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All Journal Rotasi CHEMICA Jurnal Teknik Kimia Rekayasa Mesin Sinergi Jurnal Teknik Sipil Jurnal Teknik Mesin Turbo : Jurnal Program Studi Teknik Mesin Indonesian Journal of Chemistry Jurnal Pendidikan dan Konseling International Journal of Advanced Technology in Mechanical, Mechatronics and Material (IJATEC) International Journal of Community Service Jurnal Rekayasa Energi dan Mekanika JOURNAL OF CHEMICAL NATURAL RESOURCES (JCNaR) International Journal of Innovation in Mechanical Engineering and Advanced Materials Journal Of Carbazon
Sagir Alva
Universitas Mercu Buana
Religion Aerospace Engineering Humanities Automotive Engineering Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Civil Engineering, Building, Construction & Architecture Control & Systems Engineering Education Electrical & Electronics Engineering Energy Engineering Environmental Science Industrial & Manufacturing Engineering Languange, Linguistic, Communication & Media Law, Crime, Criminology & Criminal Justice Library & Information Science Materials Science & Nanotechnology Mathematics Mechanical Engineering Public Health Social Sciences Other

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Journal : Sinergi

 1 
CHLORIDE SENSOR FABRICATION BASED ON SPE Ag/AgCl THROUGH CYCLIC VOLTAMMETRIC TECHNIQUE: SCAN RATE EFFECT Mas'ud Asadullah; Sagir Alva; Ali Rinaldi; Rita Sundari
SINERGI Vol 25, No 3 (2021)
Publisher : Universitas Mercu Buana

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22441/sinergi.2021.3.012

Abstract

The Cyclic Voltammetric (CV) technique is one of the Ag/AgCl fabrication processes. In electrochemical processes using this CV technique, the microstructure of the surface of a substrate or electrode can affect the scan rate. Thus, this study aims to identify the scan rate effect of the Cl-ion sensor fabrication process using the CV technique on the performance of the Cl-ion sensor. First, the CV process was carried out in one cycle to grow the AgCl layer on the Ag surface. Then, this process was carried out at varied scan rates of 20, 40, 60, 80, and 100 mV/s. After completing the Ag/AgCl fabrication process, it was followed by the characterization process, selectivity coefficient test, lifetime test, and validation test to compare the test results of the Cl SPE Ag/AgCl ion sensor with Ag/AgCl commercial. The results showed that the optimum Cl-ion sensor response was obtained at the scan rate of 60 mV/s. Then, based on the validation test, the Cl-ion in the two samples did not show significant differences. Therefore, it indicates that the SPE Ag/AgCl ion sensor has the same performance as the Ag/AgCl commercial.
TIRE WASTE AS A POTENTIAL MATERIAL FOR CARBON ELECTRODE FABRICATION: A REVIEW Ahmad Ariri; Sagir Alva; Siti Aishah Hasbullah
SINERGI Vol 25, No 1 (2021)
Publisher : Universitas Mercu Buana

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22441/sinergi.2021.1.001

Abstract

Nowadays, tire waste is a big issue since the rapid growth of vehicle population worldwide. The disposal of tire waste should be done properly due to the environmental impact caused by stockpile the tire waste in landfill.  Many kinds of research had been conducted to dispose of tire waste efficiently for getting valuable material from tire waste by using pyrolysis technology; one of them is carbon. In this review paper, production and application of carbon from tire waste presented. In several studies, carbon derived from tire waste was used as an adsorbent, electrode in energy storage application, like batteries and fuel cell.
Fabrication of mercury (Hg) sensor based on Tire Waste (TW) carbon electrode and voltammetry technique Baihaqi Baihaqi; Khairi Suhud; Sagir Alva; Eka Safitri; Julinawati Julinawati; Binawati Ginting; Syafrizal Fonna; Ahmad Kamal Arifin; Zulnazri Zulnazri; Nurul Islami
SINERGI Vol 27, No 3 (2023)
Publisher : Universitas Mercu Buana

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22441/sinergi.2023.3.012

Abstract

Voltammetry is widely used to detect heavy metals such as mercury (Hg). The sensor material influences the results of the voltammetry method. Carbon-based sensors are commonly developed because of their wide potential range, low background current, inexpensive, inert, and suitable for various sensors. Recently, Tire Waste (TW) was chosen as a carbon source for the manufacture of electrodes because it is rich in carbon (88%). The material is easy to obtain, green technology and a carbon source that has not been properly utilized. Separation of carbon material from TW using the pyrolysis method produces 4.32 gr (2.6%) of soot (from 200 gr TW) as a material for making carbon-based Hg sensors. The XRD pattern of TW soot has amorphous phases. SEM topography shows that the surface of TW soot consists of particles that are almost uniform in shape. The estimated particle size is about 0.25 µm. The sensor was made with a mixture of TW soot and paraffin with a 2:1 ratio. Testing the specific value of sensor capacitance using the Cyclic Voltammetry (CV) method showed the presence of cathodic and anodic currents. The Hg deposit occurred at a peak cathodic current at a scan rate of 20 mV/s. The Limit of Detection (LoD) value is 0.0681 ppm and the Limit of Quantitation (LoQ) is 0.229 ppm. Measurement of Hg in natural water samples used river water from the Aceh Jaya sub-district at two points representing the upstream and downstream of the river. The Hg concentrations obtained were 0.000536 ppm and 0.00182 ppm, respectively and were compared with the inspection results using Atomic Absorbance Spectroscopy (AAS), 0.00058 ppm and 0.00186 ppm, respectively. The t-test results of the two Hg measurement methods at a significance level (α) of 5% obtained tcount > ttable (0.0208 <2.306), indicating that there is a significant difference between the two Hg concentration measurement methods for natural water.
Co-Authors Adelfy Dara Arianti Agnes Hanna Patty, Armin Naibaho, Singgih Fitra Utama, Ahmad Ariri Ahmad Kamal Arifin Aiman Sajidah Abd Aziz Aiman Sajidah binti Abdul Aziz Albert Phak Jie Wong Ali Rinaldi Andi Firdaus Sudarma Arianti, Adelfy Dara Arifin, Ahmad Kamal Ariri, Ahmad Asadullah, Mas'ud Asadullah, Masud Asep Setia Kristanto Ayu Arwati, I G. Baihaqi Baihaqi Basyari, Aziz Binawati Ginting Dafit Feriyanto Dayanti, Meri Deni Shidqi Khaerudini Edy Herianto Majlan Eka Safitri Eka Safitri Elin Yusibani Elly Sufriadi Fadhilla, Eky Nur Fidi Fidi Fidi, Fidi Fitri , Muhammad Fitri Dara Fonna, Syafrizal Friliandita, Vivi G. Ayu Arwati, I Ginting, Dianta Hadi Pranoto Hadi Pranoto Hasbullah, Siti Aishah I Gusti Ayu Arwati Ibdal Satar Indradewa, Rhian Iqhrammullah, Muhammad Julinawati Julinawati Julinawati, Julinawati Khairi Suhud KHAIRI SUHUD Kurniawan Kurniawan Leni Heliawati Marysca Shintya Dewi Mas&#039;ud Asadullah Mohd Ismahadi bin Syono Muhammad Farhan Muhammad Fitri, Muhammad Muhammad Ihsan Muhammad Isa Mustanir Mustanir Nanang Ruhyat Noviyanto, Alfian Noviyanto, Alvian Nurato , Nurato Nurul Islami, Nurul Pandriana, Aap Popy Yuliarty Pudjiwati, Sri Resista Vikaliana Resmi Bestari Muin Rinaldi, Ali Rini Anggraini Rita Sundari Robi Suherman Rohadi Satrio Budi Utomo Sawarni Hasibuan Siti Aishah Hasbullah Subekti Subekti Sudarma, Andi Firdaus Suhud, Khairi Sukoma, Sukoma Sundari, Rita Supaat Zakaria Surbakti, Muhammad Syukri Suyadi, Yadi Swandya Eka Pratiwi, Swandya Eka Syafrizal Fonna Tarigan, Kontan Teddy Kurniawan Thasyah Pitanova Vivi Friliandita Wahyu Irwansyah Wahyudi, Haris Wan Adil bin Wan Jamil Wan Adil Wan Jamil Winnugroho Wiratman, Manfaluthy Hakim, Tiara Aninditha, Aru W. Sudoyo, Joedo Prihartono Wiwit Suprihatiningsih Zakaria Zakaria Zulnazri, Z