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All Journal ILMU KELAUTAN: Indonesian Journal of Marine Sciences JURNAL KIMIA SAINS DAN APLIKASI Jurnal Ilmu Kimia Universitas Brawijaya Journal of Innovation and Applied Technology Indonesian Green Technology Journal The Journal of Pure and Applied Chemistry Research JURNAL INTEGRASI PROSES Journal of Geoscience, Engineering, Environment, and Technology JFMR (Journal of Fisheries and Marine Research) Indonesian Journal of Chemistry CARADDE: Jurnal Pengabdian Kepada Masyarakat Jurnal Kartika Kimia Molekul: Jurnal Ilmiah Kimia JKPK (Jurnal Kimia dan Pendidikan Kimia) Acta Chimica Asiana Bulletin of Chemical Reaction Engineering & Catalysis Indonesian Mining Journal
Yuniar Ponco Prananto
Department Chemistry, Faculty Of Mathematics And Natural Sciences, University Of Brawijaya, Jl. Veteran 65145, Malang, Indonesia
Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Earth & Planetary Sciences Education Energy Engineering Environmental Science Materials Science & Nanotechnology Medicine & Pharmacology Physics Social Sciences Other

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Journal : Bulletin of Chemical Reaction Engineering

 1 
Synthesis of Fluorite (CaF2) Crystal from Gypsum Waste of Phosphoric Acid Factory in Silica Gel Mohammad Misbah Khunur; Andri Risdianto; Siti Mutrofin; Yuniar Ponco Prananto
Bulletin of Chemical Reaction Engineering & Catalysis 2012: BCREC Volume 7 Issue 1 Year 2012 (June 2012)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.7.1.3171.71-77

Abstract

This paper report the synthesis and characterization of fluorite single crystal prepared from gypsum waste of phosphoric acid production in silica gel. Instead of its high calcium, gypsum was used to recycle the waste which was massively produces in the phosphoric acid production. The gypsum waste, the raw material of CaCl2 supernatant, was dissolved in concentrated HCl and then precipitated as calcium oxalate (CaC2O4) by addition of ammonium oxalate. The CaCl2 was obtained by dissolving the CaC2O4 with HCl 3M. The crystals were grown at room temperature in silica gel and characterized by AAS, FTIR and powder XRD. The optimum crystal growth condition, which is pH of gel, CaCl2 concentration and growth time, were investigated. The result shows that at optimum condition of pH 5.80, CaCl2 concentrations of 1.2 M, and growth time of 144 hours, colorless crystals with the longest size of 3 mm, were obtained (72.57%). Characterization of the synthesized crystal by AAS indicates that the obtained crystal has high purity. Meanwhile, analysis by FTIR spectra shows a Ca–F peak at 775 cm-1, and powder-XRD analysis confirms that the obtained crystal was fluorite (CaF2). © 2012 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0)
Study of Gel Growth Cobalt (II) Oxalate Crystals as Precursor of Co3O4 Nano Particles Yuniar Ponco Prananto; Mohammad Misbah Khunur; Dini Tri Wahyuni; Rizky Arief Shobirin; Yoga Rizky Nata; Efiria Riskah
Bulletin of Chemical Reaction Engineering & Catalysis 2013: BCREC Volume 7 Issue 3 Year 2013 (March 2013)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.7.3.4066.198-204

Abstract

Crystal growth of cobalt (II) oxalate in silica gel at room temperature as precursor of Co3O4 nano particles has been studied. Specifically, this project is focusing on the use of two different reaction tube types toward crystallization of cobalt (II) oxalate in gel. The gel was prepared at pH 5 by reacting sodium metasilicate solution with dilute nitric acid (for U-tube) and oxalic acid (for straight tube), with gelling time of 4 days and crystal growth time of 8 (for straight tube) and 12 (for U-tube) weeks. Result shows that pink crystalline powder was directly formed using straight tube method. The use of different solvents in straight tube method affects crystallization and could delay direct precipitation of the product. In contrast, bigger and better shape of red block crystal was yielded from U-tube method; however, longer growth time was needed. FTIR studies suggest that both growth method produces identical compound of hydrated cobalt (II) oxalate. © 2013 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0)
Synthesis and Structure of 2D Cobalt(II)-tartrate Hydrate Coordination Polymers Crystallised from Aqueous Solution Mohammad Misbah Khunur; Yuniar Ponco Prananto
Bulletin of Chemical Reaction Engineering & Catalysis 2018: BCREC Volume 13 Issue 2 Year 2018 (August 2018)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.13.2.1342.213-219

Abstract

Cobalt(II)-tartrate hydrate coordination polymer is successfully crystallisedfrom aqueous solution at room temperature. Unlike previous methods, diammonium tartrate was used and reacted directly with an aqueous solution of cobalt(II). Single crystal X-ray and ATR-IR analyses were performed toward the synthesized crystal. The crystal structure displaysa (6,3) 2D sheet which then grow into a 3D hydrogen-bonded network. Tetra- and hexa-dentate dianionic tartaric ligands are observed in the crystal structure, in which the hexadentate ligand connects four different cobalt centres. This method is considered feasible, affordable, and simple for the production of functional polymeric cobalt(II)-tartrate hydrate. 
One Pot Synthesis of Calcium Sulfate Hemihydrate from Fishbone-derived Carbon Teguh Wirawan; Mukhamad Nurhadi; Agung Rahmadani; Yuniar Ponco Prananto; Zhiying Zhu; Sin Yuan Lai; Hadi Nur
Bulletin of Chemical Reaction Engineering & Catalysis 2023: BCREC Volume 18 Issue 3 Year 2023 (October 2023)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.19515

Abstract

Calcium Sulfate Hemihydrate (CSH) with uniform morphology and high crystallinity were successfully prepared by a precipitation-hydrolysis method in a concentrated sulfuric acid solution containing fishbone-derived carbon. The CSH was produced by carbonization of fishbone powder at 500 °C for 2 h, followed by sulfonation with concentrated sulfuric acid for 3 h. The solid mixture was washed until the pH of 2, then left at room temperature for 3 days. Physical properties of synthesized CSH were characterized using Fourier transform infrared (FTIR) spectroscopy, X-ray diffraction (XRD), wavelength dispersive X-ray fluorescence (WDXRF), Scanning Electron Microscope (SEM), nitrogen adsorption-desorption isotherm, and melting point test. It is concluded that the CSH were formed due to hydrolysis of fishbone-derived carbon in a moderately concentrated sulfuric acid solution of carbon-derived fishbone and crystallization into a fibrous octa calcium phosphate (OCP) form. In this research, effect of crystal growth time, effect of pH during the crystal growth, and effect of volume of the solution were also investigated. Copyright © 2023 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). 
Oxidation of Styrene to Benzaldehyde Using Environmentally Friendly Calcium Sulfate Hemihydrate-Supported Titania Catalysts Koesnarpadi, Soerja; Wirawan, Teguh; Nurhadi, Mukhamad; Wirhanuddin, Wirhanuddin; Prananto, Yuniar Ponco; Nazarudin, Nazarudin; Degirmenci, Volkan; Lai, Sin Yuan; Nur, Hadi
Bulletin of Chemical Reaction Engineering & Catalysis 2024: BCREC Volume 19 Issue 4 Year 2024 (December 2024)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.20224

Abstract

This paper presents the synthesis and characterization of calcium sulfate hemihydrate (CSH)-supported titania (TiO2) catalysts and their application in the environmentally friendly oxidation of styrene to benzaldehyde using hydrogen peroxide (H2O2) as the oxidant. The study explores the catalyst's structure-activity relationship, emphasizing the importance of mesoporous materials for enhanced catalytic performance. The CSH-Titania catalysts were synthesized using fish bone-derived CSH as a support, which aligns with green chemistry principles. Characterization techniques such as Fourier Transform Infra Red (FTIR), X-ray Diffraction (XRD), Scanning Electron Microscope (SEM), and Brunauer-Emmett-Teller (BET) surface area analysis confirmed the successful impregnation of titania and its catalytic efficiency. The catalysts exhibited high selectivity for benzaldehyde, achieving up to 49.45% conversion of styrene, with benzaldehyde as being the main product. The research highlights that the catalyst’s performance decreased after calcination due to a reduced surface area and pore volume, yet it maintained recyclability across three cycles with minimal  lose  in selectivity loss. Overall, this study introduces a cost-effective and sustainable approach to styrene oxidation, demonstrating the potential for industrial application in producing high-value chemicals with minimal environmental impact. Copyright © 2024 by Authors, Published by BCREC Publishing Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).
Co-Authors Adhinanda, Arrival Arsyad Adi Kurnia Soesantyo Adiba, Naila Azmi Afif Eka Rahma Setiyanto Agustina, Laily Aulia Ahmad Syarwani Andi Nafis An Naafi Andri Risdianto Andri Risdianto Ani Mulyasuryani Arie Srihardyastutie Ariesta, Muhammad Naufal Atsuhiko Isobe Choi, Jonghyun Danar Purwonugroho Danar Purwonugroho Danar Purwonugroho Danar Purwonugroho Danar Purwonugroho Danu Setia Wardana Darjito Darjito Darjito Defri Yona Degirmenci, Volkan Diana Ningrum, Diana Dias Satria Dini Tri Wahyuni Dini Tri Wahyuni Dyah Ajeng Pitaloka Efiria Riskah Efiria Riskah Elvian Eka Krisnaniningrum Evitantri, Mangesti Reza Fanny Prasetia Faustina De Yesu Prisila Abi Febriani, Rakhma Finisia, Yenni Firsta Luthfiani Salsabila Fuad, M.Arif Zainul Grafist, Therra Raditya Hadi Nur Hadi Nur Karti'a, Galuh Wahyu Kashifa Maria Jihan Lai, Sin Yuan Ledhyane Ika Harlyan M. Naufal Tsaqif Dzakwan Mangesti Reza Evitantri Mochamad Arif Zainul Fuas Mochamad Nurcholis Mohammad Misbah Khunur Mohammad Misbah Khunur Mohammad Misbah Khunur Mohammad Misbah Khunur Muhammad Misbah Khunur Mukhamad Nurhadi, Mukhamad Naila Azmi Adiba Nazarudin Nidatul Syarifah Qonitah Fardiyah Rachmat Tjahjanto Rachmat Triandi Tjahjanto Radiansyah, Muhamad Agus Rafi Dwiasis Wibisono Rahmadani, Agung Rizky Arief Shobirin Rizky Arief Shobirin Rosmawati, Angelina Sasti Gona Fadhilah Silvi Zakiyatul Ilmiyah Sin Yuan Lai Siti Mutrofin Siti Mutrofin Soerja Koesnarpadi Sri Wardhani Suyono, Suyono Syarifah, Nidatul Taufiq, Muhammad Arif Teguh Wirawan Teguh Wirawan, Teguh Tutik Setianingsih Tutik Setianingsih Wenny Bekti Sunarharum Wirhanuddin, Wirhanuddin Yeni Dwi Lestari Yenni Finisia Yofandi, Muhammad Farrel Yoga Rizky Nata Yoga Rizky Nata Yogi Rifki Wijayanto Zhiying Zhu