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All Journal Prosiding Seminar Nasional MIPA Alchemy : Journal of Chemistry Biota: Jurnal Ilmiah Ilmu-Ilmu Hayati Indonesian Journal of Mathematics and Natural Sciences Natural B Jurnal Kimia Riset Science and Technology Indonesia BIOEDUKASI Agrotekma: Jurnal Agroteknologi dan Ilmu Pertanian Jurnal Saintek Lahan Kering Jurnal Kreativitas PKM Jurnal Inovasi Teknik Kimia Jurnal Abdi Insani Sciscitatio : Journal for Biological Science Indigenous Biologi Ainara Journal (Jurnal Penelitian dan PKM Bidang Ilmu Pendidikan) Jurnal Dedikasi J.Abdimas: Community Health BERBAKTI: Jurnal Pengabdian Kepada Masyarakat Jurnal Penelitian Hasil Hutan Jurnal Ilmiah Teknologi Pertanian Agrotechno
Merpiseldin Nitsae
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Journal : Alchemy : Journal of Chemistry

 1 
Perbandingan Butiran Kitosan dengan Pengikat Silang Epiklorohidrin (ECH) dan Glutaraldehid (GLA): Karakterisasi dan Kemampuan Adsorpsi Timbal (Pb) Armeida Dwi Ridhowati Madjid; Merpiseldin Nitsae; Akhmad Sabarudin
ALCHEMY:Journal of Chemistry Vol 6, No 1 (2018): ALCHEMY: JOURNAL OF CHEMISTRY
Publisher : Department of Chemistry, Faculty of Science and Technology UIN Maulana Malik Ibrahim Malan

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (758.544 KB) | DOI: 10.18860/al.v6i1.6790

Abstract

Chitosan was an abundantly available source but it has a drawback which unstable in acid or base. So, it must be added with a crosslinker. In this article, we would compare the using of 2 crosslinkers, glutaraldehyde (GLA) and epichlorohydrin (ECH). Chitosan was formed as bead using tripolyphosphate (TPP). Chitosan beads crosslinked with GLA became browny beads and chitosan beads crosslinked with ECH became pearly white. IR characterization showed peaks in 1640 and 1540 cm-1 represent phosphate contained TPP. There is no significant or unique peak differ GLA chitosan bead from ECH chitosan bead. Adsorption capacity of lead (Pb) in ECH chitosan bead was higher than in GLA chitosan bead. Morphology in SEM characterization exhibited a crinkle GLA chitosan bead then ECH chitosan bead. Kitosan merupakan polimer alam dengan ketersediaan yang meruah tetapi memiliki kelemahan yaitu kurang stabil dalam asam maupun basa sehingga diperlukan pengikat silang. Dalam artikel ini akan dibandingkan dengan penggunaan 2 agen pengikatsilang yang dapat mengatasi permasalahan tersebut yaitu epiklorohidrin (ECH) dan glutaraldehid (GLA). Untuk pembuatan butiran kitosan digunakan tripolyphosphate (TPP). Setelah menjadi butiran kitosan diikatsilangkan dengan GLA menjadi butiran kitosan yang berwarna kecoklatan dan diikatsilangkan dengan ECH menjadi butiran kitosan bening. Karakterisasi spektrofotometri Infra Merah menunjukkan puncak pada daerah 1640 dan 1540 cm-1 yang merupakan serapan khas dari tripolyphospate sedangkan tidak nampak perbedaan puncak spektra yang signifikan dari butiran kitosan GLA maupun ECH. Kemampuan adsorpsi butiran logam timbal (Pb) butiran kitosan ECH lebih tinggi jika dibandingkan dengan butiran kitosan GLA. Morfologi butiran kitosan dianalisis menggunakan Scanning Electron Morphology (SEM) dan menunjukkan bahwa morfologi untuk butiran GLA memiliki morfologi yang lebih berkerut jika dibandingkan dengan butiran ECH.
Co-Authors Adri Gabriel Sooai Akhmad Sabarudin Akhmad Sabarudin Aloisius M. Kopon Aloisius Masan Kopon Alwan M. Ninef Ambrosius Faofeto Ame, Joni Alvonsius Amelia M Salmon Anselmus Boy Baunsele Armeida D. R. Madjid Armeida Dwi Ridhowati Madjid Arnold Ch. Hendrik arnold christian hendrik Banu, Erik Sandy Blegur, Willem Amu Daud E. Adu Daud, Yanti Dwi Siswanta Egertha Karpada Arsun Banamtuan Mellissa E. S. Ledo Elsita Rambu Kahi Erly Grizca Boelan eunike puteri ate Hariyati Lubis, Hariyati Hartini R.L. Solle Henderina Mowata Hendrik, Gersandi Hildegardis Missa Imanuel Jacob Emola Irma, Mutia James Ngginak Joenrith Agrid Kana, Belandina Here Kii, Arniati Ina Koehuan, Jonathan Ebet Lano, Lans Asideo Lans Asideo Lano Ledo, M E S Ledo, Mellisa E.S. Ledo, Mellissa Erlyn Stephanie Lenciani Seran Lolonrian, Patrisia Marfiana Dae Lukman Hakim M Nitsae, M Maria A. U. Leba Maria Aloisia Uron Leba Medah, Andreas Isakh melkianus mola kore Mellissa E. S. Ledo, Egertha Karpada Arsun Banamtuan mellissa e.s ledo Mesri Welhelmina Nisriani Manafe Nomleni, Fransina T Perdinan Sinuhaji Philiphi de Rozari Philiphi de Rozari Pius Dore Ola Rafly Ihsan As Siddiq, Muhammad Rahayu Rahayu Rahayu Realista Lydia Solle, Hartini Redo, Irmina Rinaldi, Fajar Rony S. Mauboy Rupidara, Anggreini D.N Sabuna, Alan Ch. Serliani M. Martinus Soleman Sayuna Solissa, Arfie Solle, Hartini Realista Lidya Solvina Tanggu Sana Sonya Titin M. Nge Sonya Titin Marlina Nge Sonya Titin Nge Sooai, Adry Gabriel Susilawati Tini Margarita Talan Toulasik, Yulita Wempi Silla Wora, Theresia Wea Yoaclina D. Ninu Yulita Iryani Mamulak