on the quality of life of the residents of Jemare Island, support their business activities and economy, and provide a solution to the uneven distribution of electricity by the state electricity company (PLN). This solution is practical because it utilizes renewable energy in the form of sunlight, which is abundantly available on Jemare Island.