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Syukri Arief
Andalas University
Agriculture, Biological Sciences & Forestry Astronomy Automotive Engineering Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Civil Engineering, Building, Construction & Architecture Computer Science & IT Control & Systems Engineering Earth & Planetary Sciences Education Energy Engineering Environmental Science Industrial & Manufacturing Engineering Materials Science & Nanotechnology Mathematics Mechanical Engineering Medicine & Pharmacology Nursing Physics Social Sciences Other

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Journal : INDONESIAN JOURNAL OF APPLIED PHYSICS

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Sintesis dan Karakterisasi Struktur dan Sifat Magnet Nanokomposit Fe3O4@PEG:ZnO Astuti Astuti; ihda khaira; syukri Arief; Sri Rahayu Alfitri Usna
INDONESIAN JOURNAL OF APPLIED PHYSICS Vol 12, No 2 (2022): October
Publisher : Department of Physics, Sebelas Maret University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.13057/ijap.v12i2.58514

Abstract

Fe3O4@PEG:ZnO nanocomposites were synthesized by the coprecipitation method with various of the samples were Fe3O4, Fe3O4@ZnO (1:1), Fe3O4@PEG: ZnO (1:2), and Fe3O4@ PEG: ZnO (1:3). The samples were synthesized with variation in the concentration of ZnO to Fe3O4. The concentration ratio of (Fe3O4:ZnO) were (1:1), (1:2), and (1:3). In addition, polyethylene glycol (PEG) is also used to prevent the agglomeration of Fe3O4. Sample characterization was carried out using X-Ray Diffraction (XRD), Transmission Electron Microscope (TEM), Fourier Transform Infrared (FTIR), Particle Size Analyzer (PSA), and vibrating Sample Magnetometer (VSM). The XRD patterns show that the sample is composed of Fe3O4phase and ZnO phase with crystal structure cubic and wurtzite respectively. The TEM image shows the formation of a core-shell structure where PEG: ZnO is the shell and Fe3O4 is the core. From the FTIR results, there are C-O and C-C bonds which indicate the formation of PEG, Fe-O bonds indicate the formation of Fe3O4 and Zn-O bonds indicate the formation of ZnO. Characterization with PSA obtained particle sizes of 33 nm, 23 nm, and 16 nm with particle size distributions of 25%, 50%, and 75% so that the average particle size is 24 nm. The VSM results show that Fe3O4@PEG: ZnO (1:2) nanocomposite has a high magnetic saturation of 66.58 emu/g, with superparamagnetic properties, which has the potential to be developed as a bioimaging material.
Co-Authors -, Emdeniz -, Rahmayeni -, Rianda -, Yulfitrin . Darwison . Syukri Abdi Dharma Abral, Hairul Ade saputra Ade Saputra Adlis Santoni Admi Admin Alief Admin Alif Admin Alif Admin Alif Admin Alif Admin Alif Ahmad Hafizullah Ritonga Aju Deska Alif, Admin Alif, Admin Alif, Admin Amelia Amir Anggresani, Lia Anwar Kasim Ariadi Hazmi Aritonang, Barita Astuti Astuti Aulia Arivin Billah Aulia Aulia Baharuddin Shaleh Boy Isfa Boy isfa Budi Hermawan BUSTANUL ARIFIN Denny Akbar Tanjung Denny Akbar Tanjung Desfitri, Erda Rahmilaila Deswati Deswati Devi Pebrina Eka Putra Waldi Ellyta Sari Emdeniz - Emriadi - Erda Rahmilaila Desfitri Evi Adhelina Fatiha, Widya Yuliani Fitri, Ernarisa Hamdi, Hayatul Hary Sanjaya Hayatul Hamdi Herlin Oktavani Hermansyah Aziz Hermawan, Budi ihda khaira Kazuhiro Manseki Khoirul Amru Kusuma, Theresia Sita Lestari Ningsih Lia Anggresani Lisa Utami Lisa Utami Lusi Puspitasari M. H. Ahmad Mahardika, Melbi Mai Efdi Mai Efdi Maria Erna Maria Erna Maria Erna Kustyawati Matlal Fajri Alif Melbi Mahardika Mirzah Mirzah Mochamad Asrofi Mohd Hafizi Ahmad Mohd Jain Noordin Muhammad Rizki Mulyati Sukma Naldi, Nofri Nancy Willian Nengsih, Zarnida Widia Neswati Neswati Nofri Naldi Novesar Jamarun Novesar Jamarun Novizar Nazir Oktavani, Herlin Olly Norita Tetra Putri Perdana Roza Radiatun Mardiah Rahadian Zainul Rahayu Rahayu Reni Desmiarti Reni Desmiarti Restina Bemis Restina Bemis, Restina Rianda - Rianda Rizal Rini Ramadhani Risma Sari Rosadi, Maulana Yusup Roza, Putri Perdana Rudy Fernandez Safni Safni Selfa Dewati Samah Sestry Misfadhila Shaleh, Baharuddin Sry Wahyuni Suarnikan Hulu Suci Auliya Rahmi Elsya Sumaryati Syukur Suryati Suryati Syukri Syukri Syukri Takashi Sugiura Theresia Sita Kusuma Upita Septiani Upita Septiani Usna, Sri Rahayu Alfitri Widya Yuliani Fatiha Yeni Stiadi Yessi Rahmayani Yestria Rilda Yetria Rilda Yetti Marlida Yulfitrin - Yulidar Laila Safitri Yulizar Yusuf Yurniwati Yurniwati Zilfa Zilfa Zulhadjri Zulhadjri