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All Journal International Journal of Renewable Energy Development Jurnal AGROTEKNOLOGI Jurnal Ilmu Dasar BERKALA SAINSTEK Pelita Perkebunan Bulletin of Chemical Reaction Engineering & Catalysis Alchemy Jurnal Penelitian Kimia Jurnal Kimia Mulawarman UNEJ e-Proceeding Jurnal Kimia Riset Jurnal Pemberdayaan Masyarakat Madani (JPMM) ALCHEMY Jurnal Penelitian Kimia J-Dinamika: Jurnal Pengabdian Kepada Masyarakat Jurnal Abdi: Media Pengabdian Kepada Masyarakat Computational and Experimental Research in Materials and Renewable Energy (CERiMRE) Indonesian Chimica Letters Warta LPM Molekul: Jurnal Ilmiah Kimia International Journal of Renewable Energy Development Engagement: Jurnal Pengabdian Kepada Masyarakat al Kimiya : Jurnal Ilmu Kimia dan Terapan
Bambang Piluharto
Jurusan Kimia, Fakultas Matematika Dan Ilmu Pengetahuan Alam, Universitas Jember
Religion Agriculture, Biological Sciences & Forestry Arts Humanities Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Control & Systems Engineering Earth & Planetary Sciences Economics, Econometrics & Finance Education Electrical & Electronics Engineering Energy Engineering Environmental Science Health Professions Languange, Linguistic, Communication & Media Materials Science & Nanotechnology Mathematics Physics Social Sciences Other

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Effect of Addition of Monosodium Glutamate (MSG) on Coagulation Basin to Characteristics of Cellulose Acetate Membranes Rofiqoh, Siti; Indarti, Dwi; Piluharto, Bambang
Jurnal ILMU DASAR Vol 17 No 2 (2016)
Publisher : Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (252.307 KB) | DOI: 10.19184/jid.v17i2.2687

Abstract

The aim of recearch is study the effect of MSG in coagulation basin on cellulose acetat membranes properties. It was preparated by phase inversion technique. As the result showed that the higher the concentration of MSG in coagulation basin, which is character of membrane permeability coefficients and lower water flux. Dextran rejection of 11, 40, 100-200, and 500 kDa increased. The morphology analysis has shown that sub layer membranes structure with 2% MSG addition more uniform than 0,5% MSG addition.Keywords: cellulose acetat, phase inversion, MSG, coagulation basin
Synthesis and Characterization of Bacterial Cellulose-Polyaniline Composite with Variation of Dopant Concentration Ummami, Riza; Busroni, Busroni; Piluharto, Bambang
BERKALA SAINSTEK Vol 9 No 2 (2021)
Publisher : Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/bst.v9i2.18120

Abstract

Polyaniline is a type of conductive polymer. Bacterial cellulose has high mechanical properties, so it can be made into polyaniline base composite materials. A stable form of polyaniline oxidation at room temperature is emeraldine base. The emeraldine base has a conductivity value of 10-6 S/cm. Dopants can change the shape of emeraldine base to emeraldine salt by protonation process. Emeraldine salt is a conductive form of polyaniline. The conductivity value of emeraldine salt is 0,03-0,07 S/cm. The addition of dopan in synthesis of polymer was carried out to determine its effect on the conductivity value. The disadvantage of polyaniline is that its mechanical properties are weak and easily brittle. Modifications are needed to improve the mechanical properties of polyaniline, one of which is the manufacture of composite. Bacterial celluloce has high mechanical properties so it can be made into polyaniline base composite materials. Synthesis of bacterial cellulose-polyaniline composites by in situ chemical polymerization methods. Syntehsis is started with BC membrane was dipped into aniline solution for about 2h with stirring at room temperature. The BC was immersed into ammonium peroxydisulfate solution for about 30m with stirring. The bacterial cellulose-polyaniline compositions obtained are black color which is characteristic of the emeraldine salt. The highest conductivity value of composite was obtained from the addition of 3,5M HCl dopant which was 4,70x10-4 S/cm. FTIR analysis of composite obtained peak of the characteristic polyanilin was conductive at 1565,92 cm-1 as C=C quinoid ring and 1442,95 cm-1 as C=C benzoid ring.
Performance of cotton fabric treated with chitosan-based mordanty as affected by extraction time variations on tannin dyes produced from cocoa husk Fatwa, Muhammad Iqbal; Firmanto, Hendy; Indarti, Dwi; Piluharto, Bambang; Sulistyo, Yudi Aris; Reza, Muhammad; Ula, Mohammad Munal; Dharmawan, Aditya Dwiki
Pelita Perkebunan (a Coffee and Cocoa Research Journal) Vol. 40 No. 1 (2024)
Publisher : Indonesian Coffee and Cocoa Research Institute

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22302/iccri.jur.pelitaperkebunan.v40i1.584

Abstract

Natural dyes are substances obtained from animals or plants through extraction. The application of synthetic dyes can affect to environmental problems, therefore replace it with natural dyes is become an alternative. Cocoa pod husk still considered as a waste, whereas it is one of source for natural dyes. Cacao pod husk contains flavonoids, tannins, and β-carotene compounds which is generate colour. Natural dye is extracted from the husk of the cocoa pod and applied to cotton cloth. Extraction of cocoa husk dyes was carried out with distilled water at 60˚C with variations of 1, 2, and 3 hours. The resulting extract contains positive tannins but negative β-carotene. Variations in the extraction time of natural dyes affect the tannin content extracted. The tannin content extracted with variations of 1, 2, and 3 hours was 18.32; 18.67; and 17.93 ppm. Respectively chitosan-based mordant has a significant effect on the color yield of the fabric. Fabrics with mordant have a darker color than fabrics that are not applied with mordant process. The use of nanochitosan and citric acid crosslinkers can maintain the aging color of the fabric. The FTIR results on the fabric showed that color aging occurred due to the presence of ester groups formed between chitosan and dyes. Chitosan-based mordant coating provides better color than without mordant coating. Fabrics coated with chitosan had the best fastness value of 4 (Good).
The Production of Solid and Liquid Organic Fertilizers From Cow and Goat Manure and Their Application to Corn Crops Roziq, Ahmad; Shulthoni, Moch.; Piluharto, Bambang; Afif Difa Asy Syafiq, Muhammad; Ilma Ahmad, Zakiyyah
Engagement: Jurnal Pengabdian Kepada Masyarakat Vol 8 No 2 (2024): November 2024
Publisher : Asosiasi Dosen Pengembang Masyarajat (ADPEMAS) Forum Komunikasi Dosen Peneliti

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29062/engagement.v8i2.1915

Abstract

Bangsri is a village in the Plandaan Sub-district, Jombang Regency, East Java Province, where most residents live as farmers. In Bangsri, several farmers and breeders have over 500 goats and sheep. However, they face challenges in processing goat manure into solid and liquid organic fertilizers that would be more beneficial for plants. Currently, goat farmers lack the innovation to process the manure, often just piling it up or discarding it. Additionally, the sharecropping system in agriculture is becoming increasingly unprofitable, and crop yields are suboptimal, particularly during the dry season, due to high processing costs. As a result, many rice fields are abandoned by their owners. The way to overcome this problem is through a service-learning approach. In service activities, the team provides training and assistance in making organic fertilizer to provide added value for farmers and breeders. As a result, farmers and breeders have started implementing the techniques learned in the training to produce both solid and liquid organic fertilizers. This initiative has been positively received in Bangsri Village, with noticeable improvements in crop yields
Synthesis and Characterization of Glutaraldehyde-Crosslinked Chitosan for Urea Controlled Release Piluharto, Bambang; Indarti, Dwi; Handoko, Donatus Setyawan Purwo; Ananda, Tinok Dwi
Indonesian Chimica Letters Vol. 3 No. 2 (2024)
Publisher : Department of Chemistry, Faculty of Mathematics and Natural Sciences, University of Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/icl.v3i2.4325

Abstract

Urea exhibits high nitrogen content (∼46%), which is essential for plant growth. However, significant nitrogen losses occur through decomposition, leaching, denitrification, and volatilization. Employing controlled-release systems, such as chitosan membranes crosslinked with glutaraldehyde, can mitigate these losses and enhance fertilizer efficiency. Therefore, this study aimed to develop and characterize chitosan-glutaraldehyde membranes as controlled-release fertilizer systems for urea. Chitosan membranes were crosslinked with varying glutaraldehyde concentrations (0%, 0.4%, 0.9%, 1.3%, and 1.8%) and used to encapsulate urea. The membrane produced was characterized using FTIR and swelling degree assay. The potency of glutaraldehyde-crosslinked chitosan as a urea coating agent was also studied spectrophotometrically using the Nessler reagent. FTIR analysis revealed low intensity of the C=N stretching vibration, indicating limited crosslinking reaction. Additionally, both swelling degree and urea release increased proportionally with increasing glutaraldehyde concentration. These findings suggest limited crosslinking reactions occurred between glutaraldehyde and chitosan within the studied concentration range.
PENGEMBANGAN DAN PEMBERDAYAAN INDUSTRI RUMAH TANGGA (IRT) JAMUR TIRAM DI DESA PONTANG, KECAMATAN AMBULU, KABUPATEN JEMBER Piluharto, Bambang; Ubaidillah, Firdaus; Triono, Agus
Jurnal ABDI: Media Pengabdian Kepada Masyarakat Vol. 10 No. 2 (2025): JURNAL ABDI : Media Pengabdian Kepada masyarakat
Publisher : Universitas Negeri Surabaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26740/abdi.v10i2.31765

Abstract

Home industry Oyster Mushroom “Kayla” which is located in Dusun Tengan RT 47 RW 12 Pontang Village, Ambulu District, Jember Regency is a business unit that produces oyster mushrooms. This home industry’s production capacity is 5 kgs of mushrooms per day, with the main consumers being melijo traders and the sorrounding community. The demand for mushrooms from customers is often not met due to limited production capacity. Mushroom baglog as a growth medium is an important component in mushroom production. So far, Mushroom baglogs have been suplied from self-made baglogs and purchased from other parties. Self-made baglogs was produced manually by hand. This is inefficient, besides purchasing baglog from other parties also increases production costs. This activity aims to provide training and assistance to partners, namely the oyster mushroom home industry “Kayla” as a form of training in production of mushroom baglog using the baglog press technique along with digital marketing technique. To achieve this goal, the methods used include training and assistance to activity partners. From the results obtained, the activity partners were independently able to carry out production using the baglog press technique. Apart from that, digital marketing development using social media has been carried out to market mushroom products. The impact obtained from this activity is an increase in the number of baglog obtained, thereby increasing mushroom production capacity to around 10 kgs/day. In the future, skill development and economic empowerment of activity partners can be continued with an emphasis on training on mushroom – based product diversification.
Effect of Molecular Weight of Chitosan in The Coating Solutions on The Shelf Life of Tuna Fish Fillets Indarti, Dwi; Khofifah, Marhamatul; Piluharto, Bambang; Ananda, Tinok Dwi
al Kimiya: Jurnal Ilmu Kimia dan Terapan Vol. 12 No. 1 (2025): June 2025
Publisher : Department of Chemistry, Faculty of Science and Technology, UIN Sunan Gunung Djati Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.15575/ak.v12i1.44715

Abstract

Tuna, a valuable Indonesian marine commodity, is known for its highly valued dietary and nutritional sources. However, this red meat fish is particularly prone to deterioration and spoilage due to its inherent properties. Liquid smoking, a popular fish preservation method in Indonesia, has garnered significant consumer interest but remains insufficient to prevent fish decay entirely. Therefore, this study aimed to enhance tuna fish fillet (TFF) shelf life by developing a novel coating solution. This solution contains liquid smoke seasoning and chitosan with varying molecular weights (MW), as this property affects chitosan’s chemical, physical, and biological characteristics. In this research, fresh tuna were divided into four groups: a control group with no coating, a group with liquid smoke coating only (LS), a group coated using chitosan solution (Ch) with variations of MW (Low: 50-190 kDa, Medium: 190-310 kDa, and High: 210-375 kDa), and a group coated using liquid smoke seasoning with the same chitosan MW variation (Ch + LS). During 15 days of storage in the freezer, their chemical properties (pH, and Total Volatile Base Nitrogen - TVB-N) were analyzed. The finding showed that combining high MW of chitosan and liquid smoke as a coating solution improved TFF appearance, maintaining a desirable uniformly cherry red color. Moreover, this treatment showed a slower increase in pH (5.5 – 5.7) and TVB-N level (22 – 28 mg TVB-N/100 gram), indicating deterioration and spoilage delay during 15 days of storage compared to other treatments. This study underscores the efficacy of a preservation strategy in inhibiting deterioration and spoilage in tuna fish fillets during storage, thereby enhancing product quality and ensuring consumer safety.
Immobilization of Endo-Β-1,4-D-Xylanase using Alginate/Nanocellulose for Xylooligosaccharide Production Ratnadewi, Anak Agung Istri; Aprilia, Selvina Rizky; Piluharto, Bambang; Yulvia, Ana
Indonesian Chimica Letters Vol. 2 No. 2 (2023)
Publisher : Department of Chemistry, Faculty of Mathematics and Natural Sciences, University of Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/icl.v2i2.5607

Abstract

Free endo-β-1,4-D-xylanase cannot be used more than once, so it needs to be modified by immobilizing the enzyme. Endo-β-1,4-D-xylanase was obtained from termite abdomen sources by isolation, ammonium sulfate purification, and dialysis methods. Endo-β-1,4-D-xylanase was immobilized with an alginate/nanocellulose matrix. This study aims to determine the activity, protein content, and repeated use of immobilized Endo-β-1,4-D-xylanase. This study used variations of Alginate/nanocellulose (0; 2.5; 5; 7.5; 10) %. Protein levels of Endo-β-1,4-D-xylanase were tested using the Bradford method and activity using the Miller method. The total protein bound to the immobilized Endo-β-1,4-D-xylanase was stated with the immobilized yield data. The immobilized yield with the composition of Alginate Nanocellulose (ANC) (0%) was 45.33% greater than the other compositions. Immobilized Endo-β-1,4-D-xylanase activity is efficient. ANC 5% produces an efficiency of 62.384% at the 12th hour, which is greater than the other ANC compositions.
The Influence of Cellulose Acetate Concentration for Ultrafiltration Membranes Apriliasari, Yekti; Indarti, Dwi; Oktavianawati, Ika; Piluharto, Bambang
Indonesian Chimica Letters Vol. 2 No. 2 (2023)
Publisher : Department of Chemistry, Faculty of Mathematics and Natural Sciences, University of Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/icl.v2i2.5618

Abstract

Separation process using a membrane is a common method used in many fields. The objective of this research is to find out the influence of polymer concentration on the physical properties and performance of cellulose acetate as an ultrafiltration membrane. The cellulose acetate membrane is made by phase inversion technique. This technique is carried at by dissolving cellulose acetate in a range of concentration (18%, 19%, 20%, 21%, and 22%) in the solvent (acetone/DMSO = 15%/60%) and DMP as additives (3% mL). Then the mixtures homogenized and added PEG400 for 10% of cellulose acetate concentration (% w/w), strired ± 12 hours left in place until the buble disappeared. Then the dope solution is printed the glass plate, evaporated for 3 minutes, and immersed in a coagulation bath containing 5% acetone. The results suggest that the greater the concentration of cellulose acetate membrane increase the number density while the swelling degree decrease. The performance of the membrane showed that the greater concentration of cellulose acetate will water of flux the membrane decrease and rejection coefficient increase. Cellulose acetate membrane by varying the concentration of 21% and 22% included in the classification of ultrafiltration membranes for rejection coefficient value (90,37% and 91,43%) 90% may rejection by a membrane.
Co-Authors A Sjaifullah Abdulloh Abdulloh Achmad Sjaifullah Achmad Subagio Achmad Subagio Afif Difa Asy Syafiq, Muhammad Agus Triono Agus Wedi Pratama Ahmad Roziq Ahmad, Zakiyyah Ilma Anak Agung Istri Ratnadewi Ancah Caesarina Novi Marchianti Anggia Rose Sukaton Aprilia, Selvina Rizky Apriliasari, Yekti Asnawati Asnawati Asnawati Bayu Rudiyanto Busroni, Busroni Dafit Ari Prasetyo Deltaningtyas Tri Cahyaningrum Dharmawan, Aditya Dwiki Djamali, R. Abdoel Dwi Indarti Dwi Jayanti, Denik Dwi Kusuma Wahyuni Dwiyanti, Inayatus Nur Erix Nurharianto Fatwa, Muhammad Iqbal Firdaus Ubaidillah, Firdaus Firmanto, Hendy HARDIAN SUSILO ADDY Henry Adi Syahputra Sidabutar Hermanto, Toto I Rahmawati Ika Oktavianawati Imam Syafi’i Indarto Indarto Indarto Indarto Intan Rida Agustina Irsyam, Mahrus Istiqomah Rahmawati Iswahyono Iswahyono Karisma Wulan Ningtyas Khofifah, Marhamatul Lulus Kartika Ningtias Mahrus Irsyam Maryanto - Maryanto Maryanto Miftah Hijriawan Moch. Shulthoni, Moch. Mufrihah Nurhayati Muhammad Reza Naning Retnowati Nida Andriana Nur Aisyah Nurud Diniyah Purkan Purkan, Purkan Purwo Handoko, Donatus Setyawan R. Abdoel Djamali R. Indahsari Riska Rian Fauziah S. Purwo Handoko, Donatus Siswoyo Siswoyo Siti Rofiqoh, Siti Sofijan Hadi Sri Sumarsih Sudarko, S. Sulistyo, Yudi Aris Sulistyowati, Fitri Syahbanu, Intan Syahrul Khairi Tanti Haryati Tinok Dwi Ananda Totok Prasetyo Ula, Mohammad Munal Ummami, Riza Wulandari, Melysa Wuryanti Handayani Yudi Aris Sulistiyo, Yudi Aris Yulvia, Ana Zeni Ulma Zulfikar Zulfikar