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All Journal VALENSI JURNAL KIMIA SAINS DAN APLIKASI Jurnal Ilmu Dasar Jurnal Natur Indonesia Sainstek TELKOMNIKA (Telecommunication Computing Electronics and Control) Jurnal Matematika & Sains Eksergi: Chemical Engineering Journal Jurnal Riset Kimia ROTOR: JURNAL ILMIAH TEKNIK MESIN Jurnal Kimia dan Kemasan PROSIDING SEMINAR KIMIA Chimica et Natura Acta INDONESIAN JOURNAL OF APPLIED PHYSICS ALCHEMY Jurnal Penelitian Kimia Indonesian Journal of Chemistry JURNAL PHOTON Eksakta : Berkala Ilmiah Bidang MIPA Indonesian Journal of Electrical Engineering and Computer Science Warta Pengabdian Andalas: Jurnal Ilmiah Pengembangan Dan Penerapan Ipteks Hydrogen: Jurnal Kependidikan Kimia Jurnal Kimia dan Kemasan AJARCDE (Asian Journal of Applied Research for Community Development and Empowerment) Makara Journal of Science SAINTI: Majalah Ilmiah Teknologi Industri Jurnal Kimia Unand
Syukri Arief
Andalas University
Agriculture, Biological Sciences & Forestry Astronomy Automotive Engineering Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Civil Engineering, Building, Construction & Architecture Computer Science & IT Control & Systems Engineering Earth & Planetary Sciences Education Energy Engineering Environmental Science Industrial & Manufacturing Engineering Materials Science & Nanotechnology Mathematics Mechanical Engineering Medicine & Pharmacology Nursing Physics Social Sciences Other

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Efektifitas Kitosan sebagai Inhibitor Korosi pada Baja Lunak dalam Air Gambut Erna, Maria; Emriadi, Emriadi; Alif, Admin; Arief, Syukri
Jurnal Natur Indonesia Vol 13, No 2 (2011)
Publisher : Lembaga Penelitian dan Pengabdian kepada Masyarakat Universitas Riau

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (70.13 KB) | DOI: 10.31258/jnat.13.2.118-122

Abstract

This research is intended to learn inhibition efficiency of mild steel corrosion in peat water using two type ofchitosan. First chitosan is without treatment and the second one is synthesized by ionotropic gelation method andthen is characterized by Fourier transform Infrared spectroscopy (FT-IR) and Scanning Electron Microscopy (SEM).Diameter of chitosan porous is about 500 nm which is measured based on morphological photo using SEM withinhomogeneous porous shape and porous distribution is unsmooth . Effect of chitin and chitosan on the corrosionof mild steel in peat water is studied using weight loss method. It is found that corrosion inhibition efficiencydepends on peat water pH, inhibition technique and interaction time. The results show that inhibition efficiency ofchitosan without treatment and with treatment are 88.73% and 93.32% respectively. The inhibition is assumed tooccur via physicsorption of the chitin and chitosan molecules on the metal surface. The Langmuir adsorptionisotherm is tested for their fit to the experimental data.
Sintesis dan Aplikasi Karboksimetil Kitosan sebagai Inhibitor Korosi pada Baja Karbon dalam Air Erna, Maria; Emriadi, Emriadi; Alif, Admin; Arief, Syukri; Noordin, Mohd Jain
Jurnal Natur Indonesia Vol 12, No 1 (2009)
Publisher : Lembaga Penelitian dan Pengabdian kepada Masyarakat Universitas Riau

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (351.132 KB) | DOI: 10.31258/jnat.12.1.87-92

Abstract

Carboxymethyl chitosan (CMC) was synthesized with different methods by reacting chitosan with monochloroaceticacid in the presence of sodium hydroxide under variation conditions. The above samples were characterized byFourier transform infrared spectroscopy (FTIR) and soluble in water in range of pH. The CMc were soluble in watera wide range of pH and applied as corrosion inhibitor for steel in water. The inhibiting influence of CMC was studiedby potentiodynamic polarization method. It was found thad corrosion rate was dependent on water pH and CMCconcentration. The results show that optimum the inhibition efficiency at pH 5 and 1 ppm concentration CMC, i.e.,77%. The adsorption of used compound on the steel surface obeys modified Langmuir isotherm. Polarizationmeasurement show that the CMC acts essentially as a anodic-type inhibitor.
Modifikasi dan Karakterisasi Titania (M-TiO2) Dengan Doping Ion Logam Transisi Feni dan Cuni Rilda, Yetria; Arief, Syukri; Dharma, Abdi; Alif, Admin
Jurnal Natur Indonesia Vol 12, No 2 (2010)
Publisher : Lembaga Penelitian dan Pengabdian kepada Masyarakat Universitas Riau

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (632.25 KB) | DOI: 10.31258/jnat.12.2.178-185

Abstract

Structure and size of titania nanoparticles have been modified with doping the transition metal (FeNiand CuNi) and controlling the calcinations temperature. Gel and M-TiO 2 powder were characterized byFT-IR showed the changed in intensity at 4000-400 cm-1. TG-DTA curve show the weigh of sample wasdecreased with the increasing of temperature 25-800°C. XRD pattern used to identify the titania structureshows the highest intensity of anatase at temperature calcination as 500°C. XRD of FeNi-TiO 2 and CuNi-TiO2 FeNi 10.5-41.9 nm and CuNi 12.1-33.5 converted using Debye-Scherrer’s equation and TEM analysisthe distribution of crystal size as FeNi-TiO2 and CuNi-TiO2 10-15 nm. SEM has shown that morphology ofdifferent surface from the FeNi-TiO 2 and CuNi-TiO 2 at different calcinations temperatures. Titaniacomposition can be determined by EDX analysis give as FeNi-TiO2 1:1, 97.01% and CuNi-TiO2 1:1, 94.63%respectly. The surface area has been determined by BET as FeNi-TiO 2 was 64.38 m2/g and CuNi-TiO2was 40.9 m2/g.
PEMBUATAN LAPISAN TIPIS TiO2 PADA PLAT KACA DENGAN METODA DIP-COATING DAN UJI AKTIVITAS FOTOKATALISNYA PADA AIR GAMBUT Sanjaya, Hary; Arief, Syukri; Alif, Admin
Sainstek VOL 07, NO 01, 2013
Publisher : Jurnal Sainstek

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (425.019 KB)

Abstract

It Has been studied the preparation of Titania thin film on glass plate by dip-coating method and their photocatalityc activity test in peat swamp water. This study is performed by using TIP as precursor and DEA as aditive in isopropanol. The addition of DEA affect the stability of titania solution. The titania thin film was made by dip-coating method on glass plate. The glass plate was coated on to titania solution, then dryed at 110 C for 10 minute and at 500 C for 30 minute. The titania coating on the glass plate was made by varying the titania concentration : 0,5 M ; 0,75 M and 1,0 M. Analiyzing of the products by XRD shown that the titania coating on the glass plate are in anatase form. By visual analysis an photo optic, the best film on the glass plate that is coated with titania 0,5 M solution. Based on the glass plate that is coated with titania 1,0 M solution with peat swamp water shown relative good (68,26%) fot the irradiation during 24 hours.
An optimized method of partial discharge data retrieval technique for phase resolved pattern Eka Putra Waldi; Aulia Aulia; Ariadi Hazmi; Hairul Abral; Syukri Arief; Mohd Hafizi Ahmad
TELKOMNIKA (Telecommunication Computing Electronics and Control) Vol 14, No 1: March 2016
Publisher : Universitas Ahmad Dahlan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.12928/telkomnika.v14i1.2602

Abstract

The measurement of phase resolved partial discharge requires a gigantic memory capacity to store all the waves of the PD test results. This limitation eventually hinders the testing. It is necessary to optimize on the aspect of memory storage capability to reduce the storage requirements. In light of foregoing, the partial discharge data retrieval techniques with sampling rate methods were used to detect the peak of partial discharge as well as the PD constituent representatives. The optimization process was performed by using integration of oscilloscope and LabVIEW software. The partial discharge data recording can be easily confined to the points of the partial discharge occurrence only. As results, the storage points were reduced by taking wave magnitude associated with PD, thereby resulting in more representative data. Therefore, this optimized method was able to reduce the file size of the test results up to 97 percent of PD original size thereby decreasing the usage of hard disk storage.
Sintesis dan Karakterisasi Nanopartikel Perak-Tricalcium Phosphate (TCP) dengan Bantuan Ekstrak Daun Alpukat (Percea americana) Yessi Rahmayani; Zulhadjri Zulhadjri; Syukri Arief
Jurnal Kimia Valensi Jurnal Kimia VALENSI Volume 5, No. 1, May 2019
Publisher : Syarif Hidayatullah State Islamic University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (793.553 KB) | DOI: 10.15408/jkv.v5i1.8652

Abstract

Sintesis nanopartikel perak-TCP telah dilakukan pada penelitian ini. Nanopartikel perak dibuat dengan mereduksi larutan perak nitrat dengan menggunakan ekstrak daun alpukat sebagai bioreduktor. Tricalsium Phosphate (TCP) dicelupkan kedalam nanopartikel perak membentuk komposit perak-tricalcium phosphate. Hasil analisis UV-Vis menunjukkan pembentukan puncak serapan nanopartikel perak pada panjang 445-446 nm, yakni puncak yang khas dari nanopartikel perak yang disebabkan oleh adanya fenomena Surface Plasmon Resonance (SPR). Penelitian ini menghasilkan perak-TCP dengan ukuran nanopartikel. Sesuai  hasil X-Ray Diffraction (XRD) yang menunjukkan bahwa ukuran kristal TCP adalah 64 nm dan ukuran Kristal perak dalam komposit adalah 46 nm. Hasil Scanning Electron Microscopy (SEM) menunjukan partikel perak terdistribusi dipermukaan partikel TCP. Kata Kunci: Komposit perak-TCP, nanopartikel perak, Percea americana,  tricalcium phosphate.  The silver-TCP nanoparticle synthesis was carried out in this study. Silver nanoparticles are made by reducing silver nitrate solution using avocado leaf extract as a bioreactor. Tricalcium Phosphate (TCP) is dipped into silver nanoparticles to form a silver-tricalcium phosphate composite. The UV-Vis analysis shows the formation of silver nanoparticle absorption peaks at a length of 445-446 nm, which is a typical peak of silver nanoparticles caused by the Surface Plasmon Resonance (SPR) phenomenon. X-Ray Diffraction (XRD) shows that the TCP crystal size is 64 nm and the size of the Silver Crystal in the composite is 46 nm. The results of Scanning Electron Microscopy (SEM) show silver particles distributed on the surface of TCP particles Keywords: Percea americana, silver-TCP composite, silver nanoparticle, tricalcium phosphate.
Pendekatan Green Synthesis Nanopartikel CuFe2O4 Dengan Bantuan Ekstrak Daun Gambir Dan Sifat Anti Bakterinya Suci Auliya Rahmi Elsya; Zulhadjri Zulhadjri; Syukri Arief
Jurnal Kimia dan Kemasan Vol. 41 No. 2 Oktober 2019
Publisher : Balai Besar Kimia dan Kemasan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24817/jkk.v41i2.5417

Abstract

Perkembangan nanoteknologi berkaitan dengan nanomaterial berfungsi untuk meningkatkan kemampuan antibakteri serta mengurangi jumlah pemakaian logam. Penelitian ini bertujuan untuk mengetahui pengaruh suhu, pH dan waktu sintesis hidrotermal terhadap karakteristik nanopartikel tembaga ferit (CuFe2O4­) yang selanjutnya diaplikasikan sebagai antibakteri. Nanopartikel tembaga ferit (NTF) telah disintesis dengan memadukan metode green sintesis dan hidrotermal. Ekstrak daun gambir (Uncaria gambir Roxb) digunakan sebagai capping agent dalam penelitian ini. Hasil analisis XRD memberikan informasi bahwa NTFyang disintesis dengan penambahan ekstrak daun gambir dan NaOH serta dengan penambahan NaOH saja pH 12 suhu 180˚C selama 8 jam berfase kubik. NTF yang disintesis dengan penambahan ekstrak daun gambir dan NaOH pH 12 suhu 180˚C selama 8 jam memiliki ukuran paling kecil yaitu 24nm. Dari hasil fotograf SEM diketahui NTF yang disintesis pada suhu 180˚C selama 8 jam pH 12 berbentuk spheric dan masih ada yang teraglomerasi. Nanopartikel tembaga ferit yang disintesis diaplikasikan pada bakteri gram positif (S.aureus) dan gram negatif (E.coli) menggunakan metode difusi sumuran. NTF yang disintesis pada suhu 180˚C selama 8 jam pH 10 dan 12 efektif menghambat pertumbuhan bakteri E. coli dan S. aureus.
Ekstrak Daun Andalas sebagai Capping Agent dalam Green Hydrothermal Synthesis Nanopartikel Mangan Ferrit dan Aplikasinya sebagai Antibakteri Lusi Puspitasari; Syukri Arief; Zulhadjri Zulhadjri
Chimica et Natura Acta Vol 7, No 1 (2019)
Publisher : Departemen Kimia

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (449.611 KB) | DOI: 10.24198/cna.v7.n1.19925

Abstract

Pada penelitian ini telah dilakukan sintesis nanopartikel MnFe2O4 secara hidrotermal menggunakan ekstrak daun andalas (M. macroura Miq.)  sebagai capping agent. Penelitian ini bertujuan untuk mengetahui pengaruh pH terhadap bentuk dan ukuran nanopartikel MnFe2O4. MnFe2O4 EN10 dan  MnFe2O4 EN12 disintesis menggunakan ekstrak daun andalas dan NaOH dengan pH masing-masing 10 dan 12, sementara MnFe2O4 N10 dan MnFe2O4 N12 disintesis tanpa menggunakan ekstrak daun andalas hanya dengan penambahan NaOH pada pH 10 dan 12. Hasil analisis X-Ray Diffraction (XRD) menunjukkan karakteristik MnFe2O4 spinel kubik  dengan ukuran kristal 11-16 nm, sedangkan MnFe2O4 E menunjukkan tidak terbentuknya spinel ferrit MnFe2O4 yang terbentuk hanya pengotor yaitu α-Fe2O3. Hasil karakterisasi Scanning Electron Microscopy (SEM) menunjukkan  bahwa morfologi nanopartikel MnFe2O4 berbentuk spheric. Nanopartikel MnFe2O4 diaplikasikan sebagai antibakteri terhadap bakteri S. aureus dan E. coli dengan metode sumur.
PENGARUH SUHU PADA PEMBENTUKAN PRECIPITATED CALCIUM CARBONATE (PCC) MELALUI METODA KAUSTIK SODA DENGAN MENGGUNAKAN PELARUT ASAM KLORIDA Budi Hermawan; Syukri Arief; Novesar Jamarun
Jurnal Riset Kimia Vol. 3 No. 1 (2009): September
Publisher : Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jrk.v3i1.36

Abstract

 ABSTRACT Precipitated Calcium Carbonate (PCC) is the limestone product resulting from certain process steps. By XRF measurement it has found that the content of CaO (oxide calcium) in limestone Bukit Tui Padang Panjang as follows 54.19%, SiO2 1.03%, Al2O3 0.39%, MgO 0.46% and Fe2O3 0.2%. Rendemen PCC at optimum concentration of 0.75 M HCl is 69.77%. The formation of PCC by using the highest PCC rendemen aquabides is 9.28% at optimum temperature of 50°C. With 0.75 M HCl, the highest rendemen is 79.32% at optimum temperature 70°C. The formation of crystals in the form vaterite, aragonite and calcite were evidenced by X-ray Diffraction (XRD). Treatment with 2.00 M HCl at 30°C showed the formation of vaterite (45.83%), aragonite (35.93%) and calcite (18.24%) with crystals size of 28.43 nm. In the other case, preparation with 0.75 M HCl at 30°C resulting the percentage of vaterite and aragonite which were 73.01% and 26.99% respectively fairished 28.06 nm. Then for the one which were treated with 0.75 M HCl at 70°C indicated the formation of vaterite (75.53%) fairished 33.68 nm and aragonite (24.47%). SEM (Scanning Electron Microscopy) towards the sample prepared from 0.75 M HCl at 30°C have clearly shown that the particle sphere fairished at 3.68 nm where the one treated with 0.75 M HCl at 70°C having particle sphere fairished at 3.3 µm showing needle like estimated of 3.8 µm. Keywords : Precipitated Calcium Carbonate (PCC), caustic soda method 
PEMBUATAN PRECIPITATED CALCIUM CARBONATE (PCC) DARI BATU KAPUR DENGAN METODA KAUSTIK SODA Novesar Jamarun; Yulfitrin -; Syukri Arief
Jurnal Riset Kimia Vol. 1 No. 1 (2007): September
Publisher : Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jrk.v1i1.54

Abstract

 ABSTRAK PCC dapat dihasilkan dari batu kapur melalui tiga metoda yaitu metoda solvay, karbonasi dan metoda kaustik soda.  Pada penelitian ini PCC disintesis dengan metoda kaustik soda yang dimodifikasi, yakni dengan mereaksikan batu kapur yang sudah dikalsinasi (CaO) dengan asam nitrat, membentuk garam kalsium nitrat yang mudah larut. Larutan garam yang terbentuk direaksikan dengan larutan natrium karbonat sehingga terbentuk endapan kalsium karbonat (PCC).  Berdasarkan analisis XRF kandungan CaO dalam batu kapur yang diambil dari 5 daerah (Halaban, Lintau Buo, Bukit Tui, Solok, Indarung) di Sumatera Barat berkisar antara 52,79% sampai 54,93%, dengan kandungan tertinggi pada daerah Lintau Buo (54,93%).   PCC yang dihasilkan paling banyak  diperoleh pada konsentrasi 2,00 M yaitu 96,52%.  Berdasarkan  analisis XRD, PCC mempunyai bentuk kristal kalsit dan vaterit  dengan ukuran kristal  13,95-14,02 nm, analisis dengan SEM menunjukkan partikel berbentuk kubus (kalsit)  dengan ukuran 2 µm.
Co-Authors -, Emdeniz -, Rahmayeni -, Rianda -, Yulfitrin . Darwison . Syukri Abdi Dharma Abral, Hairul Ade saputra Ade Saputra Adlis Santoni Admi Admin Alief Admin Alif Admin Alif Admin Alif Admin Alif Admin Alif Ahmad Hafizullah Ritonga Aju Deska Alif, Admin Alif, Admin Alif, Admin Amelia Amir Anggresani, Lia Anwar Kasim Ariadi Hazmi Aritonang, Barita Astuti Astuti Aulia Arivin Billah Aulia Aulia Baharuddin Shaleh Boy Isfa Boy isfa Budi Hermawan BUSTANUL ARIFIN Denny Akbar Tanjung Denny Akbar Tanjung Desfitri, Erda Rahmilaila Deswati Deswati Devi Pebrina Eka Putra Waldi Ellyta Sari Emdeniz - Emriadi - Erda Rahmilaila Desfitri Evi Adhelina Fatiha, Widya Yuliani Fitri, Ernarisa Hamdi, Hayatul Hary Sanjaya Hayatul Hamdi Herlin Oktavani Hermansyah Aziz Hermawan, Budi ihda khaira Kazuhiro Manseki Khoirul Amru Kusuma, Theresia Sita Lestari Ningsih Lia Anggresani Lisa Utami Lisa Utami Lusi Puspitasari M. H. Ahmad Mahardika, Melbi Mai Efdi Mai Efdi Maria Erna Maria Erna Maria Erna Kustyawati Matlal Fajri Alif Melbi Mahardika Mirzah Mirzah Mochamad Asrofi Mohd Hafizi Ahmad Mohd Jain Noordin Muhammad Rizki Mulyati Sukma Naldi, Nofri Nancy Willian Nengsih, Zarnida Widia Neswati Neswati Nofri Naldi Novesar Jamarun Novesar Jamarun Novizar Nazir Oktavani, Herlin Olly Norita Tetra Putri Perdana Roza Radiatun Mardiah Rahadian Zainul Rahayu Rahayu Reni Desmiarti Reni Desmiarti Restina Bemis Restina Bemis, Restina Rianda - Rianda Rizal Rini Ramadhani Risma Sari Rosadi, Maulana Yusup Roza, Putri Perdana Rudy Fernandez Safni Safni Selfa Dewati Samah Sestry Misfadhila Shaleh, Baharuddin Sry Wahyuni Suarnikan Hulu Suci Auliya Rahmi Elsya Sumaryati Syukur Suryati Suryati Syukri Syukri Syukri Takashi Sugiura Theresia Sita Kusuma Upita Septiani Upita Septiani Usna, Sri Rahayu Alfitri Widya Yuliani Fatiha Yeni Stiadi Yessi Rahmayani Yestria Rilda Yetria Rilda Yetti Marlida Yulfitrin - Yulidar Laila Safitri Yulizar Yusuf Yurniwati Yurniwati Zilfa Zilfa Zulhadjri Zulhadjri