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Synthesis of Hydroxyapatite From Chicken Bones Using the High Temperature Method Bagus Setiawan, Riyanda; Zhafran Mumtaz, Faishal; Suprianti, Lilik; Mahendra Kusuma, Ramadhani
AJARCDE (Asian Journal of Applied Research for Community Development and Empowerment) Vol. 10 No. 1 (2026)
Publisher : Asia Pacific Network for Sustainable Agriculture, Food and Energy (SAFE-Network)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29165/ajarcde.v10i1.869

Abstract

This study investigates the syntesys of hydroxyapatite (HAp) from chicken bone waste, which is abundantly available due to high poultry production, using a high-temperature method. The objective of this study was to determine the effect of variations in sintering temperature (300, 400, 500, and 600°C) and sintering time (3, 4, 5, 6, and 7 hours) on the yield and Ca/P ratio of the HAp produced. The prepared chicken bone powder was first calcined at 900°C for 3 hours before sintering. The results showed that the optimal conditions were 600°C for 7 hours, characterized by a change in the sample's colour to white and a yield of 69%. XRF analysis confirmed the formation of HAp with a Ca/P ratio of 1.69. It was concluded that a sintering temperature of 600°C for 7 hours is optimal for producing pure HAp from chicken bone waste. Contribution to Sustainable Development Goals (SDGs):SDG 3: Good Health and Well-beingSDG 9: Industry, Innovation and InfrastructureSDG 12: Responsible Consumption and Production
Optimasi Konsentrasi HCl Dan Suhu Kalsinasi Terhadap Yield Produk MgCl2 Dari Bittern Annisa, Nur; Diah Nur Fitri Midayoga; Lilik Suprianti; Srie Muljani
Jurnal Serambi Engineering Vol. 11 No. 1 (2026): Januari 2026
Publisher : Faculty of Engineering, Universitas Serambi Mekkah

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Abstract

The brine solution remaining after salt crystallization contains high levels of valuable minerals, particularly magnesium, which can be extracted and processed into magnesium chloride (MgCl₂), a compound widely used in various industrial applications. This study examines the effect of hydrochloric acid (HCl) concentration and calcination temperature on the yield of MgCl₂ synthesized from brine-derived magnesium hydroxide. Magnesium hydroxide was precipitated using sodium hydroxide and subsequently reacted with HCl solutions of varying concentrations (1N–5N) before being calcined at temperatures ranging from 350°C to 550°C. The results show that both HCl concentration and calcination temperature significantly influence the product yield. The highest yield, 80.07%, was obtained at an HCl concentration of 4N and a calcination temperature of 550°C. While increasing acid concentration and temperature generally improved yield, concentrations above 4N did not provide further benefits and instead tended to decrease efficiency. These findings highlight key processing parameters for optimizing MgCl₂ production from brine, contributing to more efficient resource utilization and environmentally sustainable mineral processing practices.