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JURNAL KIMIA SAINS DAN APLIKASI

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Published by Universitas Diponegoro

ISSN : 14108917 EISSN : 25979914 DOI : -

Core Subject : Science, Engineering,

Chemical Engineering, Chemistry & Bioengineering Chemistry Engineering

urnal Kimia Sains dan Aplikasi (p-ISSN: 1410-8917) and e-ISSN: 2597-9914) is published by Department of Chemistry, Diponegoro University. This journal is published four times per year and publishes research, review and short communication in field of Chemistry.

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Articles 796 Documents

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Mass Effect of Coconut Shell-derived Activated Carbon on Adsorption of Benzene, Toluene, Ethylbenzene, and Xylene in Motorcycle Emissions Trisna Yuliana; Aini Aspiati Rohmah; Yusuf Eka Maulana; Arie Hardian
Jurnal Kimia Sains dan Aplikasi Vol 24, No 4 (2021): Volume 24 Issue 4 Year 2021
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

The use of motorized transportation in Indonesia is now proliferating. The higher the use of motorized vehicle-based transportation in an area, the higher the potential for air pollution. One of the air pollutants is a mixture of benzene, toluene, ethylbenzene, and xylene (BTEX). This study examines the effect of coconut shell-derived activated carbon adsorbent mass which is adjusted with different thicknesses on its adsorption ability for BTEX. The adsorbent is used to adsorb the emissions of the 1990 GL-Pro motorcycle with premium fuel. The results of gas chromatography-mass spectroscopy (GC-MS) show that motor vehicle emissions contain BTEX and other hydrocarbons. ANOVA variant analysis showed that the difference in mass of activated carbon in the range of this study did not provide a significant difference in BTEX adsorption.Keywords: adsorbent; motor vehicle emissions; BTEX pollutants; coconut shell

Design New Compound of Meisoindigo Derivative as Anti Breast Cancer Based on QSAR Approach Agus Dwi Ananto; Handa Muliasari; Saprizal Hadisaputra
Jurnal Kimia Sains dan Aplikasi Vol 23, No 9 (2020): Volume 23 Issue 9 Year 2020
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

Design new compounds of Meisoindigo using the QSAR approach with semiempirical methods have been successfully made with better biological activity as anti-breast cancer results. The research method used to design the new compound of meisoindigo derivatives uses the semiempirical methods. The research procedure divide into tree step, molecular modeling, QSAR equation analysis, and design of new compounds. The PM3 method was chosen as a better method because it has model results that are more representative of physicochemical aspects. The selection of the best model is made by multilinear regression statistical analysis. New compounds derived from the design are expected to bind to the Cyclin-Dependent Kinase 4 (CDK4) enzyme that helps in the cell cycle to prevent cell division. Based on the design, the compound of (E)-2-(2-oxo-1-(2-(trifluoromethyl) benzyl)indolin-3-ylidene)-N-(quinoline-7-yl) acetamide choose as a new compound with more better biological activity (log 1/IC50 = 6.992) than before (log 1/IC50 = 5.823)

The Effectiveness of Adding Red Fruit Oil (Pandanus conoideus Lamk.) into Ethanol Extract of Temulawak rhizome (Curcuma xanthorrhiza Roxb.) as Antioxidant Sari Purbaya; Lilis Siti Aisyah; Dona Nopitasari
Jurnal Kimia Sains dan Aplikasi Vol 23, No 11 (2020): Volume 23 Issue 11 Year 2020
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

Curcuma xanthorrhiza Roxb (temulawak) is a native Indonesian plant; ethnobotanically, it can facilitate breast milk, body fresheners, stomach lozenges, and seizure medications. Temulawak contains essential oils, curcuminoids, and xanthorrhizol. Curcuminoids and xanthorrhizol have potential as antioxidants. Antioxidants in the body are useful for preventing oxidation reactions caused by free radicals, both from body metabolism and external factors. Curcuminoids are difficult to dissolve in water and have a very low bioavailability. Combining curcuminoids with oil can increase the absorption of curcuminoids into the systemic system. The low solubility and bioavailability can be overcome by combining temulawak rhizome extract and red fruit oil. Pandanus conoideus Lamk (red fruit), ethnobotanically, effectively prevents blindness, intestinal worms, skin diseases, and increasing stamina. Red fruit contains vitamin C, vitamin E, flavonoids, and β-carotene, potentially as antioxidants. Each sample of Curcuma and red fruit, as well as a mixture of Curcuma and red fruit samples, were tested for their antioxidant activity using the DPPH method (1,1-diphenyl-2-picrylhydrazyl). The ethanol extract of temulawak rhizome has intense antioxidant activity because it has an IC50 of 55.21 ppm. Red fruit oil has feeble antioxidant activity because it has an IC50 of 2604.77 ppm. The 1: 1 ratio between red fruit oil and the ethanol extract of temulawak rhizome has weak antioxidant activity because it has an IC50 of only 1568.24 ppm. Meanwhile, the 1:10 ratio of red fruit oil and ethanol extract of temulawak rhizome has robust antioxidant activity because it has an IC50 of 19.85 ppm. It is concluded that the addition of oil to the ethanol extract of Curcuma can increase antioxidant activity.

Docking and Molecular Dynamic Simulations Study to Search Curcumin Analogue Compounds as Potential Inhibitor Against SARS-CoV-2: A Computational Approach Neni Frimayanti; Adel Zamri; Yum Eryanti; Noval Herfindo; Veza Azteria
Jurnal Kimia Sains dan Aplikasi Vol 24, No 3 (2021): Volume 24 Issue 3 Year 2021
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

Coronavirus is a pandemic in the world. It requires researchers and scientists to work hard to find a vaccine or drug to inhibit the development of the coronavirus. Many drugs have been used, such as remdesivir, lopinavir, and chloroquine. However, how effective is the use of these drugs for inhibiting the coronavirus’s growth? There is no research has been done. Curcumin is now known as one of the compounds that have some biological activities, and it is also can potentially be used as a CoV-2 inhibitor. The computational study, i.e., molecular docking and molecular dynamic, can help researchers to predict which compounds have the potential as an inhibitor against the CoV-2 coronavirus. In this study, lopinavir was used as a positive control. Lopinavir and 45 curcumin analog compounds were docked against the main protease protein with 6LU7 PDB ID. Based on the docking results, it was discovered that compound 1, compound 2, and compound 4 have the same binding orientation as lopinavir. Molecular dynamic simulation with the lowest binding free energy conformation was used to check these compounds’ stability. Only compound 4 was maintained to observe hydrogen bonding with Lys5 and Lys137 with a distance of 2.9 Å. The distance of hydrogen bonds and binding free energy over simulation time is essential to elucidate the potential compound’s affinity. For then, compound 4 can be used as a potential inhibitor against the CoV-2 coronavirus.

MgO-supported Ni-Sn Catalysts: Characterization and Catalytic Properties for Aqueous-phase Catalytic Reforming of Glycerol Kiky Corneliasari Sembiring; Anis Kristiani; Luthfiana Nurul Hidayati; Sudiyarmanto Sudiyarmanto; Fauzan Aulia; Asif Aunillah
Jurnal Kimia Sains dan Aplikasi Vol 24, No 6 (2021): Volume 24 Issue 6 Year 2021
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

The aqueous phase reforming (APR) of glycerol into value-added products, including H2 and alkanes, is environmentally green. In this work, the conversion of glycerol into syngas was demonstrated using MgO-supported Ni-Sn catalysts. Ni species is known for its capability of converting glycerol, but the activity towards water gas shift (WGS) reaction has not been satisfied. Loading Ni-Sn onto MgO has increased the catalyst basicity, which promotes a positive effect in WGS reaction. A series of bimetallic catalysts, impregnated Ni-Sn on MgO support, was prepared with various Ni-Sn loading amounts. To better understand the behavior of prepared catalysts, they were evaluated physio-chemically through XRD, BET, and FTIR. The catalytic activity test was performed for APR in a continuous flow reactor with aqueous glycerol 10 v-% as a feedstock at a reaction temperature of 250°C. As a result, the maximum hydrogen selectivity was obtained at about 73 v-%.

The Coated-Wire Ion-Selective Electrode (CWISE) of Tartrazine Using Chitosan as an Ionophore Dewi Umaningrum; Radna Nurmasari; Siti Hasnah; Maria Dewi Astuti; Kiki Amalia Wardhani; Shofia Qalby
Jurnal Kimia Sains dan Aplikasi Vol 24, No 6 (2021): Volume 24 Issue 6 Year 2021
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

Research on the Ion-Selective Electrode (ISE) of coated wire-type tartrazine using chitosan as an ionophore has been developed. The variables used in the manufacture of ISE are membrane composition and immersion time. Meanwhile, the basic characteristics of ISE measured are Nernst value, measurement concentration range, detection limit, and measurement response time. The results showed that ISE tartrazine coated wire type had an optimum membrane composition in a mixture of chitosan: PVC: DOP of 3: 34: 63 (% w/w) and a membrane immersion time 20 minutes. The basic characteristics of ISE produce a Nernst value of 20.976 mV/decade. The measurement concentration range is 1×10-7-1×10-2 M with a detection limit of 2.749×10-7 M or 0.1469 ppm. The response time ranges from 10-60 seconds, with an average of 40 seconds.

Production of Organic Acid and Short-Chain Fatty Acids (SCFA) from Lactic Acid Bacteria Isolate on Oligosaccharide Media Yati Maryati; Lilis Nuraida; Ratih Dewanti Hariyadi
Jurnal Kimia Sains dan Aplikasi Vol 24, No 6 (2021): Volume 24 Issue 6 Year 2021
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

The growth of microorganisms in food, one of which is lactic acid bacteria (LAB), can produce metabolites beneficial to health. It is essential to study the results of LAB metabolism to improve the quality of a functional food product. This study aimed to evaluate the isolates Lactobacillus acidophilus FNCC 0051 and Lactobacillus rhamnosus R23 to metabolize oligosaccharides as a carbon source so that the final fermentation product can benefit health especially in lowering cholesterol. In vitro testing was carried out on MRS media with or without oligosaccharides, either singly or in a combination consisting of galactooligosaccharides (GOS), fructooligosaccharides (FOS), inulin (IN), inulin hydrolyzate (HI), or their combination as prebiotics by adding 0.3 % oxbile (bile salt) and inoculated with 1% v/v LAB isolate culture and incubated at 37°C for 24 hours. The results showed that the main product of oligosaccharide metabolism by L. acidophilus FNCC 0051 and L. rhamnosus R23 produced several organic acids (lactic acid), including short-chain fatty acids (SCFA) (acetic acid, propionic acid, and butyric acid). The single and combined carbon sources affected the proportion of lactic acid and acetic acid produced by L. acidophilus FNCC0051 (p<0.05). However, they did not affect the proportions of propionic acid and butyric acid. While in L. rhamnosus R23 (p<0.05), the presence of a single carbon source significantly affected the proportions of lactic acid, acetic acid, propionic acid, and butyric acid, while the combination of oligosaccharides affected the proportions of lactic acid and butyric acid produced. SCFA is the main product of prebiotic metabolism, but the characteristics of the acid produced have not been identified. The fermentation pattern is thought to be related to molecular weight, chain length, and oligosaccharide structure. Short-chain molecules, such as FOS generally ferment more rapidly than long-chain molecules such as inulin. The results of this study indicate that both isolates can be used as probiotics in the development of symbiotic products with the addition of oligosaccharides, which have a physiological effect in lowering cholesterol levels.

Facile Synthesis of ZnO Nanoparticles for the Photodegradation of Rhodamine-B Tety Sudiarti; Neng Hani Handayani; Yusuf Rohmatulloh; Silmi Rahma Amelia; Ravli Maulana Yusuf; Atthar Luqman Ivansyah
Jurnal Kimia Sains dan Aplikasi Vol 24, No 6 (2021): Volume 24 Issue 6 Year 2021
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

River pollution is a problem that is still very poorly handled. Industrial growth is the most significant contributor to produce this wastewater. The industry produces liquid waste such as dyes that do not meet handling standards because of the high cost. Photocatalyst is way better than other methods such as adsorption, coagulation, fluctuation, and others. However, there are still many shortcomings of the existing methods, such as high cost, high temperature, and dangerous by-products. This research seeks to provide a solution by synthesizing zinc oxide (ZnO) nanoparticles as a photocatalyst to reduce rhodamine B dye under visible light irradiation. ZnO nanoparticles were successfully synthesized through a simple sol-gel method in the form of a white powder by heating at a low temperature, 60°C. The XRD results show that the results have a diffraction peak that follows the standard ZnO with a hexagonal wurtzite crystal structure. According to the Scherrer equation, the crystal has a size of 22.61 nm. SEM analysis showed that the particle morphology and particle size were homogeneous with a spherical shape, ranging from 22-24 nm. Optimal ZnO photocatalytic activity at 90 minutes with an efficiency of 98.83%.

TiO2-PDMS Super Hydrophilic Coating with Self-Cleaning and Antimicrobial Properties Dessy Ariyanti; Afiatin Afiatin; Pury Diana Shintawati; Aprilina Purbasari
Jurnal Kimia Sains dan Aplikasi Vol 24, No 6 (2021): Volume 24 Issue 6 Year 2021
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

In this paper, self-synthesized TiO2 nanoparticle was used as a coating material with the addition of polydimethylsiloxane (PDMS) on the surface of the glass and ceramic substrate via spray coating. The self-cleaning properties of the coating with photocatalytic activity mechanism were observed under irradiation of black lamp as well as surface wettability. The antimicrobial properties and the morphology under a scanning electron microscope were also investigated. The results showed that the coating exhibited self-cleaning properties, as demonstrated by the photocatalytic degradation of methylene blue up to 80% and wettability as a super hydrophilic layer with a water contact angle less than 10° for both glass and ceramic substrate. The coating also shows an antimicrobial property by extending the radius of microbial growth up to 67% compared to the uncoated sample. 3% TiO2 addition with 50% w/w PDMS is the optimum coating ratio for maximum photocatalytic activity, super hydrophilic, and antimicrobial properties.

Encapsulation of Gemor Bark Extract Using Cetyltrimethylammonium bromide-Modified Nanocellulose Salsabila Aqila Putri; Sunardi Sunardi
Jurnal Kimia Sains dan Aplikasi Vol 24, No 7 (2021): Volume 24 Issue 7 Year 2021
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

Gemor (Nothaphoebe coriacea) is one of the plants of Non-Timber Forest Product typical of wetlands with secondary metabolite compounds such as alkaloids, steroids, flavonoids, triterpenoids, and phenolics. Besides being used as an insecticide, gemor bark also has antioxidant activities, anti-influenza, antivirus, antiherpes, and anti-inflammatory. This study aimed to encapsulate gemor bark extract using cetyltrimethylammonium bromide (CTAB)-modified nanocellulose to increase the effectiveness of its use. The result showed that gemor bark extract had an IC50 value of 39.97 ppm. In comparison, encapsulated gemor bark extract (Gemor-Nc-4 mM CTAB) had an excellent antioxidant activity with an IC50 value of 98.41 ppm and encapsulation efficiency of 53.70 %.

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Adi Darmawan

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Adi Darmawan

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Kota semarang,

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