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Mechanical and tribological properties of nano-sized Al2O3 particles on ADC12 alloy composites with Strontium modifier produced by stir casting method Muhammad Wira Akira; Hanuna Haritsah; Anne Zulfia; Ekavianti Prajatelistia
ADI Journal on Recent Innovation Vol. 3 No. 1 (2021): September
Publisher : ADI Publisher

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.34306/ajri.v3i1.346

Nano-Al2O3 particles were incorporated into ADC12 alloy with the addition of Al-5Ti-B, Al-Sr, and Mg to achieve high performance in mechanical and tribological properties. In this study, varied nano-Al2O3 was used from 0.25 vf-% to 0.5 vf-% through stir casting methods to discover the optimum amount to obtain high performance. Besides, the inclusion of grain refiner Al-5Ti-B and microstructure modifier Al-Sr is expected to improve performance to the next level. However, porosity and agglomeration still be a concern in Aluminum alloy matrix composite fabrication. The presence of spinel phase MgAl2O4 in the interface area between nano-Al2O3 particles and ADC12 alloy is relied upon to minimize this porosity and agglomeration issue. The optimum of tensile strength and hardness was found at 0.35 vf-% Al2O3 and wear rate at 0.4 vf%. Although, the optimum point of wear found at 0.4 vf%, porosity began to increase at 0.4 vf% as well. As a result, 0.35 vf% addition of the nano-Al2O3 gives the best performance for the composite.

Influence of Chemical Treatments Sequence on Morphology and Crystallinity of Sorghum Fibers Ismojo Ismojo; Abdul Aziz Ammar; Ghiska Ramahdita; Anne Zulfia; Mochamad Chalid
Indonesian Journal of Chemistry Vol 18, No 2 (2018)
Publisher : Universitas Gadjah Mada

Micro-fibrillated cellulose (MFC) derived from natural fibre is continuously gaining interest to produce an environmentally-friendly material, due to economic and ecological reasons. In consequence, sorghum is one of the most-cultivated crops that usually remain the waste as by product of bioethanol production. Indeed, it will be a promising area to utilize sorghum waste to produce MFC for enhancing polymer performance, especially in terms of crystallinity. The objective of this study is to investigate the effect of a sequence of chemical modification was applied to sorghum fibres, i.e. alkalization using 4% sodium hydroxide followed by bleaching using 1.7% sodium chlorite plus acetic acid as a buffer. The treatment was purposed to unbundle the lignocellulose networks into microfibrils cellulose with less amorphous part and lower hydrophilic properties. Evaluation of the chemical treatments effect on internal microstructure, crystallinity index and chemical composition of sorghum fibre was measured via Field-Emission Scanning Electron microscope (FE-SEM), X-ray Diffraction (XRD) and Fourier Transformation Infra-Red (FTIR) Spectroscopy. The experiments show that treatments led to a removal of binding materials, such as amorphous parts hemicellulose and lignin, from the sorghum fibres, resulting MFC of sorghum fibres and enhanced crystallinity index from 41.12 % to 75.73%.

Effect of Sodium in LiNi0,5Mn0,3Co0,2O2 as a Lithium Ion Battery Cathode Material by Solid State Reaction Method Yustinus Purwamargapratala; Indra Gunawan; Evvy Kartini; Anne Zulfia; Alexey Glushshenkov; D.N. Haerani; Sudirman Sudirman
Journal of Fibers and Polymer Composites Vol. 1 No. 1 (2022): Journal of Fibers and Polymer Composites
Publisher : Green Engineering Society

Abstract. Lithium-ion batteries (LIBs) have become widely used powder sources for portable electronics and electric vehicles. The discovery of lithium nickel manganese cobalt oxide (LiNi0.5Mn0.3Co0.2O2, NMC532), tremendous efforts have been paid to the development of Ni-rich layer-structured NMC532 materials due to its high capacity when charged to potentials higher than 4.3 V vs Li+/Li. In this work we report effect of Sodidium in NMC532 layer, the characterization was done by using X-Ray Diffractometer (XRD) to investigate the crystal structure, Electrochemical impedance spectroscopy (EIS) was used to illustrate the resistance change during cycling. The particles morphology and surface chemistry characterizations of both cathode and anode electrodes were performed on Scanning Electron Microscope (SEM). The XRD pattern of the sample shows diffraction peaks at 2θ = 18.663 o, 36.773 o, 44.459 o, 48.611 o, 58.604 o, 64.322 o, 65.069 o, 68.339 o and 77.798 o. Na does not affect the NMC532 lattice parameters, which means that Na which is expected to substitute for Li does not occur. The NMC532 conductivity with the addition of Na=0.03 showed a slightly lower value than the NMC532 conductivity with the addition of Na=0.01. Meanwhile, the highest conductivity was seen at NMC532 with the addition of Na=0.05. The addition of Na to NMC532 did not increase the conductivity linearly. SEM images of NMC532 and NMC532 with the addition of Na=0.01; Na = 0.03 and Na = 0.05 can be seen that the Na flakes wrap around the NMC532 granules. The Na flakes surrounding the NMC532 grains at Na = 0.01 were more abundant than the Na flakes surrounding the NMC532 at Na = 0.03.

Studi Pelapisan Komposit Ni-P-Nano Al2O3 Dengan Metode Electroless Co-Deposition [Study of Ni-P-Nano Al2O3 Composite Coating With Electroless Co-Deposition Methode] Yulinda Lestari; Effendi Mabruri; Anne Zulfia Syahrial
Metalurgi Vol 31, No 1 (2016): Metalurgi Vol. 31 No. 1 April 2016
Publisher : National Research and Innovation Agency (BRIN)

The Ni-P-nano powder Al2O3 composite coating have been prepared by electroless codeposition method. It has advantage that the process does not require an electrode, fast deposition rate, good corrosion and wear resistance. In this study, the variable parameters are the addition of nano powder Al2O3 composition. The aim of this research is to determine microstructure phenomenon, phase and crystalinity, chemical composition and distribution on coating surface, and corrosivity Ni-P-nano powder Al2O3 composite coating.The substrate is used stainless steel 410. Substrates have been pre treated in order to activate the surface. Then, substrate immersed in solution that consisting of nickel sulfate, sodium hypophosphite, ammonium sulfate, sodium acetate, lead acetate and nano alumina powder. The substrate is immersed about 60 minutes at a 90±2 °C temperature with speed of 150 rpm. Sample characterization has done by SEM-EDS, XRD, and CMS. Results indicate there is a microstructure visual difference before and after electroless coating process.Based on variable experiment, the optimum nanopowder Al2O3 compositionis 10 gr/l which have given the best paticle distribution and most excellent corrosion resistance.AbstrakPelapisan material dengan komposit Ni-P-nano powder Al2O3 yang menggunakan metode electroless kodeposisi memiliki keunggulan yaitu prosesnya tidak membutuhkan elektroda, laju deposisi yang cepat danmemiliki ketahanan korosi dan ketahanan aus yang baik. Pada penelitian ini, parameter yang divariasikan adalah komposisi penambahan nano powder Al2O3. Penelitian ini bertujuan untuk mengetahui fenomena struktur mikro, fasa dan kristalinitas, komposisi kimia dan distribusi unsur di permukaan coating, danketahanan korosi komposit coating Ni-P-nano powder Al2O3. Substrat yang digunakan yaitu baja tahan karat 410 dilaku awal (pretreatment) untuk mengaktivasi permukaan, kemudian direndam dalam larutan yang terdiri dari nikel sulfat, natrium hypophosphite, ammonium sulfat, sodium asetat, lead asetat dan serbuk nano alumina. Substrat direndam selama 60 menit, dalam suhu proses 90±2 °C dengan kecepatan putaran 150 rpm. Karakterisasi sampel dilakukan menggunakan alat SEM-EDS (scanning electron microscopy-energy dispersive spectroscopy), XRD (x-ray diffraction), dan CMS (corrosion measurement system). Dari hasil percobaan menunjukkan terdapat perbedaan struktur mikro antara substrat logam dasar dan substrat setelahproses electroless coating. Berdasarkan variabel percobaan, untuk komposisi nano powder Al2O3 yang optimum adalah 10 gr/l karena memberikan distribusi partikel dan ketahanan korosi yang paling baik.

PENGARUH Mg TERHADAP KEKERASAN KOMPOSIT MATRIKS KERAMIK Al2O3/Al Sahari, G.N. Anastasia; Zulfia, Anne; Siradj, Eddy S.
Makara Journal of Science Vol. 13, No. 1
Publisher : UI Scholars Hub

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Magnesium Effect to the Hardness of Al2O3/Al Ceramic Matrix Composites. Composite is an alternative material which has satisfying properties and can be accommodated for certain applications. Ceramic Matrix Composites (CMCs) is one of the composite types that are very interesting in terms of high temperature applications material. In this paper, we investigate the effects of Mg addition on the hardness of Al2O3 Ceramic Matrix Composites which was produced by directed metal oxidation (Dimox) method. The CMCs material is made by placing Al ingot under mixture alumina and percentage of Mg 5, 8, 10, and 12% wt. The processing temperature was 1100°C for 24 hours followed by cooling to room temperature in the furnace. The results show that increasing of infiltration, the hardness increased to 1221 VHN maximum at 8% wt Mg and then decrease again as the increment amount of Mg.

KOMPAKTIBILITAS KOMPOSIT ISOTROPIK Al/Al2O3 DENGAN VARIABEL WAKTU TAHAN SINTER Widyastuti, Widyastuti; Siradj, Eddy S; Priadi, Dedi; Zulfia, Anne
Makara Journal of Science Vol. 12, No. 2
Publisher : UI Scholars Hub

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Compactibility of Al/Al2O3 Isotropic Composite with Variation of Holding Time Sintering. The requirement of component with structural ability, light weight and also strength is increasing base on Metal Matrix Composites (MMCs) by aluminum as matrix (AMCs). A structural ability is connected to composites compactibility which is depend on quality of interfacial bounding. Powder metallurgy is one of method to produce composite with powder mixing, compacting and sintering. Volume fractions reinforced and sintering time can influence composites compactibility. Volume fractions reinforced variable can produce different reinforcement effect. Beside that, on sintering enables the formation of new phase during sintering time. In this research, Al/Al2O3 isotropic composites are made with aluminum as matrix and alumina (Al2O3) as reinforced. Volume fraction reinforced used 10%. 20%. 30% and 40%. Sintering temperature and compaction pressure are each 600o C and 15 kN. The tests that applied are compression and metallographic test. The result that obtained is optimum compactibility of Al/Al2O3 composite reached at holding time 2 hour. During sintering, new phase can occur that is aluminum oxides (alumina), with unstable properties. The best volume fraction reinforced and holding time sintering are 40% and 2 hours.

PENGARUH PELAPISAN PERMUKAAN PARTIKEL SiC DENGAN OKSIDA METAL TERHADAP MODULUS ELASTISITAS KOMPOSIT Al/SiC Zainuri, M; Siradj, Eddy S; Priadi, Dedi; Zulfia, Anne; Darminto, Darminto
Makara Journal of Science Vol. 12, No. 2
Publisher : UI Scholars Hub

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The Influence of Coating Oxide Metal on Surface of SiC Particles to Elastic Modulus of Al/SiC Composites. The isotropic composites of Al/SiC is made by powder metallurgy method, the quality of mechanical materials depend on interfacial bonding between matrix (Al) and reinforcement (SiC). The quality of interfacial bonding can influence to elastic modulus of composites which is made by solid process. SiC particles were coated by metal oxide aim to enhance quality interfacial bonding between matrix and reinforcement. These research using three kinds of coating materials, which are Mg oxide, Cu oxide and Al oxide, and these materials were deposited on surface of SiC particles. From three kinds of materials coating Al2O3 is the best to enhance quality interfacial bonding between matrix and reinforce than the others as CuO or MgO. There is Intermetalic phase formatted on CuO coating, and MgO coating have many porous where they can make decrease quality of Al-SiC composites. All of volume fraction of SiC on the Al/SiC composites, which oxide aluminum coating on SiC surface have highest value of elastic modulus than the others metal oxides.

KOMPAKTIBILITAS KOMPOSIT ISOTROPIK Al/Al2O3 DENGAN VARIABEL WAKTU TAHAN SINTER Widyastuti, Widyastuti; Siradj, Eddy S; Priadi, Dedi; Zulfia, Anne
Makara Journal of Science Vol. 11, No. 2
Publisher : UI Scholars Hub

Show Abstract | Download Original | Original Source | Check in Google Scholar

Compactibility of Al/Al2O3 Isotropic Composite with Variation of Holding Time Sintering. The requirement of component with structural ability, light weight and also strength is increasing base on Metal Matrix Composites (MMCs) by aluminum as matrix (AMCs). A structural ability is connected to composites compactibility which is depend on quality of interfacial bounding. Powder metallurgy is one of method to produce composite with powder mixing, compacting and sintering. Volume fractions reinforced and sintering time can influence composites compactibility. Volume fractions reinforced variable can produce different reinforcement effect. Beside that, on sintering enables the formation of new phase during sintering time. In this research, Al/Al2O3 isotropic composites are made with aluminum as matrix and alumina (Al2O3) as reinforced. Volume fraction reinforced used 10%. 20%. 30% and 40%. Sintering temperature and compaction pressure are each 600o C and 15 kN. The tests that applied are compression and metallographic test. The result that obtained is optimum compactibility of Al/Al2O3 composite reached at holding time 2 hour. During sintering, new phase can occur that is aluminum oxides (alumina), with unstable properties. The best volume fraction reinforced and holding time sintering are 40% and 2 hours.

PENGARUH PELAPISAN PERMUKAAN PARTIKEL SiC DENGAN OKSIDA METAL TERHADAP MODULUS ELASTISITAS KOMPOSIT Al/SiC Zainuri, M; Siradj, Eddy S; Priadi, Dedi; Zulfia, Anne; Darminto, Darminto
Makara Journal of Science Vol. 11, No. 2
Publisher : UI Scholars Hub

Show Abstract | Download Original | Original Source | Check in Google Scholar

The Influence of Coating Oxide Metal on Surface of SiC Particles to Elastic Modulus of Al/SiC Composites. The isotropic composites of Al/SiC is made by powder metallurgy method, the quality of mechanical materials depend on interfacial bonding between matrix (Al) and reinforcement (SiC). The quality of interfacial bonding can influence to elastic modulus of composites which is made by solid process. SiC particles were coated by metal oxide aim to enhance quality interfacial bonding between matrix and reinforcement. These research using three kinds of coating materials, which are Mg oxide, Cu oxide and Al oxide, and these materials were deposited on surface of SiC particles. From three kinds of materials coating Al2O3 is the best to enhance quality interfacial bonding between matrix and reinforce than the others as CuO or MgO. There is Intermetalic phase formatted on CuO coating, and MgO coating have many porous where they can make decrease quality of Al-SiC composites. All of volume fraction of SiC on the Al/SiC composites, which oxide aluminum coating on SiC surface have highest value of elastic modulus than the others metal oxides.

KOMPAKTIBILITAS KOMPOSIT ISOTROPIK Al/Al2O3 DENGAN VARIABEL WAKTU TAHAN SINTER Widyastuti, Widyastuti; Siradj, Eddy S; Priadi, Dedi; Zulfia, Anne
Makara Journal of Science Vol. 12, No. 2
Publisher : UI Scholars Hub

Show Abstract | Download Original | Original Source | Check in Google Scholar

Compactibility of Al/Al2O3 Isotropic Composite with Variation of Holding Time Sintering. The requirement of component with structural ability, light weight and also strength is increasing base on Metal Matrix Composites (MMCs) by aluminum as matrix (AMCs). A structural ability is connected to composites compactibility which is depend on quality of interfacial bounding. Powder metallurgy is one of method to produce composite with powder mixing, compacting and sintering. Volume fractions reinforced and sintering time can influence composites compactibility. Volume fractions reinforced variable can produce different reinforcement effect. Beside that, on sintering enables the formation of new phase during sintering time. In this research, Al/Al2O3 isotropic composites are made with aluminum as matrix and alumina (Al2O3) as reinforced. Volume fraction reinforced used 10%. 20%. 30% and 40%. Sintering temperature and compaction pressure are each 600o C and 15 kN. The tests that applied are compression and metallographic test. The result that obtained is optimum compactibility of Al/Al2O3 composite reached at holding time 2 hour. During sintering, new phase can occur that is aluminum oxides (alumina), with unstable properties. The best volume fraction reinforced and holding time sintering are 40% and 2 hours.

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