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All Journal Prosiding Semnastek Alchemy Jurnal Penelitian Kimia Metalurgi Journal of Comprehensive Science Indonesian Research Journal on Education Metalurgi Journal of Social Science and Education Research
Eko Sulistiyono, Eko
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Journal : Metalurgi

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The Effect of pH and Sodium Silicate Dosage on the Separation of Magnesium and Lithium from Artificial Brine Water Using Chemical Precipitation Techniques Lalasari, Latifa Hanum; Sulistiyono, Eko; Harjanto, Sri; Irawan, Januar; Firdiyono, Florentinus; Arini, Tri; Andriyah, Lia; Suharyanto, Ariyo; Natasha, Nadia Chrisayu; Yunita, Fariza Eka
Metalurgi Vol 38, No 3 (2023): Metalurgi Vol. 38 No. 3 2023
Publisher : National Research and Innovation Agency (BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/metalurgi.2023.728

Abstract

This study aims to report the findings of an investigation into the separation of lithium and magnesium ions in the artificial brine water. The artificial brine water contains concentrations of magnesium, calcium, and lithium cations that closely resemble the concentrations seen in natural brine water sourced from Gunung Panjang using magnesium chloride, calcium chloride, and lithium chloride p.a. The objective of this experiment was to investigate the impact of pH and the addition of sodium silicate on the separation of magnesium and calcium ions from lithium ions in artificial brine water. The best outcomes were achieved when the pH of the brine water was set at 10, and sodium silicate was added in a stoichiometric ratio of 219%. These parameters led to a lithium content of 90.06%, magnesium removal of  70.32%, and a Mg/Li ratio of 6.29, indicating a substantial presence of magnesium ions precipitated as solids with pyroxene (MgSiO3) phase. This research also succeeded in increasing the lithium content by 94.28% and reducing the Mg/Li ratio to 4.96 after the precipitated solids were subjected to a water-leaching process.
Study of Iron and Calcium Removal on Manganese Sulfate Precursors for Battery Cathode Raw Material Applications Hakim, Agsel Fauzia; Andriyah, Lia; Oediyani, Soesaptri; Lalasari, Latifa Hanum; Sulistiyono, Eko; Irawan, Januar; Arini, Tri; Yunita, Fariza Eka; Suharyanto, Ariyo; Setiawan, Iwan; Firdiyono, Florentinus; Yuwono, Akhmad Herman
Metalurgi Vol 39, No 2 (2024): Metalurgi Vol. 39 No. 2 2024
Publisher : National Research and Innovation Agency (BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/metalurgi.2024.753

Abstract

Global battery sales are expected to reach $310.8 billion in 2027, up 14.1% from 2020. 95% of the world's batteries are lead-acid, lithium-ion, or nickel-based. One of the most popular batteries on the global market is lithium-ion, which uses MnSO4 powder as its cathode raw material. Manganese sulfate-based lithium-ion batteries can be made using Indonesian resources, specifically manganese ore from Trenggalek. Trenggalek manganese ore is of poor quality and contains impurities, primarily Fe and Ca. To produce 98% powder manganese sulfate, the solution is prepared, reduced with briquette charcoal, leached, precipitated, carbonated, and crystallised. NH4OH reagent is used to remove Fe through precipitation, and the carbonatation process is employed to eliminate Ca, resulting in 97.237% purity of manganese sulfate powder product. This outcome is achieved under precipitation process conditions of [NH4OH 2M], T = 80 °C, pH = 4, t =180 minutes, while carbonatation process conditions are T=50 °C, t = 120 minutes.
Co-Authors A.A. Ketut Agung Cahyawan W Adlan Nawawi, Muhammad Ahmad Jawandi Akhmad Herman Yuwono Andriyah, Lia Antoro, Iwan Dwi Ari Handono Ramelan Azwar Manaf Edi Pramono Faqih, Mustofa firdiyono, F Firdiyono, Felix Florentinus Firdiyono Hakim, Agsel Fauzia Hari Hidayatullah, Hari Irawan, Januar Iwan Setiawan Lalasari, Latifa Hanum Natasha, Nadia Chrisayu Saifuddin Zuhri Sayekti Wahyuningsih Sentot Budi Rahardjo Sholikhah, Linda Dwi Sisno Riyoko Soesaptri Oediyani Sri Harjanto Suharyanto, Ariyo Suharyanto, Ariyo Tri Arini, Tri Yunita, Fariza Eka