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Journal : Transmisi

Effect of Electrodeposition Time on the Growth Rate of Carbon Nanotubes (CNTs) Faishol, Faishol; Andoko, Andoko; Suryanto, Heru; Prasetya, Riduwan
TRANSMISI Vol. 20 No. 2 (2024): September (2024)
Publisher : Universitas Merdeka Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26905/jtmt.v20i2.13672

Abstract

Carbon Nanotubes (CNTs) are nano-sized carbon that resembles tubes and has the potential to be used in various aspects of applications. Some of  the CNT carbon capture  methods include arc discharge, lasser ablation, CVD and electrodeposition. The advantage of the electrodeposition method is that the production cost is cheap and the preparation is easy. Electrodeposition is the precipitation of substances by using a direct electric current, with CO2 as the reactant. Factors that affect the growth rate of CNT are voltage, temperature, carbon source, electrode and time. The variation of the electorative time used was 60 minutes, 90 minutes, 120 minutes, 150 minutes, 180 minutes. The data collection process begins by shaping and measuring the weight of the electrode (Ni) with a diameter of 2 cm CNT deposition area. measuring the weight and melting Li2CO3 at a temperature of 750. then the CO2 flow rate setting, voltage setting  5V and time setting were then characterized by SEM-EDX and XRD. The results of the study showed that the optimal time obtained with a time of 120 minutes, the resulting CNT deposition rate was 1,618 g cm-2 h-1. Then based on the characterization of XRD and SEM, it shows that the longer the electrodeposition time, the less impurities are contained in the results obtained.
Effect of Temperature on the Growth Rate of Carbon Nanotubes (CNTs) using Electrodeposition Method Prabowo, Agung; Andoko, Andoko; Suryanto, Heru; Prasetya, Riduwan
TRANSMISI Vol. 20 No. 2 (2024): September (2024)
Publisher : Universitas Merdeka Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26905/jtmt.v20i2.13673

Abstract

Electrodeposition is one of the carbon capture methods used to produce carbon nanotubes with temperature as one of the variable. The research aims to analyze the effect of temperature on the growth rate of carbon nanotubes of 723oC, 750oC, 800oC, 850oC and 900oC using X-Ray Diffraction (XRD) testing. Analyzing deposit morphology at the same temperature using Scanning Electron Microscope (SEM) testing. The results of research show that the most optimal growth rate for carbon nanotubes occurred at 750oC of 7,949 g cm-2 hours-1. At a temperature of 750oC, carbon deposits are easier than at 723oC because that’s the melting point of lithium carbonate and has not completely decomposed. The XRD test show that at 750oC is the highest peak at 2θ= 26.21o. The SEM test show that the optimal morphological structure formed occurs at a temperature variation of 750oC with a fibrous morphology and little impurity at the ends. The results of the CNT percentage using the Material Analysis Using Diffraction (MAUD) method show that the largest quantitative value of the CNT percentage occurs at a temperature of 800oC of 4.08%.
Co-Authors Adhitya, Dewa Sukma Trinanda Agung Prabowo Ahmad Atif Fikri Aisyah Larasati Ali, Alamry Amasda, Naufal Rizky Aminnudin, Aminnudin Ananto, Rifqi Ryandi Dwi Andoko Andoko, Andoko Anni Faridah Apri Supii Arbianto, Ferian Rizki Ardianto Prasetiyo Asus Maizar Suryanto H Avita Ayu Permanasari Bili Darnanto Susilo Binoj, Joseph Selvi Daimon Syukri Dyah Kinasih Wuragil Eddy Rudianto Fadillah, Faqih Faishol, Faishol Fakris Muslim Fauliza, Tifa Femiana Gapsari MF Gian Suryanatha Hartawan Gunanti Mahasri Herly Evanuarini Iqbal, Ahmad Ismail, Mahrus Jibril Maulana Komarudin Komarudin Kris Witono M. Muhajir Malik Abdurrachman Manawan, Maykel Marsono Marsono Masera, Kemal Mito, Mohamed T Mufidah, Rhobithotus Muhamad Muhajir Muhamad Muhajir Muhamad Syaifuddin Muhammad Musa Muhammad Musa Muhammad Sumsanto Muhdi, Krisna Dwipa Murdanto, Putut Nanang Eko Wahyuningtiyas Nanang Eko Wahyuningtyas Nashrullah, Fikri Munif Navis, Akbar Nico Rahman Caesar Nusantara, Fajar Osman, Azlin Fazlina Pahlefi, Reval Panicker, Nithin Pradana, Yanuar Rohmat Aji Prasetya, Riduwan Pratama, Daniel Febrian Putra, Abyan Farras Rachmat Setiawibawa Ramadhan, Rahmad Ikrom Reddy .A. Dharmabintara Redyarsa Dharma Bintara Retno Wulandari Riyanto, Mochammad Deny Rizali, Dede Rr. Poppy Puspitasari Rudy Soenoko S.M.Shahrul N.S. Zahari Setyayunita, Tamaryska Sias, Quota Alief Subhan, Muhammad Ferindin Nuha Sudarno, Kurnia Agung Sukarni Sukarni Sukarni Sukarni Suprayitno Suprayitno Suprayitno Suprayitno Susilo, Bili Darnanto Syahtaria, Moh Ikhwan Tito Arif Sutrisno Uksan, Arifuddin Ulhaq, Ulfieda Anwar Utari, Inpita Casuarina Eqisetia Wardani, Nezya Pramudya Wiguna, Chrisrulita Sekaradi Wuragil, Dyah Kinasih Yanuar. R. A. Pradana Yanuhar, Uun Yudy Surya Irawan