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All Journal ILMU KELAUTAN: Indonesian Journal of Marine Sciences JURNAL KIMIA SAINS DAN APLIKASI Jurnal Ilmu Kimia Universitas Brawijaya Journal of Innovation and Applied Technology Indonesian Green Technology Journal The Journal of Pure and Applied Chemistry Research JURNAL INTEGRASI PROSES Journal of Geoscience, Engineering, Environment, and Technology JFMR (Journal of Fisheries and Marine Research) Indonesian Journal of Chemistry CARADDE: Jurnal Pengabdian Kepada Masyarakat Jurnal Kartika Kimia Molekul: Jurnal Ilmiah Kimia Acta Chimica Asiana Bulletin of Chemical Reaction Engineering & Catalysis
Yuniar Ponco Prananto
Department Chemistry, Faculty Of Mathematics And Natural Sciences, University Of Brawijaya, Jl. Veteran 65145, Malang, Indonesia
Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Earth & Planetary Sciences Education Engineering Environmental Science Materials Science & Nanotechnology Medicine & Pharmacology Physics Social Sciences Other

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Hydrothermal synthesis of crystalline Aluminium(III)-Tartrate: effect of tartrate type and molar ratio Yuniar Ponco Prananto; Danar Purwonugroho; M. Naufal Tsaqif Dzakwan; Tutik Setianingsih; Nidatul Syarifah
Acta Chimica Asiana Vol. 8 No. 1 (2025)
Publisher : The Indonesian Chemical Society, Chapter Nusa Tenggara and The University of Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29303/aca.v8i1.244

Abstract

Aluminium(III)-tartrate (Al-T) complex is a compound that commonly used as mordent in textile dyeing. This complex is soluble in hot water; thus, information on the isolation of crystallised Al-T is limited. Isolation of crystallised Al-T is needed to gain a high purity complex for further application in the textile industry. This study aims to synthesize and isolate crystalline complex of Al-T. Hydrothermal method was used to obtain the targeted complex. Effects of tartrate precursor and Al(III):tartrate mol ratio in the synthesis of Al-T complex were also investigated. The synthesis was done at 150 °C for 24 hours in several Al(III):tartrate mol ratios (1:2, 2:1, and 2:3) using two different tartrate precursors, namely L-tartaric acid and KNa-tartrate. The synthesized complexes were identified by infrared spectroscopy and powder-XRD analyses, and then further characterised by UV Vis - DRS, DTA-TGA, and SEM. Experimental data shows that the mol ratio affects the precipitation of the Al-T complex, in which a white crystalline solid was only precipitated out from the 2:1 reaction by both tartrate precursors. Different tartrate precursors used in the synthesis may alter the crystallization and result in an Al-T complex with slightly different thermal decomposition profile, UV-Vis DRS spectra profile, and different yield due to the different nature of the tartrate precursor. This finding is expected to support the possibility of Al-T mass production as mordent in textile dyeing
Co-Authors Adhinanda, Arrival Arsyad Adi Kurnia Soesantyo Adiba, Naila Azmi Afif Eka Rahma Setiyanto Agustina, Laily Aulia Ahmad Syarwani Andi Nafis An Naafi Andri Risdianto Andri Risdianto Ani Mulyasuryani Arie Srihardyastutie Ariesta, Muhammad Naufal Atsuhiko Isobe Choi, Jonghyun Danar Purwonugroho Danar Purwonugroho Danar Purwonugroho Danar Purwonugroho Danar Purwonugroho Danu Setia Wardana Darjito Darjito Darjito Defri Yona Degirmenci, Volkan Diana Ningrum, Diana Dias Satria Dini Tri Wahyuni Dini Tri Wahyuni Dyah Ajeng Pitaloka Efiria Riskah Efiria Riskah Elvian Eka Krisnaniningrum Evitantri, Mangesti Reza Fanny Prasetia Faustina De Yesu Prisila Abi Febriani, Rakhma Finisia, Yenni Firsta Luthfiani Salsabila Fuad, M.Arif Zainul Grafist, Therra Raditya Hadi Nur Hadi Nur Kashifa Maria Jihan Lai, Sin Yuan Ledhyane Ika Harlyan M. Naufal Tsaqif Dzakwan Mangesti Reza Evitantri Mochamad Arif Zainul Fuas Mochamad Nurcholis Mohammad Misbah Khunur Mohammad Misbah Khunur Mohammad Misbah Khunur Mohammad Misbah Khunur Muhammad Misbah Khunur Mukhamad Nurhadi, Mukhamad Naila Azmi Adiba Nazarudin Nidatul Syarifah Qonitah Fardiyah Rachmat Tjahjanto Rachmat Triandi Tjahjanto Radiansyah, Muhamad Agus Rafi Dwiasis Wibisono Rahmadani, Agung Rizky Arief Shobirin Rosmawati, Angelina Sasti Gona Fadhilah Silvi Zakiyatul Ilmiyah Sin Yuan Lai Siti Mutrofin Siti Mutrofin Soerja Koesnarpadi Sri Wardhani Suyono, Suyono Syarifah, Nidatul Taufiq, Muhammad Arif Teguh Wirawan Teguh Wirawan, Teguh Tutik Setianingsih Tutik Setianingsih Wenny Bekti Sunarharum Wirhanuddin, Wirhanuddin Yeni Dwi Lestari Yenni Finisia Yofandi, Muhammad Farrel Yoga Rizky Nata Yoga Rizky Nata Yogi Rifki Wijayanto Zhiying Zhu