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Resti Nurmala Dewi
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JURNAL REKAYASA KIMIA & LINGKUNGAN
Published by Universitas Syiah Kuala
ISSN : 14125064     EISSN : 23561661     DOI : https://doi.org/10.23955/rkl.v18i2.34018
Core Subject : Science, Engineering,
Chemical Engineering, Chemistry & Bioengineering Energy Engineering
The Journal of Chemical Engineering and Environment is an open access journal that publishes papers on chemical engineering and environmental engineering. The following topics are included in these sciences: Food and biochemical engineering Catalytic reaction engineering Clean energy technology Environmental and safety technology Fundamentals of chemical engineering and applied industrial engineering Industrial chemical engineering Material science engineering Process and control engineering Polymer and petrochemical technology Membrane technology Agro-industrial technology Separation and purification technology Environmental modelling Environmental and information sciences Water and waste water treatment and management Material flow analysis Mechanisms of clean development
Arjuna Subject : Teknik Kimia (semua kategori) - Bioengineering
Articles 319 Documents
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Simulasi Unit Stripping CO2 Dalam Packed Column Skala Industri Dengan Kondisi Non-Isothermal Nisa, Nur Ihda Farikhatin; Altway, Ali; S, Susianto
Jurnal Rekayasa Kimia & Lingkungan Vol 14, No 1 (2019): Jurnal Rekayasa Kimia & Lingkungan (June, 2019)
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v14i1.13547

Abstract

Emisi karbondioksida ke atmosfer dianggap sebagai penyebab utama perubahan iklim, termasuk pemanasan global dan permasalahan pertanian. Berbagai teknologi pemisahan CO2 banyak dikembangkan. Absorpsi kimia adalah teknologi pemisahan yang paling efektif dan banyak digunakan dalam industri kimia maupun petrokimia. Dimana pelarut yang telah digunakan dapat di regenerasi kembali di kolom stripper. Stripping adalah proses regenerasi termal pelarut dimana larutan tersebut dikontakkan dengan pelarut gas yang tidak larut terhadap cairan tersebut. Penelitian ini bertujuan untuk mengembangkan simulasi unit stripping CO2 dalam packed column skala industri dengan mengestimasi kinerja unit stripping CO2 yang dinyatakan dengan % efisiensi kolom stripping dan komposisi gas yang keluar dari stripper. Simulasi dilakukan secara teoritis dengan mengembangkan model matematis untuk proses stripping CO2 dalam packed column skala industri. Selanjutnya hasil simulasi divalidasi dengan data riil pada salah satu industri pupuk di Indonesia. Variabel-variabel yang digunakan adalah tekanan operasi kolom, temperatur rich solution dan laju steam. Hasil simulasi untuk tekanan stripper 2,56 atm dengan laju rich solution 2943316 kg/jam dan temperatur rich solution 390 K menunjukkan CO2 (% mol) 99,038%, sedangkan data pabrik menunjukkan 97,5862%.
Kombinasi Proses Elektrokoagulasi Oksidasi Lanjut Berbasis O3/GAC Pada Limbah Cair Industri Batik Enjarlis, Enjarlis; Hartanto, Singgih; Christwardana, Marcelinus; Sijabat, Boy Frando; Fatlan, Ode Resa
Jurnal Rekayasa Kimia & Lingkungan Vol 14, No 1 (2019): Jurnal Rekayasa Kimia & Lingkungan (June, 2019)
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v14i1.12274

Abstract

Gabungan proses Elektrokoagulasi-Oksidasi Lanjut (EC-OL) berbasis O3/GAC merupakan teknologi alternatif untuk mengolah limbah cair industri Batik. Limbah cair industri batik mengandung Bahan Berbahaya dan Beracun, mempunyai COD 500 - 3000 ppm, BOD 1200 ppm dan TSS 10.000 ppm serta tidak memenuhi Baku Mutu Lingkungan.Tujuan penelitian gabungan EC-OL pada limbah cair batik yaitu menentukan: (a) waktu optimum proses Elektrokoagulasi (EC), (b) dosis ozon dan jumlah karbon aktif yang tepat pada Oksidasi Lanjut berbasis O3/GAC (OL), dan (c) pengaruh gabungan proses Elektrokoagulasi-Oksidasi Lanjut (EC-OL) berbasis O3/GAC terhadap konstanta laju degradasi kontaminan organik (k) dalam limbah cair industri Batik. Pada gabungan proses EC-OL, untuk elektrokoagulasi digunakan elektroda Al, kuat arus 1 A tetap, dan waktu proses (20, 40 dan 60 menit) dan Oksidasi Lanjut (OL) dilakukan pada dosis ozon (0,0625; 0,125 dan 0,1875 gr O3/liter) dan massa GAC (10, 20 dan 30 gram). Parameter uji yang digunakan yaitu nilai COD, Total suspention solid (TSS) dan warna limbah. Dari hasil percobaan diperoleh: (a) waktu proses elekrtrokoagulasi terbaik selama 60 menit dengan penurunan COD 54 % dan TSS 31%, (b) pada proses OL berbasis O3/GAC diperoleh dosis ozon terbaik sebesar 0,125 gr O3/L dan massa GAC sebanyak 30 gram dengan penurunan COD 61,11% dan TSS 15,33% dan (c) Pada gabungan proses EC-OL penurunan COD terjadi sebesar 95,08% dan TSS 81,39% dan konstanta laju degradasi kontaminan organik sebesar 0,6931 min-1.
Modifikasi Alat Penyuling Uap untuk Peningkatan Rendemen dan Mutu Minyak Nilam (Pogostemon cablin Benth) Mahlinda, Mahlinda; Arifiansyah, Vinno; Supardan, Muhammad Dani
Jurnal Rekayasa Kimia & Lingkungan Vol 14, No 1 (2019): Jurnal Rekayasa Kimia & Lingkungan (June, 2019)
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v14i1.13475

Abstract

Penyulingan minyak nilam konvensional umumnya menggunakan peralatan penyulingan sederhana yang memilikii beberapa kekurangan yaitu: waktu proses yang lama, konsumsi energi yang besar dan rendemen minyak yang rendah. Tujuan penelitian ini adalah melakukan modifikasi alat penyuling uap untuk peningkatkan rendemen dan mutu minyak nilam yang dihasilkan. Modifikasi yang dilakukan adalah: penambahan pipa api pada boiler, pengaturan aliran air yang masuk ke dalam boiler, pemasangan economizer dan penambahan unit pemanas lanjut. Hasil penelitian menunjukkan bahwa dengan penggunaan alat penyuling uap modifikasi dapat menghasilkan rendemen yang lebih tinggi dan waktu proses yang lebih cepat dibandingkan dengan alat penyuling uap konvensional. Hasil analisis gas chomatography-mass spectrometry menunjukkan kandungan patchouli alcohol minyak nilam hasil penyulingan alat modifikasi sebesar 31,96%. Spektra hasil analisis Fourier Transform Infrared menunjukkan minyak nilam hasil penyulingan alat penyuling modifikasi dan konvensional memiliki gugus fungsi yang sama. Namun, warna minyak hasil penyulingan alat penyuling modifikasi lebih gelap dibandingkan alat penyuling konvensional. Hasil pengujian mutu minyak nilam menunjukkan warna, densitas, indeks bias dan putaran optik sudah memenuhi standar SNI No. 062385-1998.
Transesterifikasi Minyak Biji Buta-Buta menjadi Biodiesel pada Katalis Heterogen Kalsium Oksida (CaO) Zaki, Muhammad; Husin, M.T., Husni; Alam, Pocut Nurul; Darmadi, Darmadi; Rosnelly, Cut Meurah; Nurhazanah, Nurhazanah
Jurnal Rekayasa Kimia & Lingkungan Vol 14, No 1 (2019): Jurnal Rekayasa Kimia & Lingkungan (June, 2019)
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v14i1.13495

Abstract

Penelitian ini menggunakan katalis padat CaO untuk reaksi transesterifikasi minyak biji buta-buta menjadi biodiesel. Minyak biji buta-buta diekstraksi menggunakan alat press. Katalis CaO disiapkan dari cangkang kerang dengan cara dipijar pada suhu 850 oC. Sampel katalis dikarakterisasi dengan metode scanning electron microscopy (SEM) dan x-ray diffractometer (XRD). Katalis cangkang kerang memiliki ukuran partikel antara 200-2000 nm. Hal ini karena pemanasan cangkang pada 850 oC menyebabkan terjadi aglomerasi. Dari rekaman XRD teridentifikasi bahwa katalis didominasi oleh senyawa CaO dan terdapat sedikit CaCO3. Reaksi transesterifikasi dilangsungkan dalam reaktor batch dengan variasi suhu (55 oC, 60 oC, 65oC, dan 70oC), rasio metanol terhadap minyak: 3:1, 6:1, 9:1, 12:1, dan 15:1. Reaksi dilangsungkan selama 3 jam dan katalis didispersi 6 % berat dari minyak. Perolehan metil ester maksimum dicapai 96,7% pada kondisi reaksi, yaitu: molar metanol:minyak 12:1 dan suhu reaksi 65 oC. Karakteristik biodiesel hasil penelitian ini memenuhi sifat-sifat bahan bakar berkualitas tinggi sesuai dengan standar SNI dan ASTM. Proses transesterifikasi minyak biji buta-buta dan metanol menggunakan CaO sebagai katalis basa heterogen layak diaplikasikan secara komersial untuk produksi biodiesel dalam skala industri.
Optimization of the Condition of Palm Frond Torrefaction Process by Utilizing Liquid Torrefaction Product as Pre-treatment for Improve Product Quality Susanty, Wenny; Helwani, Zuchra; Bahruddin, Bahruddin
Jurnal Rekayasa Kimia & Lingkungan Vol 14, No 1 (2019): Jurnal Rekayasa Kimia & Lingkungan (June, 2019)
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v14i1.13443

Abstract

AbstractPalm frond can be converted to solid fuel using torrefaction process as an alternative energy source. Torrefaction is the process to convert the biomass into solid fuel at a temperature range of 200-300oC in inert condition. Calorific value is the most important response in solid fuel. The aim of this research is to obtain the optimum condition of palm fronds torrefaction statistically was used Response Surface Methodology. Torrefaction of palm frond on fixed bed a horizontal reactor which is equipped with horizontal condenser and condensate trap with the condition process such as the temperature (225-275oC), time (15-45 min), and N2 flow rate (50-150 ml/min). This research methodology consist of drying, washing with liquid product of torrefaction, torrefaction, and analysis. The response variables were mass yield, calorific value, energy yield, and proximate. Design Expert Trial Version 7.0 Software was used for optimization of condition process with desirability. The optimized condition process were temperature of 275oC, time of 44 minute, and N2 flow rate of 50 ml/min.Keywords: solid fuel, design expert, optimization, palm frond, torrefaction
Synthesis and Characterization of TiO2 Nanoparticle as Adsorbent on The Treatment of Methylene Blue Dye Pollutant Thahir, Ridhawati; Wahab, Abdul Wahid; Nafie, Nursiah La; Raya, Indah
Jurnal Rekayasa Kimia & Lingkungan Vol 14, No 1 (2019): Jurnal Rekayasa Kimia & Lingkungan (June, 2019)
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v14i1.13447

Abstract

The dye of methylene blue (MB) is organics pollutant from chemical industries. The parameter of MB content are available as methylene blue active substance (MBAS) do not exceed 200 g/L. The treatment of MB dye pollutant can be done by adsorption process with TiO2 nanoparticle. This aim of this research was synthesized of TiO2 nanoparticle using PVA as surfactant and titanium tetraisoproxide (TTIP) as titanium source through sol-gel preparation to hydrothermal process at temperature 400 and 600oC. The result of XRD spectrum was shown the tetragonal crystal, the phase of anatase, and the size of particle was 1.66 to 3.15 nm. Infrared spectroscopy of Ti-O functional group was at 467 cm-1 and there were hydroxyl groups of the surface TiO2. DSC analysis was indicated the thermal stability of TiO2 at 250oC. Application of TiO2 nanoparticle as an adsorbent to photodegradation of MB with Hg lamp 150 watt during 60 minutes. The highest of adsorption capacity at the sample TiO2-600 was 217 mg/g and effectiveness adsorption was 81%. Isoterm adsorption process of MB by TiO2 nanoparticle can be obtained with Langmuir and Freundlish equation, with the determined coefficient value were close to 1. These results suggest of TiO2 nanoparticle was indicated highly potential to apply for the treatment of pollutant industries.
Pengaruh Waktu Aging pada Sintesis Zeolit Linde Type-A (LTA) dari Zeolit Alam Lampung (ZAL) dengan Metode Step Change Temperature of Hydrothermal Ginting, Simparmin Br.; Arya Perdana, Guntur; Darmansyah, Darmansyah; Agustina Iryani, Dewi; Wardono, Herry
Jurnal Rekayasa Kimia & Lingkungan Vol 14, No 1 (2019): Jurnal Rekayasa Kimia & Lingkungan (June, 2019)
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v14i1.12093

Abstract

Zeolit Lynde Type-A (LTA) merupakan zeolit yang tergolong dalam kadar Si/Al rendah. Zeolit LTA memiliki berbagai kegunaan, antara lain sebagai adsorben, katalis, membran, penukar ion, maupun molecular sieve. Zeolit LTA sebagai molecular sieve memiliki kemampuan dehidrasi yang tinggi sehingga dapat digunakan untuk dehidrasi air pada campuran bioetanol-air agar diperoleh bioetanol yang sesuai dengan FGE (Fuel Grade Ethanol), yaitu kemurnian mencapai lebih besar dari 99%. Zeolit LTA dapat menyerap air di dalam bioetanol dikarenakan sifat Zeolit LTA yang hidrofilik. Penelitian ini mengkaji pengaruh waktu aging agar diperoleh persen kristalinitas relative zeolit LTA yang tinggi. Variasi waktu aging pada penelitian ini adalah 0 jam, 15 jam, 30 jam, dan 45 jam. Tahapan sintesis zeolit dilakukan pada sebuah water bath secara hidrotermal dengan metode step change temperature, yaitu pada suhu 90oC selama 1,5 jam dan 95oC selama 2,5 jam. Hasil sintesis dianalisis menggunakan SEM (Scanning Electron Microscopy), FTIR (Fourier Transmission Infra Red), BET (Brunaur, Emmet And Teller), dan XRD (X-Ray Diffracton). Berdasarkan analisis FTIR, hasil sintesis mempunyai ciri khas Zeolit LTA yaitu double rings pada bilangan gelombang 550-600 cm-1, persen kristalinitas relatif tertinggi yang didapatkan dari hasil analisis XRD adalah sebesar 66,15%, hasil analisis SEM menunjukkan morfologi Zeolit LTA berbentuk kubus, dan berdasarkan analisis BET didapatkan isotherm adsorpsi tipe ketiga.
Effect of Coagulants in Curd forming in Cheese Making Wardhani, Dyah Hesti; Jos, Bakti; Abdullah, Abdullah; Suherman, Suherman; Cahyono, Heri
Jurnal Rekayasa Kimia & Lingkungan Vol 13, No 2 (2018): Jurnal Rekayasa Kimia & Lingkungan (December, 2018)
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v13i2.12157

Abstract

Cheese is one of the popular dairy products with high nutrient content. Coagulation as an important process in making cheese, wherein, the curd will be separated from the milk whey. This coagulation can use the enzyme rennet, acid, or a combination of both. This study aims to study the effect of coagulant agents on yield, protease enzyme activity, and curd texture on cheese making. Coagulant agents used are acetic acid, citric acid, lime and lemon combined with the enzyme rennet. The process begins with pasteurized milk and analyzed, the milk is pasteurized and analyzed first to obtain moisture content, density and pH. The coagulant added is 25-45% with a base of 50 ml of milk and 5 mL of the enzyme rennet. The curd formed is then separated from the whey using a filter cloth and analyzed for its water content and pH. The coagulant of acetic acid and citric acid produced a higher yield curd of 94.66% (4% acetic acid) and 93.9% (5% citric acid) compared to the highest yield of curd that can be produced by lime and lemon coagulant which is 68 72% (lemon orange 45%) and 61.84% (lime 45%). The texture of the curd formed by lime and lemon juice is more fragile than the curd texture with coagulant of acetic acid and citric acid. Each coagulant provides a diverse response to protease enzyme activity.
Influence of Oil Content on Solution Load Ethanol-Soda Delignification of Oil Palm Mesocarp Fiber Taharuddin, Taharuddin; Iryani, Dewi Agustina; Eka Wahyu, Megananda
Jurnal Rekayasa Kimia & Lingkungan Vol 13, No 2 (2018): Jurnal Rekayasa Kimia & Lingkungan (December, 2018)
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v13i2.11145

Abstract

Mesocarp fiber palm oil industrial waste can be processed into pulp, but this fiber still contains oil with varying levels. The difference oil content in fiber affects the amount of cooking solution required to make mesocarp waste into pulp. This study consists of two stages, namely the pretreatment stage of oil extraction to obtain variations in oil content in the mesocarp fiber waste and the delignification stage using the NaOH-ethanol solution with the ratio of solids:solvent is varied to 1: 8, 1:10 and 1:12. Oil content of the fiber was analyzed, it is consist of 9,5% oil. To vary the oil content, the fibers are soaked in ethanol at room temperature and the levels drop to 7%. And soaking at 40C can lower the oil content drop to 2%. The obtained pulp had the largest cellulose content 50.77% from delignified product from fiber with 7.6% oil content and solids:solvent ratio: 1:10. While the lowest lignin that was 7.39% obtained at 2.5% oil content. In the delignification process with ratio 1:12, pulp produced is decreased in cellulose content and from FTIR results it is known that it occurs because of the degraded cellulose during the delignification process.
Adsorpsi Methyl Violet oleh Karbon Aktif dari Limbah Tempurung Kelapa dengan Aktivator ZnCl2 Menggunakan Pemanasan Gelombang Mikro Astuti, Widi; Dwi Handayani, Anggelita; Wulandari, Diah Ayu
Jurnal Rekayasa Kimia & Lingkungan Vol 13, No 2 (2018): Jurnal Rekayasa Kimia & Lingkungan (December, 2018)
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v13i2.11945

Abstract

Synthesis of activated carbon from coconut shell waste with ZnCl2 activation using microwave heating have been carried out. Coconut shell consists of 36.51% lignin, 33.61% cellulose and 19.27% hemicellulose which causes it can be used as a precursor in the synthesis of activated carbon. The activated carbon was further characterized using Scanning Electron Microscope (SEM), Fourier Transform Infrared Spectrophotometer (FTIR) and NOVA Gas Sorption Analyzer-Quantachrome and used for the adsorption of methyl violet in aqueous solution with variation of pH, contact time and concentration of solution. The result showed that the pore of activated carbon was larger than that of the char. The optimum adsorption occurred at pH 3 and the equilibrium time was reached after 180 minutes. The Langmuir equilibrium model was more appropriate than the Freundlich equilibrium model. While the kinetics model analyzed using pseudo first order, pseudo second order, internal diffusion and external diffusion indicated that the pseudo second order was most suitable for the adsorption of methyl violet by coconut shell activated carbon.

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